A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin

To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Cao, Jianfan [verfasserIn] Duan, Huajun [verfasserIn] Zou, Jiahao [verfasserIn] Zhang, Junjun [verfasserIn] Ma, Huiru [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2021

Schlagwörter:	Epoxy resin Bio-based Co-curing agent Flame retardance Mechanical properties

Übergeordnetes Werk:	Enthalten in: Polymer degradation and stability - Amsterdam [u.a.] : Elsevier Science, 1979, 187
Übergeordnetes Werk:	volume:187

DOI / URN:	10.1016/j.polymdegradstab.2021.109548

Katalog-ID:	ELV005833167

Internformat


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245	1	0	\|a A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin
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520			\|a To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully synthesized via one-pot method, and served as co-curing agent of DDM to prepare the flame-retardant EP. The structure of VFD was characterized by Fourier transform infrared (FTIR) spectra and nuclear magnetic resonance (NMR). The addition of VFD accelerated the crosslinking reaction of epoxy system and improved the flame retardance of EP. With VFD content was 7.5 wt% (only 0.52 wt% phosphorus was loaded), EP/VFD-7.5 achieved vertical burning (UL-94) V-0 rating and its limited oxygen index (LOI) value increased to 34.5%. Besides, compared with EP, the peak heat release rate (PHRR) of EP/VFD-7.5 decreased by 28% in cone calorimeter (CC) test. The analysis of char residue and pyrolysis behavior confirmed that VFD exerted bi-phase flame-retardant effect. In spite of the decrease of flame-retardant EPs’ Tg, the tensile and flexural strengths of EP/VFD-10 increased by 45% and 29%, respectively. All the results indicated the great potential of VFD for practical application in future.
650		4	\|a Epoxy resin
650		4	\|a Bio-based
650		4	\|a Co-curing agent
650		4	\|a Flame retardance
650		4	\|a Mechanical properties
700	1		\|a Duan, Huajun \|e verfasserin \|4 aut
700	1		\|a Zou, Jiahao \|e verfasserin \|4 aut
700	1		\|a Zhang, Junjun \|e verfasserin \|4 aut
700	1		\|a Ma, Huiru \|e verfasserin \|4 aut
773	0	8	\|i Enthalten in \|t Polymer degradation and stability \|d Amsterdam [u.a.] : Elsevier Science, 1979 \|g 187 \|h Online-Ressource \|w (DE-627)308447352 \|w (DE-600)1502217-1 \|w (DE-576)259484288 \|7 nnns
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936	b	k	\|a 51.70 \|j Polymerwerkstoffe \|j Kunststoffe \|x Werkstoffkunde
936	b	k	\|a 35.80 \|j Makromolekulare Chemie
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952			\|d 187

