Dynamic microwave assisted extraction coupled with dispersive micro-solid-phase extraction of herbicides in soybeans
Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of se...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Li, Na [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
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2015transfer abstract |
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8 |
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| Übergeordnetes Werk: |
Enthalten in: Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications - Mohamed, S.H. ELSEVIER, 2019, the international journal of pure and applied analytical chemistry, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:142 ; year:2015 ; day:1 ; month:09 ; pages:43-50 ; extent:8 |
| Links: |
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| DOI / URN: |
10.1016/j.talanta.2015.04.038 |
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ELV018133118 |
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| 520 | |a Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. | ||
| 520 | |a Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. | ||
| 650 | 7 | |a Herbicides |2 Elsevier | |
| 650 | 7 | |a MIL-101(Cr) |2 Elsevier | |
| 650 | 7 | |a Dynamic microwave assisted extraction |2 Elsevier | |
| 650 | 7 | |a Non-polar solvent extraction |2 Elsevier | |
| 650 | 7 | |a Soybean |2 Elsevier | |
| 700 | 1 | |a Wu, Lijie |4 oth | |
| 700 | 1 | |a Nian, Li |4 oth | |
| 700 | 1 | |a Song, Ying |4 oth | |
| 700 | 1 | |a Lei, Lei |4 oth | |
| 700 | 1 | |a Yang, Xiao |4 oth | |
| 700 | 1 | |a Wang, Kun |4 oth | |
| 700 | 1 | |a Wang, Zhibing |4 oth | |
| 700 | 1 | |a Zhang, Liyuan |4 oth | |
| 700 | 1 | |a Zhang, Hanqi |4 oth | |
| 700 | 1 | |a Yu, Aimin |4 oth | |
| 700 | 1 | |a Zhang, Ziwei |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier Science |a Mohamed, S.H. ELSEVIER |t Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications |d 2019 |d the international journal of pure and applied analytical chemistry |g Amsterdam [u.a.] |w (DE-627)ELV003060667 |
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10.1016/j.talanta.2015.04.038 doi GBVA2015001000003.pica (DE-627)ELV018133118 (ELSEVIER)S0039-9140(15)00276-3 DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Li, Na verfasserin aut Dynamic microwave assisted extraction coupled with dispersive micro-solid-phase extraction of herbicides in soybeans 2015transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Herbicides Elsevier MIL-101(Cr) Elsevier Dynamic microwave assisted extraction Elsevier Non-polar solvent extraction Elsevier Soybean Elsevier Wu, Lijie oth Nian, Li oth Song, Ying oth Lei, Lei oth Yang, Xiao oth Wang, Kun oth Wang, Zhibing oth Zhang, Liyuan oth Zhang, Hanqi oth Yu, Aimin oth Zhang, Ziwei oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:142 year:2015 day:1 month:09 pages:43-50 extent:8 https://doi.org/10.1016/j.talanta.2015.04.038 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 142 2015 1 0901 43-50 8 045F 540 |
| spelling |
10.1016/j.talanta.2015.04.038 doi GBVA2015001000003.pica (DE-627)ELV018133118 (ELSEVIER)S0039-9140(15)00276-3 DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Li, Na verfasserin aut Dynamic microwave assisted extraction coupled with dispersive micro-solid-phase extraction of herbicides in soybeans 2015transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Herbicides Elsevier MIL-101(Cr) Elsevier Dynamic microwave assisted extraction Elsevier Non-polar solvent extraction Elsevier Soybean Elsevier Wu, Lijie oth Nian, Li oth Song, Ying oth Lei, Lei oth Yang, Xiao oth Wang, Kun oth Wang, Zhibing oth Zhang, Liyuan oth Zhang, Hanqi oth Yu, Aimin oth Zhang, Ziwei oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:142 year:2015 day:1 month:09 pages:43-50 extent:8 https://doi.org/10.1016/j.talanta.2015.04.038 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 142 2015 1 0901 43-50 8 045F 540 |
| allfields_unstemmed |
10.1016/j.talanta.2015.04.038 doi GBVA2015001000003.pica (DE-627)ELV018133118 (ELSEVIER)S0039-9140(15)00276-3 DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Li, Na verfasserin aut Dynamic microwave assisted extraction coupled with dispersive micro-solid-phase extraction of herbicides in soybeans 2015transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Herbicides Elsevier MIL-101(Cr) Elsevier Dynamic microwave assisted extraction Elsevier Non-polar solvent extraction Elsevier Soybean Elsevier Wu, Lijie oth Nian, Li oth Song, Ying oth Lei, Lei oth Yang, Xiao oth Wang, Kun oth Wang, Zhibing oth Zhang, Liyuan oth Zhang, Hanqi oth Yu, Aimin oth Zhang, Ziwei oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:142 year:2015 day:1 month:09 pages:43-50 extent:8 https://doi.org/10.1016/j.talanta.2015.04.038 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 142 2015 1 0901 43-50 8 045F 540 |
