Quantification of Buckminsterfullerene (C

In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural un...
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Autor*in:	Sharma, Swati [verfasserIn] Zorzi, Sandro [verfasserIn] Cristiglio, Viviana [verfasserIn] Schweins, Ralf [verfasserIn] Mondelli, Claudia [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2021

Schlagwörter:	Non-graphitizing carbon Fullerene Small angle neutron scattering Glass-like carbon Pyrolysis

Übergeordnetes Werk:	Enthalten in: Carbon - Amsterdam [u.a.] : Elsevier Science, 1963, 189, Seite 362-368
Übergeordnetes Werk:	volume:189 ; pages:362-368

DOI / URN:	10.1016/j.carbon.2021.12.062

Katalog-ID:	ELV00730546X

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520			\|a In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural units in non-graphitizing carbons. It has been proposed that a certain fraction of completely closed spherical fullerenes, such as C60, is also present in these materials. Strongly curved structures are not expected to exist in graphitizing carbons. We report on a Small Angle Neutron Scattering (SANS) investigation conducted at the Institut Laue-Langevin, Grenoble, France, that enables us to (i) quantify C60 in a non-graphitizing carbon, (ii) investigate the evolution patterns of graphitizing and non-graphitizing carbons, and (iii) perform a detailed SANS analysis of pure crystalline C60 in dry powder form. We also revisit the formation patterns of slightly larger structures (3–5 nm) such as graphitic crystallites and voids in both classes of polymeric carbon. These results provide a strong evidence in support of the fullerene-like microstructural models of non-graphitizing carbon, adding that the curved structural units are not just “fullerene-like”, but also spherical fullerenes, C60 in particular.
650		4	\|a Non-graphitizing carbon
650		4	\|a Fullerene
650		4	\|a Small angle neutron scattering
650		4	\|a Glass-like carbon
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700	1		\|a Schweins, Ralf \|e verfasserin \|0 (orcid)0000-0001-8078-2089 \|4 aut
700	1		\|a Mondelli, Claudia \|e verfasserin \|0 (orcid)0000-0002-5452-5238 \|4 aut
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allfields	10.1016/j.carbon.2021.12.062 doi (DE-627)ELV00730546X (ELSEVIER)S0008-6223(21)01221-5 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Sharma, Swati verfasserin (orcid)0000-0003-0566-0270 aut Quantification of Buckminsterfullerene (C 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural units in non-graphitizing carbons. It has been proposed that a certain fraction of completely closed spherical fullerenes, such as C60, is also present in these materials. Strongly curved structures are not expected to exist in graphitizing carbons. We report on a Small Angle Neutron Scattering (SANS) investigation conducted at the Institut Laue-Langevin, Grenoble, France, that enables us to (i) quantify C60 in a non-graphitizing carbon, (ii) investigate the evolution patterns of graphitizing and non-graphitizing carbons, and (iii) perform a detailed SANS analysis of pure crystalline C60 in dry powder form. We also revisit the formation patterns of slightly larger structures (3–5 nm) such as graphitic crystallites and voids in both classes of polymeric carbon. These results provide a strong evidence in support of the fullerene-like microstructural models of non-graphitizing carbon, adding that the curved structural units are not just “fullerene-like”, but also spherical fullerenes, C60 in particular. Non-graphitizing carbon Fullerene Small angle neutron scattering Glass-like carbon Pyrolysis Zorzi, Sandro verfasserin (orcid)0000-0001-5024-9478 aut Cristiglio, Viviana verfasserin (orcid)0000-0003-3608-9222 aut Schweins, Ralf verfasserin (orcid)0000-0001-8078-2089 aut Mondelli, Claudia verfasserin (orcid)0000-0002-5452-5238 aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 189, Seite 362-368 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:189 pages:362-368 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 189 362-368