Indexfelder

author_variant	j c jc h d hd j z jz j z jz h m hm
matchkey_str	caojianfanduanhuajunzoujiahaozhangjunjun:2021----:boaepopoucnannccrnaetoadecletlmrtracadeh
hierarchy_sort_str	2021
bklnumber	51.70 35.80
publishDate	2021
allfields	10.1016/j.polymdegradstab.2021.109548 doi (DE-627)ELV005833167 (ELSEVIER)S0141-3910(21)00068-9 DE-627 ger DE-627 rda eng 540 660 DE-600 51.70 bkl 35.80 bkl Cao, Jianfan verfasserin aut A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully synthesized via one-pot method, and served as co-curing agent of DDM to prepare the flame-retardant EP. The structure of VFD was characterized by Fourier transform infrared (FTIR) spectra and nuclear magnetic resonance (NMR). The addition of VFD accelerated the crosslinking reaction of epoxy system and improved the flame retardance of EP. With VFD content was 7.5 wt% (only 0.52 wt% phosphorus was loaded), EP/VFD-7.5 achieved vertical burning (UL-94) V-0 rating and its limited oxygen index (LOI) value increased to 34.5%. Besides, compared with EP, the peak heat release rate (PHRR) of EP/VFD-7.5 decreased by 28% in cone calorimeter (CC) test. The analysis of char residue and pyrolysis behavior confirmed that VFD exerted bi-phase flame-retardant effect. In spite of the decrease of flame-retardant EPs’ Tg, the tensile and flexural strengths of EP/VFD-10 increased by 45% and 29%, respectively. All the results indicated the great potential of VFD for practical application in future. Epoxy resin Bio-based Co-curing agent Flame retardance Mechanical properties Duan, Huajun verfasserin aut Zou, Jiahao verfasserin aut Zhang, Junjun verfasserin aut Ma, Huiru verfasserin aut Enthalten in Polymer degradation and stability Amsterdam [u.a.] : Elsevier Science, 1979 187 Online-Ressource (DE-627)308447352 (DE-600)1502217-1 (DE-576)259484288 nnns volume:187 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.70 Polymerwerkstoffe Kunststoffe Werkstoffkunde 35.80 Makromolekulare Chemie AR 187
spelling	10.1016/j.polymdegradstab.2021.109548 doi (DE-627)ELV005833167 (ELSEVIER)S0141-3910(21)00068-9 DE-627 ger DE-627 rda eng 540 660 DE-600 51.70 bkl 35.80 bkl Cao, Jianfan verfasserin aut A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully synthesized via one-pot method, and served as co-curing agent of DDM to prepare the flame-retardant EP. The structure of VFD was characterized by Fourier transform infrared (FTIR) spectra and nuclear magnetic resonance (NMR). The addition of VFD accelerated the crosslinking reaction of epoxy system and improved the flame retardance of EP. With VFD content was 7.5 wt% (only 0.52 wt% phosphorus was loaded), EP/VFD-7.5 achieved vertical burning (UL-94) V-0 rating and its limited oxygen index (LOI) value increased to 34.5%. Besides, compared with EP, the peak heat release rate (PHRR) of EP/VFD-7.5 decreased by 28% in cone calorimeter (CC) test. The analysis of char residue and pyrolysis behavior confirmed that VFD exerted bi-phase flame-retardant effect. In spite of the decrease of flame-retardant EPs’ Tg, the tensile and flexural strengths of EP/VFD-10 increased by 45% and 29%, respectively. All the results indicated the great potential of VFD for practical application in future. Epoxy resin Bio-based Co-curing agent Flame retardance Mechanical properties Duan, Huajun verfasserin aut Zou, Jiahao verfasserin aut Zhang, Junjun verfasserin aut Ma, Huiru verfasserin aut Enthalten in Polymer degradation and stability Amsterdam [u.a.] : Elsevier Science, 1979 187 Online-Ressource (DE-627)308447352 (DE-600)1502217-1 (DE-576)259484288 nnns volume:187 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.70 Polymerwerkstoffe Kunststoffe Werkstoffkunde 35.80 Makromolekulare Chemie AR 187
allfields_unstemmed	10.1016/j.polymdegradstab.2021.109548 doi (DE-627)ELV005833167 (ELSEVIER)S0141-3910(21)00068-9 DE-627 ger DE-627 rda eng 540 660 DE-600 51.70 bkl 35.80 bkl Cao, Jianfan verfasserin aut A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully synthesized via one-pot method, and served as co-curing agent of DDM to prepare the flame-retardant EP. The structure of VFD was characterized by Fourier transform infrared (FTIR) spectra and nuclear magnetic resonance (NMR). The addition of VFD accelerated the crosslinking reaction of epoxy system and improved the flame retardance of EP. With VFD content was 7.5 wt% (only 0.52 wt% phosphorus was loaded), EP/VFD-7.5 achieved vertical burning (UL-94) V-0 rating and its limited oxygen index (LOI) value increased to 34.5%. Besides, compared with EP, the peak heat release rate (PHRR) of EP/VFD-7.5 decreased by 28% in cone calorimeter (CC) test. The analysis of char residue and pyrolysis behavior confirmed that VFD exerted bi-phase flame-retardant effect. In spite of the decrease of flame-retardant EPs’ Tg, the tensile and flexural strengths of EP/VFD-10 increased by 45% and 29%, respectively. All the results indicated the great potential of VFD for practical application in future. Epoxy resin Bio-based Co-curing agent Flame retardance Mechanical properties Duan, Huajun verfasserin aut Zou, Jiahao verfasserin aut Zhang, Junjun verfasserin aut Ma, Huiru verfasserin aut Enthalten in Polymer degradation and stability Amsterdam [u.a.] : Elsevier Science, 1979 187 Online-Ressource (DE-627)308447352 (DE-600)1502217-1 (DE-576)259484288 nnns volume:187 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.70 Polymerwerkstoffe Kunststoffe Werkstoffkunde 35.80 Makromolekulare Chemie AR 187
