Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand

Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framewo...
Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Gu, Yanan [verfasserIn] Li, Senlin [verfasserIn] Sun, Qiaozhen [verfasserIn] Zhang, Bingguang [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2022

Schlagwörter:	Zn(II) coordination polymer Dimethylthiocarbamate ligand Layered–pillared structure Luminescent property

Übergeordnetes Werk:	Enthalten in: Journal of molecular structure - New York, NY [u.a.] : Elsevier, 1967, 1274
Übergeordnetes Werk:	volume:1274

DOI / URN:	10.1016/j.molstruc.2022.134598

Katalog-ID:	ELV008908044

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245	1	0	\|a Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand
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520			\|a Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framework, namely [ZnL(4,4′–bpy)]n (1) (4,4′–bpy = 4,4′–bipyridine). Single crystal X–ray diffraction analysis of 1 reveals that the metal ions are bridged by L2– ligands to generate a two–dimensional layer, and the layers are further pillared by 4,4′–bpy to form a three–dimensional framework with a pcu topology. Furthermore, the solid state photoluminescent studies reveal that both H2L and polymer 1 display emission bands at 400 nm upon excitation at 325 nm. The average emission life time is 4.27 µs.
650		4	\|a Zn(II) coordination polymer
650		4	\|a Dimethylthiocarbamate ligand
650		4	\|a Layered–pillared structure
650		4	\|a Luminescent property
700	1		\|a Li, Senlin \|e verfasserin \|0 (orcid)0000-0001-9307-8971 \|4 aut
700	1		\|a Sun, Qiaozhen \|e verfasserin \|0 (orcid)0000-0001-6466-6336 \|4 aut
700	1		\|a Zhang, Bingguang \|e verfasserin \|4 aut
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Indexfelder

