Impact of synthesized amino alcohol plasticizer on the morphology and hydrophilicity of polysulfone ultrafiltration membrane
In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weig...
Ausführliche Beschreibung
Autor*in: |
Sharma, N. [verfasserIn] |
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Englisch |
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2017transfer abstract |
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14 |
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Enthalten in: Steering charge kinetics in W - Yue, Xin-Zheng ELSEVIER, 2019, the official journal of the North American Membrane Society, New York, NY [u.a.] |
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Übergeordnetes Werk: |
volume:522 ; year:2017 ; day:15 ; month:01 ; pages:202-215 ; extent:14 |
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DOI / URN: |
10.1016/j.memsci.2016.08.068 |
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520 | |a In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. | ||
520 | |a In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. | ||
650 | 7 | |a Plasticizer |2 Elsevier | |
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650 | 7 | |a Polyethylene glycol |2 Elsevier | |
650 | 7 | |a Isatoic anhydride |2 Elsevier | |
650 | 7 | |a Polysulfone |2 Elsevier | |
700 | 1 | |a Purkait, M.K. |4 oth | |
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10.1016/j.memsci.2016.08.068 doi GBV00000000000184A.pica (DE-627)ELV015112411 (ELSEVIER)S0376-7388(16)31478-8 DE-627 ger DE-627 rakwb eng 570 570 DE-600 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Sharma, N. verfasserin aut Impact of synthesized amino alcohol plasticizer on the morphology and hydrophilicity of polysulfone ultrafiltration membrane 2017transfer abstract 14 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. Plasticizer Elsevier Hydrophilicity Elsevier Polyethylene glycol Elsevier Isatoic anhydride Elsevier Polysulfone Elsevier Purkait, M.K. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:522 year:2017 day:15 month:01 pages:202-215 extent:14 https://doi.org/10.1016/j.memsci.2016.08.068 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 522 2017 15 0115 202-215 14 045F 570 |
spelling |
10.1016/j.memsci.2016.08.068 doi GBV00000000000184A.pica (DE-627)ELV015112411 (ELSEVIER)S0376-7388(16)31478-8 DE-627 ger DE-627 rakwb eng 570 570 DE-600 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Sharma, N. verfasserin aut Impact of synthesized amino alcohol plasticizer on the morphology and hydrophilicity of polysulfone ultrafiltration membrane 2017transfer abstract 14 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. Plasticizer Elsevier Hydrophilicity Elsevier Polyethylene glycol Elsevier Isatoic anhydride Elsevier Polysulfone Elsevier Purkait, M.K. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:522 year:2017 day:15 month:01 pages:202-215 extent:14 https://doi.org/10.1016/j.memsci.2016.08.068 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 522 2017 15 0115 202-215 14 045F 570 |
allfields_unstemmed |
10.1016/j.memsci.2016.08.068 doi GBV00000000000184A.pica (DE-627)ELV015112411 (ELSEVIER)S0376-7388(16)31478-8 DE-627 ger DE-627 rakwb eng 570 570 DE-600 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Sharma, N. verfasserin aut Impact of synthesized amino alcohol plasticizer on the morphology and hydrophilicity of polysulfone ultrafiltration membrane 2017transfer abstract 14 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. Plasticizer Elsevier Hydrophilicity Elsevier Polyethylene glycol Elsevier Isatoic anhydride Elsevier Polysulfone Elsevier Purkait, M.K. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:522 year:2017 day:15 month:01 pages:202-215 extent:14 https://doi.org/10.1016/j.memsci.2016.08.068 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 522 2017 15 0115 202-215 14 045F 570 |
allfieldsGer |
10.1016/j.memsci.2016.08.068 doi GBV00000000000184A.pica (DE-627)ELV015112411 (ELSEVIER)S0376-7388(16)31478-8 DE-627 ger DE-627 rakwb eng 570 570 DE-600 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Sharma, N. verfasserin aut Impact of synthesized amino alcohol plasticizer on the morphology and hydrophilicity of polysulfone ultrafiltration membrane 2017transfer abstract 14 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. Plasticizer Elsevier Hydrophilicity Elsevier Polyethylene glycol Elsevier Isatoic anhydride Elsevier Polysulfone Elsevier Purkait, M.K. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:522 year:2017 day:15 month:01 pages:202-215 extent:14 https://doi.org/10.1016/j.memsci.2016.08.068 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 522 2017 15 0115 202-215 14 045F 570 |
allfieldsSound |
10.1016/j.memsci.2016.08.068 doi GBV00000000000184A.pica (DE-627)ELV015112411 (ELSEVIER)S0376-7388(16)31478-8 DE-627 ger DE-627 rakwb eng 570 570 DE-600 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Sharma, N. verfasserin aut Impact of synthesized amino alcohol plasticizer on the morphology and hydrophilicity of polysulfone ultrafiltration membrane 2017transfer abstract 14 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. Plasticizer Elsevier Hydrophilicity Elsevier Polyethylene glycol Elsevier Isatoic anhydride Elsevier Polysulfone Elsevier Purkait, M.K. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:522 year:2017 day:15 month:01 pages:202-215 extent:14 https://doi.org/10.1016/j.memsci.2016.08.068 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 522 2017 15 0115 202-215 14 045F 570 |
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impact of synthesized amino alcohol plasticizer on the morphology and hydrophilicity of polysulfone ultrafiltration membrane |
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Impact of synthesized amino alcohol plasticizer on the morphology and hydrophilicity of polysulfone ultrafiltration membrane |
abstract |
In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. |
abstractGer |
In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. |
abstract_unstemmed |
In this work, polysulfone (PSF) ultrafiltration membranes with increased hydrophilicity were prepared using the amino alcohol plasticizer (AAP). The AAP was synthesized by the reaction of polyethylene glycol (PEG) and isatoic anhydride (IAH). Different molecular weight of PEG and IAH (molecular weight 163Da) were used for preparing the AAP. Asymmetric membranes were fabricated by blending these plasticizers in membrane casting solution. Formation of AAP was confirmed by FTIR and 1HNMR spectra of AAP. Characterization of membranes was done in terms of hydraulic permeability, pure water flux (PWF) and hydrophilicity. PWF was found to be increased from 29.3L/m2 h to 110.1L/m2 h and water contact angle also reduced from 72° to 62° for plain and AAP containing PSF membrane, respectively. The morphological and structural analysis of the membranes was done by scanning electron microscope and field emission scanning electron microscope. Permeation and rejection behavior of fabricated membranes was studied by Bovine serum albumin (BSA) solution. Maximum BSA rejection was increased by 20.5% for the modified membrane. FESEM images affirm that the pore size of the membranes decreased by the addition of AAP. PEG with molecular weight of 400Da based AAP gave best performance among all the membranes for each parameter. |
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Impact of synthesized amino alcohol plasticizer on the morphology and hydrophilicity of polysulfone ultrafiltration membrane |
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