Synthesis of hexagonal boron nitride fibers within two hour annealing at 500°C and two hour growth duration at 1000°C
Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitri...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Ahmad, Pervaiz [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2016transfer abstract |
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| Schlagwörter: |
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| Umfang: |
6 |
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| Übergeordnetes Werk: |
Enthalten in: Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration - Rey, F. ELSEVIER, 2018, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:42 ; year:2016 ; number:13 ; pages:14661-14666 ; extent:6 |
| Links: |
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| DOI / URN: |
10.1016/j.ceramint.2016.06.089 |
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| 245 | 1 | 0 | |a Synthesis of hexagonal boron nitride fibers within two hour annealing at 500°C and two hour growth duration at 1000°C |
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| 520 | |a Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. | ||
| 520 | |a Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. | ||
| 650 | 7 | |a Annealing |2 Elsevier | |
| 650 | 7 | |a Synthesis |2 Elsevier | |
| 650 | 7 | |a BNFs |2 Elsevier | |
| 650 | 7 | |a Growth duration |2 Elsevier | |
| 650 | 7 | |a Etching |2 Elsevier | |
| 700 | 1 | |a Khandaker, Mayeen Uddin |4 oth | |
| 700 | 1 | |a Amin, Yusoff Mohd |4 oth | |
| 700 | 1 | |a Muhammad, Nawshad |4 oth | |
| 700 | 1 | |a Khan, Ghulamullah |4 oth | |
| 700 | 1 | |a Khan, Amir Sada |4 oth | |
| 700 | 1 | |a Numan, Arshid |4 oth | |
| 700 | 1 | |a Rehman, Muhammad Abdur |4 oth | |
| 700 | 1 | |a Ahmed, Syed Muzamil |4 oth | |
| 700 | 1 | |a Khan, Asif |4 oth | |
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10.1016/j.ceramint.2016.06.089 doi GBVA2016008000005.pica (DE-627)ELV013946811 (ELSEVIER)S0272-8842(16)30922-1 DE-627 ger DE-627 rakwb eng 670 670 DE-600 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Ahmad, Pervaiz verfasserin aut Synthesis of hexagonal boron nitride fibers within two hour annealing at 500°C and two hour growth duration at 1000°C 2016transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Annealing Elsevier Synthesis Elsevier BNFs Elsevier Growth duration Elsevier Etching Elsevier Khandaker, Mayeen Uddin oth Amin, Yusoff Mohd oth Muhammad, Nawshad oth Khan, Ghulamullah oth Khan, Amir Sada oth Numan, Arshid oth Rehman, Muhammad Abdur oth Ahmed, Syed Muzamil oth Khan, Asif oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:42 year:2016 number:13 pages:14661-14666 extent:6 https://doi.org/10.1016/j.ceramint.2016.06.089 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 42 2016 13 14661-14666 6 045F 670 |
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10.1016/j.ceramint.2016.06.089 doi GBVA2016008000005.pica (DE-627)ELV013946811 (ELSEVIER)S0272-8842(16)30922-1 DE-627 ger DE-627 rakwb eng 670 670 DE-600 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Ahmad, Pervaiz verfasserin aut Synthesis of hexagonal boron nitride fibers within two hour annealing at 500°C and two hour growth duration at 1000°C 2016transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Annealing Elsevier Synthesis Elsevier BNFs Elsevier Growth duration Elsevier Etching Elsevier Khandaker, Mayeen Uddin oth Amin, Yusoff Mohd oth Muhammad, Nawshad oth Khan, Ghulamullah oth Khan, Amir Sada oth Numan, Arshid oth Rehman, Muhammad Abdur oth Ahmed, Syed Muzamil oth Khan, Asif oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:42 year:2016 number:13 pages:14661-14666 extent:6 https://doi.org/10.1016/j.ceramint.2016.06.089 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 42 2016 13 14661-14666 6 045F 670 |
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10.1016/j.ceramint.2016.06.089 doi GBVA2016008000005.pica (DE-627)ELV013946811 (ELSEVIER)S0272-8842(16)30922-1 DE-627 ger DE-627 rakwb eng 670 670 DE-600 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Ahmad, Pervaiz verfasserin aut Synthesis of hexagonal boron nitride fibers within two hour annealing at 500°C and two hour growth duration at 1000°C 2016transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Annealing Elsevier Synthesis Elsevier BNFs Elsevier Growth duration Elsevier Etching Elsevier Khandaker, Mayeen Uddin oth Amin, Yusoff Mohd oth Muhammad, Nawshad oth Khan, Ghulamullah oth Khan, Amir Sada oth Numan, Arshid oth Rehman, Muhammad Abdur oth Ahmed, Syed Muzamil oth Khan, Asif oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:42 year:2016 number:13 pages:14661-14666 extent:6 https://doi.org/10.1016/j.ceramint.2016.06.089 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 42 2016 13 14661-14666 6 045F 670 |