allfieldsGer	10.1016/j.polymdegradstab.2021.109548 doi (DE-627)ELV005833167 (ELSEVIER)S0141-3910(21)00068-9 DE-627 ger DE-627 rda eng 540 660 DE-600 51.70 bkl 35.80 bkl Cao, Jianfan verfasserin aut A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully synthesized via one-pot method, and served as co-curing agent of DDM to prepare the flame-retardant EP. The structure of VFD was characterized by Fourier transform infrared (FTIR) spectra and nuclear magnetic resonance (NMR). The addition of VFD accelerated the crosslinking reaction of epoxy system and improved the flame retardance of EP. With VFD content was 7.5 wt% (only 0.52 wt% phosphorus was loaded), EP/VFD-7.5 achieved vertical burning (UL-94) V-0 rating and its limited oxygen index (LOI) value increased to 34.5%. Besides, compared with EP, the peak heat release rate (PHRR) of EP/VFD-7.5 decreased by 28% in cone calorimeter (CC) test. The analysis of char residue and pyrolysis behavior confirmed that VFD exerted bi-phase flame-retardant effect. In spite of the decrease of flame-retardant EPs’ Tg, the tensile and flexural strengths of EP/VFD-10 increased by 45% and 29%, respectively. All the results indicated the great potential of VFD for practical application in future. Epoxy resin Bio-based Co-curing agent Flame retardance Mechanical properties Duan, Huajun verfasserin aut Zou, Jiahao verfasserin aut Zhang, Junjun verfasserin aut Ma, Huiru verfasserin aut Enthalten in Polymer degradation and stability Amsterdam [u.a.] : Elsevier Science, 1979 187 Online-Ressource (DE-627)308447352 (DE-600)1502217-1 (DE-576)259484288 nnns volume:187 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.70 Polymerwerkstoffe Kunststoffe Werkstoffkunde 35.80 Makromolekulare Chemie AR 187
allfieldsSound	10.1016/j.polymdegradstab.2021.109548 doi (DE-627)ELV005833167 (ELSEVIER)S0141-3910(21)00068-9 DE-627 ger DE-627 rda eng 540 660 DE-600 51.70 bkl 35.80 bkl Cao, Jianfan verfasserin aut A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully synthesized via one-pot method, and served as co-curing agent of DDM to prepare the flame-retardant EP. The structure of VFD was characterized by Fourier transform infrared (FTIR) spectra and nuclear magnetic resonance (NMR). The addition of VFD accelerated the crosslinking reaction of epoxy system and improved the flame retardance of EP. With VFD content was 7.5 wt% (only 0.52 wt% phosphorus was loaded), EP/VFD-7.5 achieved vertical burning (UL-94) V-0 rating and its limited oxygen index (LOI) value increased to 34.5%. Besides, compared with EP, the peak heat release rate (PHRR) of EP/VFD-7.5 decreased by 28% in cone calorimeter (CC) test. The analysis of char residue and pyrolysis behavior confirmed that VFD exerted bi-phase flame-retardant effect. In spite of the decrease of flame-retardant EPs’ Tg, the tensile and flexural strengths of EP/VFD-10 increased by 45% and 29%, respectively. All the results indicated the great potential of VFD for practical application in future. Epoxy resin Bio-based Co-curing agent Flame retardance Mechanical properties Duan, Huajun verfasserin aut Zou, Jiahao verfasserin aut Zhang, Junjun verfasserin aut Ma, Huiru verfasserin aut Enthalten in Polymer degradation and stability Amsterdam [u.a.] : Elsevier Science, 1979 187 Online-Ressource (DE-627)308447352 (DE-600)1502217-1 (DE-576)259484288 nnns volume:187 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.70 Polymerwerkstoffe Kunststoffe Werkstoffkunde 35.80 Makromolekulare Chemie AR 187
language	English
source	Enthalten in Polymer degradation and stability 187 volume:187
sourceStr	Enthalten in Polymer degradation and stability 187 volume:187
format_phy_str_mv	Article
bklname	Polymerwerkstoffe Kunststoffe Makromolekulare Chemie
institution	findex.gbv.de
topic_facet	Epoxy resin Bio-based Co-curing agent Flame retardance Mechanical properties
dewey-raw	540
isfreeaccess_bool	false
container_title	Polymer degradation and stability
authorswithroles_txt_mv	Cao, Jianfan @@aut@@ Duan, Huajun @@aut@@ Zou, Jiahao @@aut@@ Zhang, Junjun @@aut@@ Ma, Huiru @@aut@@
publishDateDaySort_date	2021-01-01T00:00:00Z
hierarchy_top_id	308447352
dewey-sort	3540
id	ELV005833167
language_de	englisch
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author	Cao, Jianfan
spellingShingle	Cao, Jianfan ddc 540 bkl 51.70 bkl 35.80 misc Epoxy resin misc Bio-based misc Co-curing agent misc Flame retardance misc Mechanical properties A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin
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topic_title	540 660 DE-600 51.70 bkl 35.80 bkl A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin Epoxy resin Bio-based Co-curing agent Flame retardance Mechanical properties