spelling	10.1016/j.carbon.2021.12.062 doi (DE-627)ELV00730546X (ELSEVIER)S0008-6223(21)01221-5 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Sharma, Swati verfasserin (orcid)0000-0003-0566-0270 aut Quantification of Buckminsterfullerene (C 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural units in non-graphitizing carbons. It has been proposed that a certain fraction of completely closed spherical fullerenes, such as C60, is also present in these materials. Strongly curved structures are not expected to exist in graphitizing carbons. We report on a Small Angle Neutron Scattering (SANS) investigation conducted at the Institut Laue-Langevin, Grenoble, France, that enables us to (i) quantify C60 in a non-graphitizing carbon, (ii) investigate the evolution patterns of graphitizing and non-graphitizing carbons, and (iii) perform a detailed SANS analysis of pure crystalline C60 in dry powder form. We also revisit the formation patterns of slightly larger structures (3–5 nm) such as graphitic crystallites and voids in both classes of polymeric carbon. These results provide a strong evidence in support of the fullerene-like microstructural models of non-graphitizing carbon, adding that the curved structural units are not just “fullerene-like”, but also spherical fullerenes, C60 in particular. Non-graphitizing carbon Fullerene Small angle neutron scattering Glass-like carbon Pyrolysis Zorzi, Sandro verfasserin (orcid)0000-0001-5024-9478 aut Cristiglio, Viviana verfasserin (orcid)0000-0003-3608-9222 aut Schweins, Ralf verfasserin (orcid)0000-0001-8078-2089 aut Mondelli, Claudia verfasserin (orcid)0000-0002-5452-5238 aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 189, Seite 362-368 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:189 pages:362-368 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 189 362-368
allfields_unstemmed	10.1016/j.carbon.2021.12.062 doi (DE-627)ELV00730546X (ELSEVIER)S0008-6223(21)01221-5 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Sharma, Swati verfasserin (orcid)0000-0003-0566-0270 aut Quantification of Buckminsterfullerene (C 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural units in non-graphitizing carbons. It has been proposed that a certain fraction of completely closed spherical fullerenes, such as C60, is also present in these materials. Strongly curved structures are not expected to exist in graphitizing carbons. We report on a Small Angle Neutron Scattering (SANS) investigation conducted at the Institut Laue-Langevin, Grenoble, France, that enables us to (i) quantify C60 in a non-graphitizing carbon, (ii) investigate the evolution patterns of graphitizing and non-graphitizing carbons, and (iii) perform a detailed SANS analysis of pure crystalline C60 in dry powder form. We also revisit the formation patterns of slightly larger structures (3–5 nm) such as graphitic crystallites and voids in both classes of polymeric carbon. These results provide a strong evidence in support of the fullerene-like microstructural models of non-graphitizing carbon, adding that the curved structural units are not just “fullerene-like”, but also spherical fullerenes, C60 in particular. Non-graphitizing carbon Fullerene Small angle neutron scattering Glass-like carbon Pyrolysis Zorzi, Sandro verfasserin (orcid)0000-0001-5024-9478 aut Cristiglio, Viviana verfasserin (orcid)0000-0003-3608-9222 aut Schweins, Ralf verfasserin (orcid)0000-0001-8078-2089 aut Mondelli, Claudia verfasserin (orcid)0000-0002-5452-5238 aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 189, Seite 362-368 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:189 pages:362-368 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 189 362-368
allfieldsGer	10.1016/j.carbon.2021.12.062 doi (DE-627)ELV00730546X (ELSEVIER)S0008-6223(21)01221-5 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Sharma, Swati verfasserin (orcid)0000-0003-0566-0270 aut Quantification of Buckminsterfullerene (C 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural units in non-graphitizing carbons. It has been proposed that a certain fraction of completely closed spherical fullerenes, such as C60, is also present in these materials. Strongly curved structures are not expected to exist in graphitizing carbons. We report on a Small Angle Neutron Scattering (SANS) investigation conducted at the Institut Laue-Langevin, Grenoble, France, that enables us to (i) quantify C60 in a non-graphitizing carbon, (ii) investigate the evolution patterns of graphitizing and non-graphitizing carbons, and (iii) perform a detailed SANS analysis of pure crystalline C60 in dry