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10.1016/j.ceramint.2016.06.089 doi GBVA2016008000005.pica (DE-627)ELV013946811 (ELSEVIER)S0272-8842(16)30922-1 DE-627 ger DE-627 rakwb eng 670 670 DE-600 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Ahmad, Pervaiz verfasserin aut Synthesis of hexagonal boron nitride fibers within two hour annealing at 500°C and two hour growth duration at 1000°C 2016transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Annealing Elsevier Synthesis Elsevier BNFs Elsevier Growth duration Elsevier Etching Elsevier Khandaker, Mayeen Uddin oth Amin, Yusoff Mohd oth Muhammad, Nawshad oth Khan, Ghulamullah oth Khan, Amir Sada oth Numan, Arshid oth Rehman, Muhammad Abdur oth Ahmed, Syed Muzamil oth Khan, Asif oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:42 year:2016 number:13 pages:14661-14666 extent:6 https://doi.org/10.1016/j.ceramint.2016.06.089 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 42 2016 13 14661-14666 6 045F 670 |
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10.1016/j.ceramint.2016.06.089 doi GBVA2016008000005.pica (DE-627)ELV013946811 (ELSEVIER)S0272-8842(16)30922-1 DE-627 ger DE-627 rakwb eng 670 670 DE-600 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Ahmad, Pervaiz verfasserin aut Synthesis of hexagonal boron nitride fibers within two hour annealing at 500°C and two hour growth duration at 1000°C 2016transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. Annealing Elsevier Synthesis Elsevier BNFs Elsevier Growth duration Elsevier Etching Elsevier Khandaker, Mayeen Uddin oth Amin, Yusoff Mohd oth Muhammad, Nawshad oth Khan, Ghulamullah oth Khan, Amir Sada oth Numan, Arshid oth Rehman, Muhammad Abdur oth Ahmed, Syed Muzamil oth Khan, Asif oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:42 year:2016 number:13 pages:14661-14666 extent:6 https://doi.org/10.1016/j.ceramint.2016.06.089 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 42 2016 13 14661-14666 6 045F 670 |
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Enthalten in Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration Amsterdam [u.a.] volume:42 year:2016 number:13 pages:14661-14666 extent:6 |
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synthesis of hexagonal boron nitride fibers within two hour annealing at 500°c and two hour growth duration at 1000°c |
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Synthesis of hexagonal boron nitride fibers within two hour annealing at 500°C and two hour growth duration at 1000°C |
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Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. |
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Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. |
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Several advantageous features like low density, large surface area, high porosity and tight pore size make the nanofiber suitable for a wide range of applications from medical to consumer products and industrial to high-tech applications. Present study concerns the synthesis of hexagonal boron nitride fibers (Ø=70–350nm) from a mixture of Boron, Magnesium oxide and Iron oxide powders via a simple CVD technique. A relatively long annealing and growth duration of two hours at 500°C and 1000°C, respectively were utilized in this synthesis. The synthesized samples seem to have the BNFs of irregular curved human hair-like morphologies in lower resolution and solid cylinder-like structures in high resolution transmission electron microscopy. The presence of Boron and Nitrogen in the synthesized BNF's sample were confirmed via the B 1s peak at 190.7eV and N 1s peak at 398.3eV in the XPS survey whereas a major peak at 1370 (cm−1) in the Raman spectrum corresponds to the vibration of E2g mode in h-BN. The sharp peaks in the XRD pattern verify the h-BN phase and highly crystalline nature of the synthesized BNFs. |
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