topic	ddc 540 bkl 51.70 bkl 35.80 misc Epoxy resin misc Bio-based misc Co-curing agent misc Flame retardance misc Mechanical properties
topic_unstemmed	ddc 540 bkl 51.70 bkl 35.80 misc Epoxy resin misc Bio-based misc Co-curing agent misc Flame retardance misc Mechanical properties
topic_browse	ddc 540 bkl 51.70 bkl 35.80 misc Epoxy resin misc Bio-based misc Co-curing agent misc Flame retardance misc Mechanical properties
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title	A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin
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title_full	A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin
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author_browse	Cao, Jianfan Duan, Huajun Zou, Jiahao Zhang, Junjun Ma, Huiru
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doi_str_mv	10.1016/j.polymdegradstab.2021.109548
dewey-full	540 660
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title_sort	a bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin
title_auth	A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin
abstract	To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully synthesized via one-pot method, and served as co-curing agent of DDM to prepare the flame-retardant EP. The structure of VFD was characterized by Fourier transform infrared (FTIR) spectra and nuclear magnetic resonance (NMR). The addition of VFD accelerated the crosslinking reaction of epoxy system and improved the flame retardance of EP. With VFD content was 7.5 wt% (only 0.52 wt% phosphorus was loaded), EP/VFD-7.5 achieved vertical burning (UL-94) V-0 rating and its limited oxygen index (LOI) value increased to 34.5%. Besides, compared with EP, the peak heat release rate (PHRR) of EP/VFD-7.5 decreased by 28% in cone calorimeter (CC) test. The analysis of char residue and pyrolysis behavior confirmed that VFD exerted bi-phase flame-retardant effect. In spite of the decrease of flame-retardant EPs’ Tg, the tensile and flexural strengths of EP/VFD-10 increased by 45% and 29%, respectively. All the results indicated the great potential of VFD for practical application in future.
abstractGer	To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully synthesized via one-pot method, and served as co-curing agent of DDM to prepare the flame-retardant EP. The structure of VFD was characterized by Fourier transform infrared (FTIR) spectra and nuclear magnetic resonance (NMR). The addition of VFD accelerated the crosslinking reaction of epoxy system and improved the flame retardance of EP. With VFD content was 7.5 wt% (only 0.52 wt% phosphorus was loaded), EP/VFD-7.5 achieved vertical burning (UL-94) V-0 rating and its limited oxygen index (LOI) value increased to 34.5%. Besides, compared with EP, the peak heat release rate (PHRR) of EP/VFD-7.5 decreased by 28% in cone calorimeter (CC) test. The analysis of char residue and pyrolysis behavior confirmed that VFD exerted bi-phase flame-retardant effect. In spite of the decrease of flame-retardant EPs’ Tg, the tensile and flexural strengths of EP/VFD-10 increased by 45% and 29%, respectively. All the results indicated the great potential of VFD for practical application in future.
abstract_unstemmed	To cater for the requirement of environmental protection, flame retardance and mechanical properties in some special fields for epoxy resin, a bio-based reactive flame retardant (VFD) derived from vanillin, furfurylamine and 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) was successfully synthesized via one-pot method, and served as co-curing agent of DDM to prepare the flame-retardant EP. The structure of VFD was characterized by Fourier transform infrared (FTIR) spectra and nuclear magnetic resonance (NMR). The addition of VFD accelerated the crosslinking reaction of epoxy system and improved the flame retardance of EP. With VFD content was 7.5 wt% (only 0.52 wt% phosphorus was loaded), EP/VFD-7.5 achieved vertical burning (UL-94) V-0 rating and its limited oxygen index (LOI) value increased to 34.5%. Besides, compared with EP, the peak heat release rate (PHRR) of EP/VFD-7.5 decreased by 28% in cone calorimeter (CC) test. The analysis of char residue and pyrolysis behavior confirmed that VFD exerted bi-phase flame-retardant effect. In spite of the decrease of flame-retardant EPs’ Tg, the tensile and flexural strengths of EP/VFD-10 increased by 45% and 29%, respectively. All the results indicated the great potential of VFD for practical application in future.
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title_short	A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin
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author2	Duan, Huajun Zou, Jiahao Zhang, Junjun Ma, Huiru
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doi_str	10.1016/j.polymdegradstab.2021.109548
up_date	2024-07-06T19:19:13.882Z
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A bio-based phosphorus-containing co-curing agent towards excellent flame retardance and mechanical properties of epoxy resin

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