Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis

Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moi...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Sivagami, Krishnasamy [verfasserIn] Tamizhdurai, Perumal [verfasserIn] Mujahed, Shaikh [verfasserIn] Nambi, Indumathi [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2020

Schlagwörter:	Tank bottom sludge Microwave process Pyrolysis Susceptor Recovery Furnace oil

Übergeordnetes Werk:	Enthalten in: Process safety and environmental protection - Amsterdam : Elsevier, 1990, 148, Seite 392-399
Übergeordnetes Werk:	volume:148 ; pages:392-399

DOI / URN:	10.1016/j.psep.2020.10.004

Katalog-ID:	ELV005795346

Internformat


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245	1	0	\|a Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis
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520			\|a Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. Char contains a higher percentage of carbon, Fe, Al, Ni, Pb, Cd, and S compounds.
650		4	\|a Tank bottom sludge
650		4	\|a Microwave process
650		4	\|a Pyrolysis
650		4	\|a Susceptor
650		4	\|a Recovery
650		4	\|a Furnace oil
700	1		\|a Tamizhdurai, Perumal \|e verfasserin \|4 aut
700	1		\|a Mujahed, Shaikh \|e verfasserin \|4 aut
700	1		\|a Nambi, Indumathi \|e verfasserin \|4 aut
773	0	8	\|i Enthalten in \|t Process safety and environmental protection \|d Amsterdam : Elsevier, 1990 \|g 148, Seite 392-399 \|h Online-Ressource \|w (DE-627)318710420 \|w (DE-600)2008004-9 \|w (DE-576)284747785 \|7 nnns
773	1	8	\|g volume:148 \|g pages:392-399
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936	b	k	\|a 58.18 \|j Chemische Betriebstechnik
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author_variant	k s ks p t pt s m sm i n in
matchkey_str	sivagamikrishnasamytamizhduraiperumalmuj:2020----:rcsotmztofrhrcvroolrmakotmldes
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publishDate	2020
allfields	10.1016/j.psep.2020.10.004 doi (DE-627)ELV005795346 (ELSEVIER)S0957-5820(20)31795-X DE-627 ger DE-627 rda eng 660 540 333.7 DE-600 58.18 bkl Sivagami, Krishnasamy verfasserin aut Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. Char contains a higher percentage of carbon, Fe, Al, Ni, Pb, Cd, and S compounds. Tank bottom sludge Microwave process Pyrolysis Susceptor Recovery Furnace oil Tamizhdurai, Perumal verfasserin aut Mujahed, Shaikh verfasserin aut Nambi, Indumathi verfasserin aut Enthalten in Process safety and environmental protection Amsterdam : Elsevier, 1990 148, Seite 392-399 Online-Ressource (DE-627)318710420 (DE-600)2008004-9 (DE-576)284747785 nnns volume:148 pages:392-399 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 58.18 Chemische Betriebstechnik AR 148 392-399
spelling	10.1016/j.psep.2020.10.004 doi (DE-627)ELV005795346 (ELSEVIER)S0957-5820(20)31795-X DE-627 ger DE-627 rda eng 660 540 333.7 DE-600 58.18 bkl Sivagami, Krishnasamy verfasserin aut Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. Char contains a higher percentage of carbon, Fe, Al, Ni, Pb, Cd, and S compounds. Tank bottom sludge Microwave process Pyrolysis Susceptor Recovery Furnace oil Tamizhdurai, Perumal verfasserin aut Mujahed, Shaikh verfasserin aut Nambi, Indumathi verfasserin aut Enthalten in Process safety and environmental protection Amsterdam : Elsevier, 1990 148, Seite 392-399 Online-Ressource (DE-627)318710420 (DE-600)2008004-9 (DE-576)284747785 nnns volume:148 pages:392-399 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 58.18 Chemische Betriebstechnik AR 148 392-399
allfields_unstemmed	10.1016/j.psep.2020.10.004 doi (DE-627)ELV005795346 (ELSEVIER)S0957-5820(20)31795-X DE-627 ger DE-627 rda eng 660 540 333.7 DE-600 58.18 bkl Sivagami, Krishnasamy verfasserin aut Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. Char contains a higher percentage of carbon, Fe, Al, Ni, Pb, Cd, and S compounds. Tank bottom sludge Microwave process Pyrolysis Susceptor Recovery Furnace oil Tamizhdurai, Perumal verfasserin aut Mujahed, Shaikh verfasserin aut Nambi, Indumathi verfasserin aut Enthalten in Process safety and environmental protection Amsterdam : Elsevier, 1990 148, Seite 392-399 Online-Ressource (DE-627)318710420 (DE-600)2008004-9 (DE-576)284747785 nnns volume:148 pages:392-399 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 58.18 Chemische Betriebstechnik AR 148 392-399
allfieldsGer	10.1016/j.psep.2020.10.004 doi (DE-627)ELV005795346 (ELSEVIER)S0957-5820(20)31795-X DE-627 ger DE-627 rda eng 660 540 333.7 DE-600 58.18 bkl Sivagami, Krishnasamy verfasserin aut Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. Char contains a higher percentage of carbon, Fe, Al, Ni, Pb, Cd, and S compounds. Tank bottom sludge Microwave process Pyrolysis Susceptor Recovery Furnace oil Tamizhdurai, Perumal verfasserin aut Mujahed, Shaikh verfasserin aut Nambi, Indumathi verfasserin aut Enthalten in Process safety and environmental protection Amsterdam : Elsevier, 1990 148, Seite 392-399 Online-Ressource (DE-627)318710420 (DE-600)2008004-9 (DE-576)284747785 nnns volume:148 pages:392-399 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 58.18 Chemische Betriebstechnik AR 148 392-399