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matchkey_str	article:00222860:2022----::otoldyteisrcuenlmnsetrpryf3lyrdilrdicioriaino
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publishDate	2022
allfields	10.1016/j.molstruc.2022.134598 doi (DE-627)ELV008908044 (ELSEVIER)S0022-2860(22)02243-8 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Gu, Yanan verfasserin aut Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framework, namely [ZnL(4,4′–bpy)]n (1) (4,4′–bpy = 4,4′–bipyridine). Single crystal X–ray diffraction analysis of 1 reveals that the metal ions are bridged by L2– ligands to generate a two–dimensional layer, and the layers are further pillared by 4,4′–bpy to form a three–dimensional framework with a pcu topology. Furthermore, the solid state photoluminescent studies reveal that both H2L and polymer 1 display emission bands at 400 nm upon excitation at 325 nm. The average emission life time is 4.27 µs. Zn(II) coordination polymer Dimethylthiocarbamate ligand Layered–pillared structure Luminescent property Li, Senlin verfasserin (orcid)0000-0001-9307-8971 aut Sun, Qiaozhen verfasserin (orcid)0000-0001-6466-6336 aut Zhang, Bingguang verfasserin aut Enthalten in Journal of molecular structure New York, NY [u.a.] : Elsevier, 1967 1274 Online-Ressource (DE-627)302469745 (DE-600)1491504-2 (DE-576)255266626 0022-2860 nnns volume:1274 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 1274
spelling	10.1016/j.molstruc.2022.134598 doi (DE-627)ELV008908044 (ELSEVIER)S0022-2860(22)02243-8 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Gu, Yanan verfasserin aut Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framework, namely [ZnL(4,4′–bpy)]n (1) (4,4′–bpy = 4,4′–bipyridine). Single crystal X–ray diffraction analysis of 1 reveals that the metal ions are bridged by L2– ligands to generate a two–dimensional layer, and the layers are further pillared by 4,4′–bpy to form a three–dimensional framework with a pcu topology. Furthermore, the solid state photoluminescent studies reveal that both H2L and polymer 1 display emission bands at 400 nm upon excitation at 325 nm. The average emission life time is 4.27 µs. Zn(II) coordination polymer Dimethylthiocarbamate ligand Layered–pillared structure Luminescent property Li, Senlin verfasserin (orcid)0000-0001-9307-8971 aut Sun, Qiaozhen verfasserin (orcid)0000-0001-6466-6336 aut Zhang, Bingguang verfasserin aut Enthalten in Journal of molecular structure New York, NY [u.a.] : Elsevier, 1967 1274 Online-Ressource (DE-627)302469745 (DE-600)1491504-2 (DE-576)255266626 0022-2860 nnns volume:1274 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 1274
allfields_unstemmed	10.1016/j.molstruc.2022.134598 doi (DE-627)ELV008908044 (ELSEVIER)S0022-2860(22)02243-8 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Gu, Yanan verfasserin aut Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framework, namely [ZnL(4,4′–bpy)]n (1) (4,4′–bpy = 4,4′–bipyridine). Single crystal X–ray diffraction analysis of 1 reveals that the metal ions are bridged by L2– ligands to generate a two–dimensional layer, and the layers are further pillared by 4,4′–bpy to form a three–dimensional framework with a pcu topology. Furthermore, the solid state photoluminescent studies reveal that both H2L and polymer 1 display emission bands at 400 nm upon excitation at 325 nm. The average emission life time is 4.27 µs. Zn(II) coordination polymer Dimethylthiocarbamate ligand Layered–pillared structure Luminescent property Li, Senlin verfasserin (orcid)0000-0001-9307-8971 aut Sun, Qiaozhen verfasserin (orcid)0000-0001-6466-6336 aut Zhang, Bingguang verfasserin aut Enthalten in Journal of molecular structure New York, NY [u.a.] : Elsevier, 1967 1274 Online-Ressource (DE-627)302469745 (DE-600)1491504-2 (DE-576)255266626 0022-2860 nnns volume:1274 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 1274
allfieldsGer	10.1016/j.molstruc.2022.134598 doi (DE-627)ELV008908044 (ELSEVIER)S0022-2860(22)02243-8 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Gu, Yanan verfasserin aut Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framework, namely [ZnL(4,4′–bpy)]n (1) (4,4′–bpy = 4,4′–bipyridine). Single crystal X–ray diffraction analysis of 1 reveals that the metal ions are bridged by L2– ligands to generate a two–dimensional layer, and the layers are further pillared by 4,4′–bpy to form a three–dimensional framework with a pcu topology. Furthermore, the solid state photoluminescent studies reveal that both H2L and polymer 1 display emission bands at 400 nm upon excitation at 325 nm. The average emission life time is 4.27 µs. Zn(II) coordination polymer Dimethylthiocarbamate ligand Layered–pillared structure Luminescent property Li, Senlin verfasserin (orcid)0000-0001-9307-8971 aut Sun, Qiaozhen verfasserin (orcid)0000-0001-6466-6336 aut Zhang, Bingguang verfasserin aut Enthalten in Journal of molecular structure New York, NY [u.a.] : Elsevier, 1967 1274 Online-Ressource (DE-627)302469745 (DE-600)1491504-2 (DE-576)255266626 0022-2860 nnns volume:1274 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 1274
