Synthesis of glycerol carbonate from glycerol and diethyl carbonate over Ce-NiO catalyst: The role of multiphase Ni
A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorp...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Wu, Yuanfeng [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2017transfer abstract |
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| Umfang: |
9 |
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| Übergeordnetes Werk: |
Enthalten in: Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners - Jacobs, Jacquelyn A. ELSEVIER, 2017, JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics, Lausanne |
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| Übergeordnetes Werk: |
volume:720 ; year:2017 ; day:5 ; month:10 ; pages:360-368 ; extent:9 |
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| DOI / URN: |
10.1016/j.jallcom.2017.05.292 |
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| 245 | 1 | 0 | |a Synthesis of glycerol carbonate from glycerol and diethyl carbonate over Ce-NiO catalyst: The role of multiphase Ni |
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| 520 | |a A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. | ||
| 520 | |a A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. | ||
| 650 | 7 | |a Glycerol carbonate |2 Elsevier | |
| 650 | 7 | |a Ce-NiO |2 Elsevier | |
| 650 | 7 | |a Diethyl carbonate |2 Elsevier | |
| 650 | 7 | |a Glycerol |2 Elsevier | |
| 650 | 7 | |a Transesterification |2 Elsevier | |
| 700 | 1 | |a Song, Xianghai |4 oth | |
| 700 | 1 | |a Cai, Fufeng |4 oth | |
| 700 | 1 | |a Xiao, Guomin |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier |a Jacobs, Jacquelyn A. ELSEVIER |t Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners |d 2017 |d JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics |g Lausanne |w (DE-627)ELV001115774 |
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10.1016/j.jallcom.2017.05.292 doi GBVA2017015000022.pica (DE-627)ELV015281914 (ELSEVIER)S0925-8388(17)31908-4 DE-627 ger DE-627 rakwb eng 670 540 670 DE-600 540 DE-600 630 VZ Wu, Yuanfeng verfasserin aut Synthesis of glycerol carbonate from glycerol and diethyl carbonate over Ce-NiO catalyst: The role of multiphase Ni 2017transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. Glycerol carbonate Elsevier Ce-NiO Elsevier Diethyl carbonate Elsevier Glycerol Elsevier Transesterification Elsevier Song, Xianghai oth Cai, Fufeng oth Xiao, Guomin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:720 year:2017 day:5 month:10 pages:360-368 extent:9 https://doi.org/10.1016/j.jallcom.2017.05.292 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 720 2017 5 1005 360-368 9 045F 670 |
| spelling |
10.1016/j.jallcom.2017.05.292 doi GBVA2017015000022.pica (DE-627)ELV015281914 (ELSEVIER)S0925-8388(17)31908-4 DE-627 ger DE-627 rakwb eng 670 540 670 DE-600 540 DE-600 630 VZ Wu, Yuanfeng verfasserin aut Synthesis of glycerol carbonate from glycerol and diethyl carbonate over Ce-NiO catalyst: The role of multiphase Ni 2017transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. Glycerol carbonate Elsevier Ce-NiO Elsevier Diethyl carbonate Elsevier Glycerol Elsevier Transesterification Elsevier Song, Xianghai oth Cai, Fufeng oth Xiao, Guomin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:720 year:2017 day:5 month:10 pages:360-368 extent:9 https://doi.org/10.1016/j.jallcom.2017.05.292 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 720 2017 5 1005 360-368 9 045F 670 |
| allfields_unstemmed |
10.1016/j.jallcom.2017.05.292 doi GBVA2017015000022.pica (DE-627)ELV015281914 (ELSEVIER)S0925-8388(17)31908-4 DE-627 ger DE-627 rakwb eng 670 540 670 DE-600 540 DE-600 630 VZ Wu, Yuanfeng verfasserin aut Synthesis of glycerol carbonate from glycerol and diethyl carbonate over Ce-NiO catalyst: The role of multiphase Ni 2017transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. Glycerol carbonate Elsevier Ce-NiO Elsevier Diethyl carbonate Elsevier Glycerol Elsevier Transesterification Elsevier Song, Xianghai oth Cai, Fufeng oth Xiao, Guomin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:720 year:2017 day:5 month:10 pages:360-368 extent:9 https://doi.org/10.1016/j.jallcom.2017.05.292 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 720 2017 5 1005 360-368 9 045F 670 |
| allfieldsGer |
10.1016/j.jallcom.2017.05.292 doi GBVA2017015000022.pica (DE-627)ELV015281914 (ELSEVIER)S0925-8388(17)31908-4 DE-627 ger DE-627 rakwb eng 670 540 670 DE-600 540 DE-600 630 VZ Wu, Yuanfeng verfasserin aut Synthesis of glycerol carbonate from glycerol and diethyl carbonate over Ce-NiO catalyst: The role of multiphase Ni 2017transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. Glycerol carbonate Elsevier Ce-NiO Elsevier Diethyl carbonate Elsevier Glycerol Elsevier Transesterification Elsevier Song, Xianghai oth Cai, Fufeng oth Xiao, Guomin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:720 year:2017 day:5 month:10 pages:360-368 extent:9 https://doi.org/10.1016/j.jallcom.2017.05.292 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 720 2017 5 1005 360-368 9 045F 670 |
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10.1016/j.jallcom.2017.05.292 doi GBVA2017015000022.pica (DE-627)ELV015281914 (ELSEVIER)S0925-8388(17)31908-4 DE-627 ger DE-627 rakwb eng 670 540 670 DE-600 540 DE-600 630 VZ Wu, Yuanfeng verfasserin aut Synthesis of glycerol carbonate from glycerol and diethyl carbonate over Ce-NiO catalyst: The role of multiphase Ni 2017transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. Glycerol carbonate Elsevier Ce-NiO Elsevier Diethyl carbonate Elsevier Glycerol Elsevier Transesterification Elsevier Song, Xianghai oth Cai, Fufeng oth Xiao, Guomin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:720 year:2017 day:5 month:10 pages:360-368 extent:9 https://doi.org/10.1016/j.jallcom.2017.05.292 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 720 2017 5 1005 360-368 9 045F 670 |
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Enthalten in Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners Lausanne volume:720 year:2017 day:5 month:10 pages:360-368 extent:9 |
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Synthesis of glycerol carbonate from glycerol and diethyl carbonate over Ce-NiO catalyst: The role of multiphase Ni |
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A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. |
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A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. |
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A series of Ce-NiO catalysts prepared by co-precipitation method were tested for glycerol transesterification with diethyl carbonate (DEC) to produce glycerol carbonate (GC). The microstructural and physicochemical properties of the catalysts were determined by XRD, XPS, SEM, EDX, CO2-TPD, N2-adsorption, FT-IR, and TG-DTG. The results showed that the particle size (100–350 nm) of the Ce-NiO was smaller than that of pure NiO (400–900 nm), suggesting addition of Ce in the catalyst synthesis could lessen the aggregation or facilitate the dispersion of NiO particles. The highest catalyst activity was observed over the Ce-NiO catalyst with Ce/Ni atomic ratio of 0.2 and calcined at 400 °C. 94.14% of glycerol conversion and 90.95% selectivity to GC were obtained over this catalyst under the optimum conditions (5 wt.% catalyst of glycerol, 85 °C, 8 h, glycerol/DEC ratio of 1:3). This catalyst can be reused up to three cycles with a slight decrease in its catalytic activity. It was found the well dispersed NiO particles and the strong basic sites derived from the substitution of Ce4+ by Ni2+ in the CeO2 lattices synergistically promoted the glycerol conversion. |
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