Best practices for electrochemical characterization of supercapacitors
We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Pedro Aguiar dos Santos, João [verfasserIn] Cesar Rufino, Fernando [verfasserIn] Yutaka Ota, João I. [verfasserIn] Fernandes, Rodolfo C. [verfasserIn] Vicentini, Rafael [verfasserIn] Pagan, Cesar J.B. [verfasserIn] Morais Da Silva, Leonardo [verfasserIn] Zanin, Hudson [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022 |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Journal of Energy Chemistry - Amsterdam [u.a.] : Elsevier, 2013, 80, Seite 265-283 |
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| Übergeordnetes Werk: |
volume:80 ; pages:265-283 |
| DOI / URN: |
10.1016/j.jechem.2022.12.034 |
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ELV009977570 |
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| 520 | |a We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the electrochemical analytical apparatus used and its configuration. The lack of such information may lead researchers, especially inexperienced ones, to misunderstand the procedures and results. Eventually, the misled electrochemical equipment configuration favors misinterpretation of data and low reproducibility rates. This paper aims to highlight these issues and clarify them. We explain fundamental concepts of some electrochemical analytical methods, such as cyclic voltammetry, galvanostatic charge–discharge, single potential step chronoamperometry, and electrochemical impedance spectroscopy, focusing on the supercapacitor field. Distinct configurations of electrical parameters are presented and discussed to highlight the effects of incorrect setup and uncover misleading results. We discuss how the electrochemical setup and data analyses matter in reliable data results for the supercapacitor. | ||
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| 650 | 4 | |a Electrochemical instrumentation | |
| 650 | 4 | |a Electrochemical methods | |
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| 700 | 1 | |a Cesar Rufino, Fernando |e verfasserin |4 aut | |
| 700 | 1 | |a Yutaka Ota, João I. |e verfasserin |4 aut | |
| 700 | 1 | |a Fernandes, Rodolfo C. |e verfasserin |4 aut | |
| 700 | 1 | |a Vicentini, Rafael |e verfasserin |4 aut | |
| 700 | 1 | |a Pagan, Cesar J.B. |e verfasserin |4 aut | |
| 700 | 1 | |a Morais Da Silva, Leonardo |e verfasserin |4 aut | |
| 700 | 1 | |a Zanin, Hudson |e verfasserin |4 aut | |
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10.1016/j.jechem.2022.12.034 doi (DE-627)ELV009977570 (ELSEVIER)S2095-4956(22)00703-3 DE-627 ger DE-627 rda eng 540 VZ Pedro Aguiar dos Santos, João verfasserin aut Best practices for electrochemical characterization of supercapacitors 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the electrochemical analytical apparatus used and its configuration. The lack of such information may lead researchers, especially inexperienced ones, to misunderstand the procedures and results. Eventually, the misled electrochemical equipment configuration favors misinterpretation of data and low reproducibility rates. This paper aims to highlight these issues and clarify them. We explain fundamental concepts of some electrochemical analytical methods, such as cyclic voltammetry, galvanostatic charge–discharge, single potential step chronoamperometry, and electrochemical impedance spectroscopy, focusing on the supercapacitor field. Distinct configurations of electrical parameters are presented and discussed to highlight the effects of incorrect setup and uncover misleading results. We discuss how the electrochemical setup and data analyses matter in reliable data results for the supercapacitor. Supercapacitor Electrochemical instrumentation Electrochemical methods Electrochemistry Cesar Rufino, Fernando verfasserin aut Yutaka Ota, João I. verfasserin aut Fernandes, Rodolfo C. verfasserin aut Vicentini, Rafael verfasserin aut Pagan, Cesar J.B. verfasserin aut Morais Da Silva, Leonardo verfasserin aut Zanin, Hudson verfasserin aut Enthalten in Journal of Energy Chemistry Amsterdam [u.a.] : Elsevier, 2013 80, Seite 265-283 Online-Ressource (DE-627)745616399 (DE-600)2714311-9 (DE-576)382032861 2096-885X nnns volume:80 pages:265-283 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 AR 80 265-283 |
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10.1016/j.jechem.2022.12.034 doi (DE-627)ELV009977570 (ELSEVIER)S2095-4956(22)00703-3 DE-627 ger DE-627 rda eng 540 VZ Pedro Aguiar dos Santos, João verfasserin aut Best practices for electrochemical characterization of supercapacitors 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the electrochemical analytical apparatus used and its configuration. The lack of such information may lead researchers, especially inexperienced ones, to misunderstand the procedures and results. Eventually, the misled electrochemical equipment configuration favors misinterpretation of data and low reproducibility rates. This paper aims to highlight these issues and clarify them. We explain fundamental concepts of some electrochemical analytical methods, such as cyclic voltammetry, galvanostatic charge–discharge, single potential step chronoamperometry, and electrochemical impedance spectroscopy, focusing on the supercapacitor field. Distinct configurations of electrical parameters are presented and discussed to highlight the effects of incorrect setup and uncover misleading results. We discuss how the electrochemical setup and data analyses matter in reliable data results for the supercapacitor. Supercapacitor Electrochemical instrumentation Electrochemical methods Electrochemistry Cesar Rufino, Fernando verfasserin aut Yutaka Ota, João I. verfasserin aut Fernandes, Rodolfo C. verfasserin aut Vicentini, Rafael verfasserin aut Pagan, Cesar J.B. verfasserin aut Morais Da Silva, Leonardo verfasserin aut Zanin, Hudson verfasserin aut Enthalten in Journal of Energy Chemistry Amsterdam [u.a.] : Elsevier, 2013 80, Seite 265-283 Online-Ressource (DE-627)745616399 (DE-600)2714311-9 (DE-576)382032861 2096-885X nnns volume:80 pages:265-283 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 AR 80 265-283 |