powder form. We also revisit the formation patterns of slightly larger structures (3–5 nm) such as graphitic crystallites and voids in both classes of polymeric carbon. These results provide a strong evidence in support of the fullerene-like microstructural models of non-graphitizing carbon, adding that the curved structural units are not just “fullerene-like”, but also spherical fullerenes, C60 in particular. Non-graphitizing carbon Fullerene Small angle neutron scattering Glass-like carbon Pyrolysis Zorzi, Sandro verfasserin (orcid)0000-0001-5024-9478 aut Cristiglio, Viviana verfasserin (orcid)0000-0003-3608-9222 aut Schweins, Ralf verfasserin (orcid)0000-0001-8078-2089 aut Mondelli, Claudia verfasserin (orcid)0000-0002-5452-5238 aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 189, Seite 362-368 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:189 pages:362-368 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 189 362-368
allfieldsSound	10.1016/j.carbon.2021.12.062 doi (DE-627)ELV00730546X (ELSEVIER)S0008-6223(21)01221-5 DE-627 ger DE-627 rda eng 540 DE-600 51.79 bkl 35.48 bkl Sharma, Swati verfasserin (orcid)0000-0003-0566-0270 aut Quantification of Buckminsterfullerene (C 2021 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural units in non-graphitizing carbons. It has been proposed that a certain fraction of completely closed spherical fullerenes, such as C60, is also present in these materials. Strongly curved structures are not expected to exist in graphitizing carbons. We report on a Small Angle Neutron Scattering (SANS) investigation conducted at the Institut Laue-Langevin, Grenoble, France, that enables us to (i) quantify C60 in a non-graphitizing carbon, (ii) investigate the evolution patterns of graphitizing and non-graphitizing carbons, and (iii) perform a detailed SANS analysis of pure crystalline C60 in dry powder form. We also revisit the formation patterns of slightly larger structures (3–5 nm) such as graphitic crystallites and voids in both classes of polymeric carbon. These results provide a strong evidence in support of the fullerene-like microstructural models of non-graphitizing carbon, adding that the curved structural units are not just “fullerene-like”, but also spherical fullerenes, C60 in particular. Non-graphitizing carbon Fullerene Small angle neutron scattering Glass-like carbon Pyrolysis Zorzi, Sandro verfasserin (orcid)0000-0001-5024-9478 aut Cristiglio, Viviana verfasserin (orcid)0000-0003-3608-9222 aut Schweins, Ralf verfasserin (orcid)0000-0001-8078-2089 aut Mondelli, Claudia verfasserin (orcid)0000-0002-5452-5238 aut Enthalten in Carbon Amsterdam [u.a.] : Elsevier Science, 1963 189, Seite 362-368 Online-Ressource (DE-627)320522164 (DE-600)2014715-6 (DE-576)103484280 0008-6223 nnns volume:189 pages:362-368 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.79 Sonstige Werkstoffe 35.48 Sonstige anorganische Elemente und ihre Verbindungen AR 189 362-368
language	English
source	Enthalten in Carbon 189, Seite 362-368 volume:189 pages:362-368
sourceStr	Enthalten in Carbon 189, Seite 362-368 volume:189 pages:362-368
format_phy_str_mv	Article
bklname	Sonstige Werkstoffe Sonstige anorganische Elemente und ihre Verbindungen
institution	findex.gbv.de
topic_facet	Non-graphitizing carbon Fullerene Small angle neutron scattering Glass-like carbon Pyrolysis
dewey-raw	540
isfreeaccess_bool	false
container_title	Carbon
authorswithroles_txt_mv	Sharma, Swati @@aut@@ Zorzi, Sandro @@aut@@ Cristiglio, Viviana @@aut@@ Schweins, Ralf @@aut@@ Mondelli, Claudia @@aut@@
publishDateDaySort_date	2021-01-01T00:00:00Z
hierarchy_top_id	320522164
dewey-sort	3540
id	ELV00730546X
language_de	englisch
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author	Sharma, Swati
spellingShingle	Sharma, Swati ddc 540 bkl 51.79 bkl 35.48 misc Non-graphitizing carbon misc Fullerene misc Small angle neutron scattering misc Glass-like carbon misc Pyrolysis Quantification of Buckminsterfullerene (C
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topic_title	540 DE-600 51.79 bkl 35.48 bkl Quantification of Buckminsterfullerene (C Non-graphitizing carbon Fullerene Small angle neutron scattering Glass-like carbon Pyrolysis
topic	ddc 540 bkl 51.79 bkl 35.48 misc Non-graphitizing carbon misc Fullerene misc Small angle neutron scattering misc Glass-like carbon misc Pyrolysis
