Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis
Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Morán, M. [verfasserIn] Álvarez, M. Vicente [verfasserIn] Vizcaíno, P. [verfasserIn] Brown, D.W. [verfasserIn] Santisteban, J. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Schlagwörter: |
Time of flight neutron diffraction analysis |
|---|
| Übergeordnetes Werk: |
Enthalten in: Journal of alloys and compounds - Lausanne : Elsevier, 1991, 929 |
|---|---|
| Übergeordnetes Werk: |
volume:929 |
| DOI / URN: |
10.1016/j.jallcom.2022.167196 |
|---|
| Katalog-ID: |
ELV008591601 |
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| 245 | 1 | 0 | |a Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis |
| 264 | 1 | |c 2022 | |
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| 520 | |a Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-ND). On samples in the extruded, cold-rolled and post-annealed conditions, the HE-XRD experiment in transmission geometry allows a detailed characterization of the dependence of the line shape on the direction of the scattering vector. Important variations of the FWHM (Full Width at Half Maximum) were observed, which was interpreted as the non-uniform distribution of dislocations among grains with different orientations. Average values of the dislocation density and subgrain size were obtained after applying the Warren-Averbach method. | ||
| 650 | 4 | |a Time of flight neutron diffraction analysis | |
| 650 | 4 | |a High energy X ray diffraction analysis | |
| 650 | 4 | |a Zr-2.5%Nb | |
| 650 | 4 | |a Dislocation density | |
| 700 | 1 | |a Álvarez, M. Vicente |e verfasserin |4 aut | |
| 700 | 1 | |a Vizcaíno, P. |e verfasserin |4 aut | |
| 700 | 1 | |a Brown, D.W. |e verfasserin |4 aut | |
| 700 | 1 | |a Santisteban, J. |e verfasserin |4 aut | |
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10.1016/j.jallcom.2022.167196 doi (DE-627)ELV008591601 (ELSEVIER)S0925-8388(22)03587-3 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Morán, M. verfasserin aut Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-ND). On samples in the extruded, cold-rolled and post-annealed conditions, the HE-XRD experiment in transmission geometry allows a detailed characterization of the dependence of the line shape on the direction of the scattering vector. Important variations of the FWHM (Full Width at Half Maximum) were observed, which was interpreted as the non-uniform distribution of dislocations among grains with different orientations. Average values of the dislocation density and subgrain size were obtained after applying the Warren-Averbach method. Time of flight neutron diffraction analysis High energy X ray diffraction analysis Zr-2.5%Nb Dislocation density Álvarez, M. Vicente verfasserin aut Vizcaíno, P. verfasserin aut Brown, D.W. verfasserin aut Santisteban, J. verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 929 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:929 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 929 |
| spelling |
10.1016/j.jallcom.2022.167196 doi (DE-627)ELV008591601 (ELSEVIER)S0925-8388(22)03587-3 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Morán, M. verfasserin aut Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-ND). On samples in the extruded, cold-rolled and post-annealed conditions, the HE-XRD experiment in transmission geometry allows a detailed characterization of the dependence of the line shape on the direction of the scattering vector. Important variations of the FWHM (Full Width at Half Maximum) were observed, which was interpreted as the non-uniform distribution of dislocations among grains with different orientations. Average values of the dislocation density and subgrain size were obtained after applying the Warren-Averbach method. Time of flight neutron diffraction analysis High energy X ray diffraction analysis Zr-2.5%Nb Dislocation density Álvarez, M. Vicente verfasserin aut Vizcaíno, P. verfasserin aut Brown, D.W. verfasserin aut Santisteban, J. verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 929 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:929 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 929 |
| allfields_unstemmed |
10.1016/j.jallcom.2022.167196 doi (DE-627)ELV008591601 (ELSEVIER)S0925-8388(22)03587-3 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Morán, M. verfasserin aut Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-ND). On samples in the extruded, cold-rolled and post-annealed conditions, the HE-XRD experiment in transmission geometry allows a detailed characterization of the dependence of the line shape on the direction of the scattering vector. Important variations of the FWHM (Full Width at Half Maximum) were observed, which was interpreted as the non-uniform distribution of dislocations among grains with different orientations. Average values of the dislocation density and subgrain size were obtained after applying the Warren-Averbach method. Time of flight neutron diffraction analysis High energy X ray diffraction analysis Zr-2.5%Nb Dislocation density Álvarez, M. Vicente verfasserin aut Vizcaíno, P. verfasserin aut Brown, D.W. verfasserin aut Santisteban, J. verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 929 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:929 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 929 |