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10.1016/j.jechem.2022.12.034 doi (DE-627)ELV009977570 (ELSEVIER)S2095-4956(22)00703-3 DE-627 ger DE-627 rda eng 540 VZ Pedro Aguiar dos Santos, João verfasserin aut Best practices for electrochemical characterization of supercapacitors 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the electrochemical analytical apparatus used and its configuration. The lack of such information may lead researchers, especially inexperienced ones, to misunderstand the procedures and results. Eventually, the misled electrochemical equipment configuration favors misinterpretation of data and low reproducibility rates. This paper aims to highlight these issues and clarify them. We explain fundamental concepts of some electrochemical analytical methods, such as cyclic voltammetry, galvanostatic charge–discharge, single potential step chronoamperometry, and electrochemical impedance spectroscopy, focusing on the supercapacitor field. Distinct configurations of electrical parameters are presented and discussed to highlight the effects of incorrect setup and uncover misleading results. We discuss how the electrochemical setup and data analyses matter in reliable data results for the supercapacitor. Supercapacitor Electrochemical instrumentation Electrochemical methods Electrochemistry Cesar Rufino, Fernando verfasserin aut Yutaka Ota, João I. verfasserin aut Fernandes, Rodolfo C. verfasserin aut Vicentini, Rafael verfasserin aut Pagan, Cesar J.B. verfasserin aut Morais Da Silva, Leonardo verfasserin aut Zanin, Hudson verfasserin aut Enthalten in Journal of Energy Chemistry Amsterdam [u.a.] : Elsevier, 2013 80, Seite 265-283 Online-Ressource (DE-627)745616399 (DE-600)2714311-9 (DE-576)382032861 2096-885X nnns volume:80 pages:265-283 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 AR 80 265-283 |
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10.1016/j.jechem.2022.12.034 doi (DE-627)ELV009977570 (ELSEVIER)S2095-4956(22)00703-3 DE-627 ger DE-627 rda eng 540 VZ Pedro Aguiar dos Santos, João verfasserin aut Best practices for electrochemical characterization of supercapacitors 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the electrochemical analytical apparatus used and its configuration. The lack of such information may lead researchers, especially inexperienced ones, to misunderstand the procedures and results. Eventually, the misled electrochemical equipment configuration favors misinterpretation of data and low reproducibility rates. This paper aims to highlight these issues and clarify them. We explain fundamental concepts of some electrochemical analytical methods, such as cyclic voltammetry, galvanostatic charge–discharge, single potential step chronoamperometry, and electrochemical impedance spectroscopy, focusing on the supercapacitor field. Distinct configurations of electrical parameters are presented and discussed to highlight the effects of incorrect setup and uncover misleading results. We discuss how the electrochemical setup and data analyses matter in reliable data results for the supercapacitor. Supercapacitor Electrochemical instrumentation Electrochemical methods Electrochemistry Cesar Rufino, Fernando verfasserin aut Yutaka Ota, João I. verfasserin aut Fernandes, Rodolfo C. verfasserin aut Vicentini, Rafael verfasserin aut Pagan, Cesar J.B. verfasserin aut Morais Da Silva, Leonardo verfasserin aut Zanin, Hudson verfasserin aut Enthalten in Journal of Energy Chemistry Amsterdam [u.a.] : Elsevier, 2013 80, Seite 265-283 Online-Ressource (DE-627)745616399 (DE-600)2714311-9 (DE-576)382032861 2096-885X nnns volume:80 pages:265-283 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 AR 80 265-283 |
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10.1016/j.jechem.2022.12.034 doi (DE-627)ELV009977570 (ELSEVIER)S2095-4956(22)00703-3 DE-627 ger DE-627 rda eng 540 VZ Pedro Aguiar dos Santos, João verfasserin aut Best practices for electrochemical characterization of supercapacitors 2022 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the electrochemical analytical apparatus used and its configuration. The lack of such information may lead researchers, especially inexperienced ones, to misunderstand the procedures and results. Eventually, the misled electrochemical equipment configuration favors misinterpretation of data and low reproducibility rates. This paper aims to highlight these issues and clarify them. We explain fundamental concepts of some electrochemical analytical methods, such as cyclic voltammetry, galvanostatic charge–discharge, single potential step chronoamperometry, and electrochemical impedance spectroscopy, focusing on the supercapacitor field. Distinct configurations of electrical parameters are presented and discussed to highlight the effects of incorrect setup and uncover misleading results. We discuss how the electrochemical setup and data analyses matter in reliable