allfieldsSound	10.1016/j.psep.2020.10.004 doi (DE-627)ELV005795346 (ELSEVIER)S0957-5820(20)31795-X DE-627 ger DE-627 rda eng 660 540 333.7 DE-600 58.18 bkl Sivagami, Krishnasamy verfasserin aut Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis 2020 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. Char contains a higher percentage of carbon, Fe, Al, Ni, Pb, Cd, and S compounds. Tank bottom sludge Microwave process Pyrolysis Susceptor Recovery Furnace oil Tamizhdurai, Perumal verfasserin aut Mujahed, Shaikh verfasserin aut Nambi, Indumathi verfasserin aut Enthalten in Process safety and environmental protection Amsterdam : Elsevier, 1990 148, Seite 392-399 Online-Ressource (DE-627)318710420 (DE-600)2008004-9 (DE-576)284747785 nnns volume:148 pages:392-399 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2031 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2108 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2119 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_2548 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 58.18 Chemische Betriebstechnik AR 148 392-399
language	English
source	Enthalten in Process safety and environmental protection 148, Seite 392-399 volume:148 pages:392-399
sourceStr	Enthalten in Process safety and environmental protection 148, Seite 392-399 volume:148 pages:392-399
format_phy_str_mv	Article
bklname	Chemische Betriebstechnik
institution	findex.gbv.de
topic_facet	Tank bottom sludge Microwave process Pyrolysis Susceptor Recovery Furnace oil
dewey-raw	660
isfreeaccess_bool	false
container_title	Process safety and environmental protection
authorswithroles_txt_mv	Sivagami, Krishnasamy @@aut@@ Tamizhdurai, Perumal @@aut@@ Mujahed, Shaikh @@aut@@ Nambi, Indumathi @@aut@@
publishDateDaySort_date	2020-01-01T00:00:00Z
hierarchy_top_id	318710420
dewey-sort	3660
id	ELV005795346
language_de	englisch
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author	Sivagami, Krishnasamy
spellingShingle	Sivagami, Krishnasamy ddc 660 bkl 58.18 misc Tank bottom sludge misc Microwave process misc Pyrolysis misc Susceptor misc Recovery misc Furnace oil Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis
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topic_title	660 540 333.7 DE-600 58.18 bkl Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis Tank bottom sludge Microwave process Pyrolysis Susceptor Recovery Furnace oil
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title	Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis
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title_full	Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis
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title_sort	process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis
title_auth	Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis
abstract	Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. Char contains a higher percentage of carbon, Fe, Al, Ni, Pb, Cd, and S compounds.
abstractGer	Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. Char contains a higher percentage of carbon, Fe, Al, Ni, Pb, Cd, and S compounds.
abstract_unstemmed	Petroleum refining generates hazardous sludge with polyaromatic hydrocarbons and heavy metals. The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. Char contains a higher percentage of carbon, Fe, Al, Ni, Pb, Cd, and S compounds.
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title_short	Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis
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up_date	2024-07-06T19:11:21.105Z
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The main objective of the study was to evaluate the performance of microwave pyrolysis for the recovery of oil from furnace oil sludge. The characteristics of furnace oil tank bottom sludge such as pH, moisture, viscosity, and volatile hydrocarbon content were determined. Thermal Gravimetric Analysis has been done to determine the cracking and degradation range of oily sludge. Gas Chromatography-Mass Spectrometry was used to fingerprint the hydrocarbon. Pyrolysis experiments were conducted in lab-scale pyrolysis set up with different susceptors and sludge in a specific weight ratio. The process parameters like microwave power, sludge: susceptor ratio were optimized to increase the oil yield. Graphite mixed sludge in 1:5 ratio at 450 W power shown higher oil yield. The calorific value of oil and char were determined as 44,442.9 and 16,686.58 kJ /kg. Physicochemical characteristics of oil such as flash point, density, and kinematic viscosity are 94 °C, 874.9, kg/m3, and 4.063 cSt. Cetane index and sulfur content were measured as 40.9, 6.85 g/kg respectively. The gas analysis had shown the presence of H2, CO2, CO, and CH4 compounds. 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Process optimization for the recovery of oil from tank bottom sludge using microwave pyrolysis

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