allfieldsSound	10.1016/j.molstruc.2022.134598 doi (DE-627)ELV008908044 (ELSEVIER)S0022-2860(22)02243-8 DE-627 ger DE-627 rda eng 540 DE-600 35.00 bkl Gu, Yanan verfasserin aut Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framework, namely [ZnL(4,4′–bpy)]n (1) (4,4′–bpy = 4,4′–bipyridine). Single crystal X–ray diffraction analysis of 1 reveals that the metal ions are bridged by L2– ligands to generate a two–dimensional layer, and the layers are further pillared by 4,4′–bpy to form a three–dimensional framework with a pcu topology. Furthermore, the solid state photoluminescent studies reveal that both H2L and polymer 1 display emission bands at 400 nm upon excitation at 325 nm. The average emission life time is 4.27 µs. Zn(II) coordination polymer Dimethylthiocarbamate ligand Layered–pillared structure Luminescent property Li, Senlin verfasserin (orcid)0000-0001-9307-8971 aut Sun, Qiaozhen verfasserin (orcid)0000-0001-6466-6336 aut Zhang, Bingguang verfasserin aut Enthalten in Journal of molecular structure New York, NY [u.a.] : Elsevier, 1967 1274 Online-Ressource (DE-627)302469745 (DE-600)1491504-2 (DE-576)255266626 0022-2860 nnns volume:1274 GBV_USEFLAG_U SYSFLAG_U GBV_ELV SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2336 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 35.00 Chemie: Allgemeines AR 1274
language	English
source	Enthalten in Journal of molecular structure 1274 volume:1274
sourceStr	Enthalten in Journal of molecular structure 1274 volume:1274
format_phy_str_mv	Article
bklname	Chemie: Allgemeines
institution	findex.gbv.de
topic_facet	Zn(II) coordination polymer Dimethylthiocarbamate ligand Layered–pillared structure Luminescent property
dewey-raw	540
isfreeaccess_bool	false
container_title	Journal of molecular structure
authorswithroles_txt_mv	Gu, Yanan @@aut@@ Li, Senlin @@aut@@ Sun, Qiaozhen @@aut@@ Zhang, Bingguang @@aut@@
publishDateDaySort_date	2022-01-01T00:00:00Z
hierarchy_top_id	302469745
dewey-sort	3540
id	ELV008908044
language_de	englisch
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author	Gu, Yanan
spellingShingle	Gu, Yanan ddc 540 bkl 35.00 misc Zn(II) coordination polymer misc Dimethylthiocarbamate ligand misc Layered–pillared structure misc Luminescent property Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand
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topic_title	540 DE-600 35.00 bkl Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand Zn(II) coordination polymer Dimethylthiocarbamate ligand Layered–pillared structure Luminescent property
topic	ddc 540 bkl 35.00 misc Zn(II) coordination polymer misc Dimethylthiocarbamate ligand misc Layered–pillared structure misc Luminescent property
topic_unstemmed	ddc 540 bkl 35.00 misc Zn(II) coordination polymer misc Dimethylthiocarbamate ligand misc Layered–pillared structure misc Luminescent property
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title	Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand
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title_full	Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand
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author_browse	Gu, Yanan Li, Senlin Sun, Qiaozhen Zhang, Bingguang
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title_sort	controlled synthesis, structure and luminescent property of a 3d layered–pillared zinc(ii) coordination polymer based on a newly designed ligand
title_auth	Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand
abstract	Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framework, namely [ZnL(4,4′–bpy)]n (1) (4,4′–bpy = 4,4′–bipyridine). Single crystal X–ray diffraction analysis of 1 reveals that the metal ions are bridged by L2– ligands to generate a two–dimensional layer, and the layers are further pillared by 4,4′–bpy to form a three–dimensional framework with a pcu topology. Furthermore, the solid state photoluminescent studies reveal that both H2L and polymer 1 display emission bands at 400 nm upon excitation at 325 nm. The average emission life time is 4.27 µs.
abstractGer	Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framework, namely [ZnL(4,4′–bpy)]n (1) (4,4′–bpy = 4,4′–bipyridine). Single crystal X–ray diffraction analysis of 1 reveals that the metal ions are bridged by L2– ligands to generate a two–dimensional layer, and the layers are further pillared by 4,4′–bpy to form a three–dimensional framework with a pcu topology. Furthermore, the solid state photoluminescent studies reveal that both H2L and polymer 1 display emission bands at 400 nm upon excitation at 325 nm. The average emission life time is 4.27 µs.
abstract_unstemmed	Continuing our previous strategy for construction of layered–pillared coordination polymer, in this paper, a new O–thiocarbamate–containing ligand H2L (5–[(dimethylamino)thioxomethoxy]–1,3–benzenedicarboxylic acid) has been designed and synthesized to construct a zinc(II)–based metal organic framework, namely [ZnL(4,4′–bpy)]n (1) (4,4′–bpy = 4,4′–bipyridine). Single crystal X–ray diffraction analysis of 1 reveals that the metal ions are bridged by L2– ligands to generate a two–dimensional layer, and the layers are further pillared by 4,4′–bpy to form a three–dimensional framework with a pcu topology. Furthermore, the solid state photoluminescent studies reveal that both H2L and polymer 1 display emission bands at 400 nm upon excitation at 325 nm. The average emission life time is 4.27 µs.
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title_short	Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand
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doi_str	10.1016/j.molstruc.2022.134598
up_date	2024-07-06T21:19:16.631Z
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Controlled synthesis, structure and luminescent property of a 3D layered–pillared zinc(II) coordination polymer based on a newly designed ligand

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