topic_unstemmed	ddc 540 bkl 51.79 bkl 35.48 misc Non-graphitizing carbon misc Fullerene misc Small angle neutron scattering misc Glass-like carbon misc Pyrolysis
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title	Quantification of Buckminsterfullerene (C
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title_full	Quantification of Buckminsterfullerene (C
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title_sort	quantification of buckminsterfullerene (c
title_auth	Quantification of Buckminsterfullerene (C
abstract	In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural units in non-graphitizing carbons. It has been proposed that a certain fraction of completely closed spherical fullerenes, such as C60, is also present in these materials. Strongly curved structures are not expected to exist in graphitizing carbons. We report on a Small Angle Neutron Scattering (SANS) investigation conducted at the Institut Laue-Langevin, Grenoble, France, that enables us to (i) quantify C60 in a non-graphitizing carbon, (ii) investigate the evolution patterns of graphitizing and non-graphitizing carbons, and (iii) perform a detailed SANS analysis of pure crystalline C60 in dry powder form. We also revisit the formation patterns of slightly larger structures (3–5 nm) such as graphitic crystallites and voids in both classes of polymeric carbon. These results provide a strong evidence in support of the fullerene-like microstructural models of non-graphitizing carbon, adding that the curved structural units are not just “fullerene-like”, but also spherical fullerenes, C60 in particular.
abstractGer	In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural units in non-graphitizing carbons. It has been proposed that a certain fraction of completely closed spherical fullerenes, such as C60, is also present in these materials. Strongly curved structures are not expected to exist in graphitizing carbons. We report on a Small Angle Neutron Scattering (SANS) investigation conducted at the Institut Laue-Langevin, Grenoble, France, that enables us to (i) quantify C60 in a non-graphitizing carbon, (ii) investigate the evolution patterns of graphitizing and non-graphitizing carbons, and (iii) perform a detailed SANS analysis of pure crystalline C60 in dry powder form. We also revisit the formation patterns of slightly larger structures (3–5 nm) such as graphitic crystallites and voids in both classes of polymeric carbon. These results provide a strong evidence in support of the fullerene-like microstructural models of non-graphitizing carbon, adding that the curved structural units are not just “fullerene-like”, but also spherical fullerenes, C60 in particular.
abstract_unstemmed	In this article we present the first experimental evidence confirming a global presence of Buckminsterfullerene (C60) in non-graphitizing polymeric carbon, along with its volume fraction calculations. Partially stacked carbon fragments featuring weak or strong curvatures constitute the structural units in non-graphitizing carbons. It has been proposed that a certain fraction of completely closed spherical fullerenes, such as C60, is also present in these materials. Strongly curved structures are not expected to exist in graphitizing carbons. We report on a Small Angle Neutron Scattering (SANS) investigation conducted at the Institut Laue-Langevin, Grenoble, France, that enables us to (i) quantify C60 in a non-graphitizing carbon, (ii) investigate the evolution patterns of graphitizing and non-graphitizing carbons, and (iii) perform a detailed SANS analysis of pure crystalline C60 in dry powder form. We also revisit the formation patterns of slightly larger structures (3–5 nm) such as graphitic crystallites and voids in both classes of polymeric carbon. These results provide a strong evidence in support of the fullerene-like microstructural models of non-graphitizing carbon, adding that the curved structural units are not just “fullerene-like”, but also spherical fullerenes, C60 in particular.
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title_short	Quantification of Buckminsterfullerene (C
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up_date	2024-07-07T00:18:07.149Z
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Quantification of Buckminsterfullerene (C

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