data results for the supercapacitor. Supercapacitor Electrochemical instrumentation Electrochemical methods Electrochemistry Cesar Rufino, Fernando verfasserin aut Yutaka Ota, João I. verfasserin aut Fernandes, Rodolfo C. verfasserin aut Vicentini, Rafael verfasserin aut Pagan, Cesar J.B. verfasserin aut Morais Da Silva, Leonardo verfasserin aut Zanin, Hudson verfasserin aut Enthalten in Journal of Energy Chemistry Amsterdam [u.a.] : Elsevier, 2013 80, Seite 265-283 Online-Ressource (DE-627)745616399 (DE-600)2714311-9 (DE-576)382032861 2096-885X nnns volume:80 pages:265-283 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_63 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_224 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2006 GBV_ILN_2008 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2038 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2065 GBV_ILN_2068 GBV_ILN_2088 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2113 GBV_ILN_2118 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2147 GBV_ILN_2148 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_2522 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4046 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4126 GBV_ILN_4242 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4335 GBV_ILN_4338 GBV_ILN_4393 AR 80 265-283 |
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Best practices for electrochemical characterization of supercapacitors |
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Pedro Aguiar dos Santos, João |
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Pedro Aguiar dos Santos, João Cesar Rufino, Fernando Yutaka Ota, João I. Fernandes, Rodolfo C. Vicentini, Rafael Pagan, Cesar J.B. Morais Da Silva, Leonardo Zanin, Hudson |
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best practices for electrochemical characterization of supercapacitors |
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Best practices for electrochemical characterization of supercapacitors |
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We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the electrochemical analytical apparatus used and its configuration. The lack of such information may lead researchers, especially inexperienced ones, to misunderstand the procedures and results. Eventually, the misled electrochemical equipment configuration favors misinterpretation of data and low reproducibility rates. This paper aims to highlight these issues and clarify them. We explain fundamental concepts of some electrochemical analytical methods, such as cyclic voltammetry, galvanostatic charge–discharge, single potential step chronoamperometry, and electrochemical impedance spectroscopy, focusing on the supercapacitor field. Distinct configurations of electrical parameters are presented and discussed to highlight the effects of incorrect setup and uncover misleading results. We discuss how the electrochemical setup and data analyses matter in reliable data results for the supercapacitor. |
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We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the electrochemical analytical apparatus used and its configuration. The lack of such information may lead researchers, especially inexperienced ones, to misunderstand the procedures and results. Eventually, the misled electrochemical equipment configuration favors misinterpretation of data and low reproducibility rates. This paper aims to highlight these issues and clarify them. We explain fundamental concepts of some electrochemical analytical methods, such as cyclic voltammetry, galvanostatic charge–discharge, single potential step chronoamperometry, and electrochemical impedance spectroscopy, focusing on the supercapacitor field. Distinct configurations of electrical parameters are presented and discussed to highlight the effects of incorrect setup and uncover misleading results. We discuss how the electrochemical setup and data analyses matter in reliable data results for the supercapacitor. |
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We discuss here essential aspects of the experimental supercapacitors characterization by a series of well-known electrochemical methods. We are motivated by a considerable number of publications that misreport procedures and results. Authors often conceal or neglect essential information about the electrochemical analytical apparatus used and its configuration. The lack of such information may lead researchers, especially inexperienced ones, to misunderstand the procedures and results. Eventually, the misled electrochemical equipment configuration favors misinterpretation of data and low reproducibility rates. This paper aims to highlight these issues and clarify them. We explain fundamental concepts of some electrochemical analytical methods, such as cyclic voltammetry, galvanostatic charge–discharge, single potential step chronoamperometry, and electrochemical impedance spectroscopy, focusing on the supercapacitor field. Distinct configurations of electrical parameters are presented and discussed to highlight the effects of incorrect setup and uncover misleading results. We discuss how the electrochemical setup and data analyses matter in reliable data results for the supercapacitor. |
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Cesar Rufino, Fernando Yutaka Ota, João I. Fernandes, Rodolfo C. Vicentini, Rafael Pagan, Cesar J.B. Morais Da Silva, Leonardo Zanin, Hudson |
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