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10.1016/j.jallcom.2022.167196 doi (DE-627)ELV008591601 (ELSEVIER)S0925-8388(22)03587-3 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Morán, M. verfasserin aut Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-ND). On samples in the extruded, cold-rolled and post-annealed conditions, the HE-XRD experiment in transmission geometry allows a detailed characterization of the dependence of the line shape on the direction of the scattering vector. Important variations of the FWHM (Full Width at Half Maximum) were observed, which was interpreted as the non-uniform distribution of dislocations among grains with different orientations. Average values of the dislocation density and subgrain size were obtained after applying the Warren-Averbach method. Time of flight neutron diffraction analysis High energy X ray diffraction analysis Zr-2.5%Nb Dislocation density Álvarez, M. Vicente verfasserin aut Vizcaíno, P. verfasserin aut Brown, D.W. verfasserin aut Santisteban, J. verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 929 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:929 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 929 |
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10.1016/j.jallcom.2022.167196 doi (DE-627)ELV008591601 (ELSEVIER)S0925-8388(22)03587-3 DE-627 ger DE-627 rda eng 670 540 DE-600 51.54 bkl 33.61 bkl 35.90 bkl Morán, M. verfasserin aut Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-ND). On samples in the extruded, cold-rolled and post-annealed conditions, the HE-XRD experiment in transmission geometry allows a detailed characterization of the dependence of the line shape on the direction of the scattering vector. Important variations of the FWHM (Full Width at Half Maximum) were observed, which was interpreted as the non-uniform distribution of dislocations among grains with different orientations. Average values of the dislocation density and subgrain size were obtained after applying the Warren-Averbach method. Time of flight neutron diffraction analysis High energy X ray diffraction analysis Zr-2.5%Nb Dislocation density Álvarez, M. Vicente verfasserin aut Vizcaíno, P. verfasserin aut Brown, D.W. verfasserin aut Santisteban, J. verfasserin aut Enthalten in Journal of alloys and compounds Lausanne : Elsevier, 1991 929 Online-Ressource (DE-627)320504646 (DE-600)2012675-X (DE-576)098615009 nnns volume:929 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 51.54 Nichteisenmetalle und ihre Legierungen 33.61 Festkörperphysik 35.90 Festkörperchemie AR 929 |
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Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis |
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Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis |
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Morán, M. |
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Journal of alloys and compounds |
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Morán, M. Álvarez, M. Vicente Vizcaíno, P. Brown, D.W. Santisteban, J. |
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10.1016/j.jallcom.2022.167196 |
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dislocation density evolution in cold-rolled zr-2.5%nb pressure tubes under thermal treatments by high energy xrd and neutron tof diffraction peak profile analysis |
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Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis |
| abstract |
Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-ND). On samples in the extruded, cold-rolled and post-annealed conditions, the HE-XRD experiment in transmission geometry allows a detailed characterization of the dependence of the line shape on the direction of the scattering vector. Important variations of the FWHM (Full Width at Half Maximum) were observed, which was interpreted as the non-uniform distribution of dislocations among grains with different orientations. Average values of the dislocation density and subgrain size were obtained after applying the Warren-Averbach method. |
| abstractGer |
Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-ND). On samples in the extruded, cold-rolled and post-annealed conditions, the HE-XRD experiment in transmission geometry allows a detailed characterization of the dependence of the line shape on the direction of the scattering vector. Important variations of the FWHM (Full Width at Half Maximum) were observed, which was interpreted as the non-uniform distribution of dislocations among grains with different orientations. Average values of the dislocation density and subgrain size were obtained after applying the Warren-Averbach method. |
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Diffraction line profile analysis was done to characterize the change in the dislocation density at different stages of the processing route of a Zr-2.5%Nb pressure tube. Two diffraction experiments were carried out: High Energy X-Ray Diffraction (HE-XRD) and Neutron Time of Flight Diffraction (TOF-ND). On samples in the extruded, cold-rolled and post-annealed conditions, the HE-XRD experiment in transmission geometry allows a detailed characterization of the dependence of the line shape on the direction of the scattering vector. Important variations of the FWHM (Full Width at Half Maximum) were observed, which was interpreted as the non-uniform distribution of dislocations among grains with different orientations. Average values of the dislocation density and subgrain size were obtained after applying the Warren-Averbach method. |
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Dislocation density evolution in cold-rolled Zr-2.5%Nb pressure tubes under thermal treatments by high energy XRD and neutron TOF diffraction peak profile analysis |
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