| allfieldsGer |
10.1016/j.talanta.2015.04.038 doi GBVA2015001000003.pica (DE-627)ELV018133118 (ELSEVIER)S0039-9140(15)00276-3 DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Li, Na verfasserin aut Dynamic microwave assisted extraction coupled with dispersive micro-solid-phase extraction of herbicides in soybeans 2015transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Herbicides Elsevier MIL-101(Cr) Elsevier Dynamic microwave assisted extraction Elsevier Non-polar solvent extraction Elsevier Soybean Elsevier Wu, Lijie oth Nian, Li oth Song, Ying oth Lei, Lei oth Yang, Xiao oth Wang, Kun oth Wang, Zhibing oth Zhang, Liyuan oth Zhang, Hanqi oth Yu, Aimin oth Zhang, Ziwei oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:142 year:2015 day:1 month:09 pages:43-50 extent:8 https://doi.org/10.1016/j.talanta.2015.04.038 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 142 2015 1 0901 43-50 8 045F 540 |
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10.1016/j.talanta.2015.04.038 doi GBVA2015001000003.pica (DE-627)ELV018133118 (ELSEVIER)S0039-9140(15)00276-3 DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Li, Na verfasserin aut Dynamic microwave assisted extraction coupled with dispersive micro-solid-phase extraction of herbicides in soybeans 2015transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. Herbicides Elsevier MIL-101(Cr) Elsevier Dynamic microwave assisted extraction Elsevier Non-polar solvent extraction Elsevier Soybean Elsevier Wu, Lijie oth Nian, Li oth Song, Ying oth Lei, Lei oth Yang, Xiao oth Wang, Kun oth Wang, Zhibing oth Zhang, Liyuan oth Zhang, Hanqi oth Yu, Aimin oth Zhang, Ziwei oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:142 year:2015 day:1 month:09 pages:43-50 extent:8 https://doi.org/10.1016/j.talanta.2015.04.038 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 142 2015 1 0901 43-50 8 045F 540 |
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English |
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Enthalten in Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications Amsterdam [u.a.] volume:142 year:2015 day:1 month:09 pages:43-50 extent:8 |
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Enthalten in Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications Amsterdam [u.a.] volume:142 year:2015 day:1 month:09 pages:43-50 extent:8 |
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Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications |
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dynamic microwave assisted extraction coupled with dispersive micro-solid-phase extraction of herbicides in soybeans |
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Dynamic microwave assisted extraction coupled with dispersive micro-solid-phase extraction of herbicides in soybeans |
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Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. |
| abstractGer |
Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. |
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Non-polar solvent dynamic microwave assisted extraction was firstly applied to the treatment of high-fat soybean samples. In the dispersive micro-solid-phase extraction (d-µ-SPE), the herbicides in the high-fat extract were directly adsorbed on metal-organic frameworks MIL-101(Cr). The effects of several experimental parameters, including extraction solvent, microwave absorption medium, microwave power, volume and flow rate of extraction solvent, amount of MIL-101(Cr), and d-µ-SPE time, were investigated. At the optimal conditions, the limits of detection for the herbicides ranged from 1.56 to 2.00μgkg−1. The relative recoveries of the herbicides were in the range of 91.1–106.7%, and relative standard deviations were equal to or lower than 6.7%. The present method was simple, rapid and effective. A large amount of fat was also removed. This method was demonstrated to be suitable for treatment of high-fat samples. |
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