Electrocatalytic determination of chloramphenicol based on molybdenum disulfide nanosheets and self-doped polyaniline
In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the stro...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Yang, Ruirui [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015transfer abstract |
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| Umfang: |
5 |
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| Übergeordnetes Werk: |
Enthalten in: Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications - Mohamed, S.H. ELSEVIER, 2019, the international journal of pure and applied analytical chemistry, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:131 ; year:2015 ; pages:619-623 ; extent:5 |
| Links: |
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| DOI / URN: |
10.1016/j.talanta.2014.08.035 |
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| 520 | |a In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. | ||
| 520 | |a In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. | ||
| 650 | 7 | |a Liquid exfoliation |2 Elsevier | |
| 650 | 7 | |a Ultrasonication |2 Elsevier | |
| 650 | 7 | |a Chloramphenicol |2 Elsevier | |
| 650 | 7 | |a Self-doped polyaniline |2 Elsevier | |
| 650 | 7 | |a Molybdenum disulfide nanosheet |2 Elsevier | |
| 650 | 7 | |a Differential pulse voltammetry |2 Elsevier | |
| 700 | 1 | |a Zhao, Jinlong |4 oth | |
| 700 | 1 | |a Chen, Meijing |4 oth | |
| 700 | 1 | |a Yang, Tao |4 oth | |
| 700 | 1 | |a Luo, Shizhong |4 oth | |
| 700 | 1 | |a Jiao, Kui |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier Science |a Mohamed, S.H. ELSEVIER |t Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications |d 2019 |d the international journal of pure and applied analytical chemistry |g Amsterdam [u.a.] |w (DE-627)ELV003060667 |
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10.1016/j.talanta.2014.08.035 doi GBVA2015001000003.pica (DE-627)ELV018139736 (ELSEVIER)S0039-9140(14)00705-X DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Yang, Ruirui verfasserin aut Electrocatalytic determination of chloramphenicol based on molybdenum disulfide nanosheets and self-doped polyaniline 2015transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. Liquid exfoliation Elsevier Ultrasonication Elsevier Chloramphenicol Elsevier Self-doped polyaniline Elsevier Molybdenum disulfide nanosheet Elsevier Differential pulse voltammetry Elsevier Zhao, Jinlong oth Chen, Meijing oth Yang, Tao oth Luo, Shizhong oth Jiao, Kui oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:131 year:2015 pages:619-623 extent:5 https://doi.org/10.1016/j.talanta.2014.08.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 131 2015 619-623 5 045F 540 |
| spelling |
10.1016/j.talanta.2014.08.035 doi GBVA2015001000003.pica (DE-627)ELV018139736 (ELSEVIER)S0039-9140(14)00705-X DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Yang, Ruirui verfasserin aut Electrocatalytic determination of chloramphenicol based on molybdenum disulfide nanosheets and self-doped polyaniline 2015transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. Liquid exfoliation Elsevier Ultrasonication Elsevier Chloramphenicol Elsevier Self-doped polyaniline Elsevier Molybdenum disulfide nanosheet Elsevier Differential pulse voltammetry Elsevier Zhao, Jinlong oth Chen, Meijing oth Yang, Tao oth Luo, Shizhong oth Jiao, Kui oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:131 year:2015 pages:619-623 extent:5 https://doi.org/10.1016/j.talanta.2014.08.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 131 2015 619-623 5 045F 540 |
| allfields_unstemmed |
10.1016/j.talanta.2014.08.035 doi GBVA2015001000003.pica (DE-627)ELV018139736 (ELSEVIER)S0039-9140(14)00705-X DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Yang, Ruirui verfasserin aut Electrocatalytic determination of chloramphenicol based on molybdenum disulfide nanosheets and self-doped polyaniline 2015transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. Liquid exfoliation Elsevier Ultrasonication Elsevier Chloramphenicol Elsevier Self-doped polyaniline Elsevier Molybdenum disulfide nanosheet Elsevier Differential pulse voltammetry Elsevier Zhao, Jinlong oth Chen, Meijing oth Yang, Tao oth Luo, Shizhong oth Jiao, Kui oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:131 year:2015 pages:619-623 extent:5 https://doi.org/10.1016/j.talanta.2014.08.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 131 2015 619-623 5 045F 540 |
| allfieldsGer |
10.1016/j.talanta.2014.08.035 doi GBVA2015001000003.pica (DE-627)ELV018139736 (ELSEVIER)S0039-9140(14)00705-X DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Yang, Ruirui verfasserin aut Electrocatalytic determination of chloramphenicol based on molybdenum disulfide nanosheets and self-doped polyaniline 2015transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. Liquid exfoliation Elsevier Ultrasonication Elsevier Chloramphenicol Elsevier Self-doped polyaniline Elsevier Molybdenum disulfide nanosheet Elsevier Differential pulse voltammetry Elsevier Zhao, Jinlong oth Chen, Meijing oth Yang, Tao oth Luo, Shizhong oth Jiao, Kui oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:131 year:2015 pages:619-623 extent:5 https://doi.org/10.1016/j.talanta.2014.08.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 131 2015 619-623 5 045F 540 |
| allfieldsSound |
10.1016/j.talanta.2014.08.035 doi GBVA2015001000003.pica (DE-627)ELV018139736 (ELSEVIER)S0039-9140(14)00705-X DE-627 ger DE-627 rakwb eng 540 540 DE-600 530 620 VZ 53.56 bkl Yang, Ruirui verfasserin aut Electrocatalytic determination of chloramphenicol based on molybdenum disulfide nanosheets and self-doped polyaniline 2015transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. Liquid exfoliation Elsevier Ultrasonication Elsevier Chloramphenicol Elsevier Self-doped polyaniline Elsevier Molybdenum disulfide nanosheet Elsevier Differential pulse voltammetry Elsevier Zhao, Jinlong oth Chen, Meijing oth Yang, Tao oth Luo, Shizhong oth Jiao, Kui oth Enthalten in Elsevier Science Mohamed, S.H. ELSEVIER Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications 2019 the international journal of pure and applied analytical chemistry Amsterdam [u.a.] (DE-627)ELV003060667 volume:131 year:2015 pages:619-623 extent:5 https://doi.org/10.1016/j.talanta.2014.08.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 53.56 Halbleitertechnologie VZ AR 131 2015 619-623 5 045F 540 |
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English |
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Enthalten in Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications Amsterdam [u.a.] volume:131 year:2015 pages:619-623 extent:5 |
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Enthalten in Optical, water splitting and wettability of titanium nitride/titanium oxynitride bilayer films for hydrogen generation and solar cells applications Amsterdam [u.a.] volume:131 year:2015 pages:619-623 extent:5 |
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In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules.</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. 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Electrocatalytic determination of chloramphenicol based on molybdenum disulfide nanosheets and self-doped polyaniline |
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In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. |
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In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. |
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In this paper, a novel molybdenum disulfide (MoS2) intercalated by self-doped polyaniline (SPAN) via ultrasonic exfoliating method was prepared to show outstanding conductivity and synergistic electrocatalytic activity using chloramphenicol (CAP) as a case. In the ultrasonic process, due to the strong π–π ⁎ stacking interaction and electrostatic repulsion, the negatively charged SPAN served as an intercalator to result in few-layers MoS2 nanosheets, which were exfoliated from bulk MoS2. This nanocomposite was characterized by scanning electron microscopy, transmission electron microscopy and differential pulse voltammetry. The obtained nanocomposite owns large conjugated structure and rich negative charge, which can improve the adsorption of conjugate structured CAP with the detection range from 0.1 to 1000μmolL−1. The results also showed that the electrocatalytic responses were further affected by the mass ratio of SPAN–MoS2 and the ultrasonication time. Our electrocatalytic platform could be further applied in the adsorption and detection of other positively charged biomolecules or aromatic molecules. |
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