Specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids
Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Terekhova, Irina [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015transfer abstract |
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| Schlagwörter: |
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| Umfang: |
7 |
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| Übergeordnetes Werk: |
Enthalten in: Plasticity in responses to dimensional variations of soil space in 19 grassland plant species - Dong, Ran ELSEVIER, 2022, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:122 ; year:2015 ; day:27 ; month:01 ; pages:97-103 ; extent:7 |
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| DOI / URN: |
10.1016/j.ces.2014.09.025 |
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| 245 | 1 | 0 | |a Specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids |
| 264 | 1 | |c 2015transfer abstract | |
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| 520 | |a Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. | ||
| 520 | |a Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. | ||
| 650 | 7 | |a Thermodynamics |2 Elsevier | |
| 650 | 7 | |a Cyclodextrin |2 Elsevier | |
| 650 | 7 | |a Complex formation |2 Elsevier | |
| 650 | 7 | |a Salt effect |2 Elsevier | |
| 650 | 7 | |a m-Aminobenzoic acid |2 Elsevier | |
| 650 | 7 | |a Nicotinic acid |2 Elsevier | |
| 700 | 1 | |a Chibunova, Ekaterina |4 oth | |
| 700 | 1 | |a Kumeev, Roman |4 oth | |
| 700 | 1 | |a Kruchinin, Sergey |4 oth | |
| 700 | 1 | |a Fedotova, Marina |4 oth | |
| 700 | 1 | |a Kozbiał, Małgorzata |4 oth | |
| 700 | 1 | |a Wszelaka-Rylik, Małgorzata |4 oth | |
| 700 | 1 | |a Gierycz, Pawel |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier Science |a Dong, Ran ELSEVIER |t Plasticity in responses to dimensional variations of soil space in 19 grassland plant species |d 2022 |g Amsterdam [u.a.] |w (DE-627)ELV008347182 |
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10.1016/j.ces.2014.09.025 doi GBV00000000000184A.pica (DE-627)ELV018841767 (ELSEVIER)S0009-2509(14)00529-6 DE-627 ger DE-627 rakwb eng 660 660 DE-600 570 630 VZ BIODIV DE-30 fid Terekhova, Irina verfasserin aut Specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Thermodynamics Elsevier Cyclodextrin Elsevier Complex formation Elsevier Salt effect Elsevier m-Aminobenzoic acid Elsevier Nicotinic acid Elsevier Chibunova, Ekaterina oth Kumeev, Roman oth Kruchinin, Sergey oth Fedotova, Marina oth Kozbiał, Małgorzata oth Wszelaka-Rylik, Małgorzata oth Gierycz, Pawel oth Enthalten in Elsevier Science Dong, Ran ELSEVIER Plasticity in responses to dimensional variations of soil space in 19 grassland plant species 2022 Amsterdam [u.a.] (DE-627)ELV008347182 volume:122 year:2015 day:27 month:01 pages:97-103 extent:7 https://doi.org/10.1016/j.ces.2014.09.025 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA AR 122 2015 27 0127 97-103 7 045F 660 |
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10.1016/j.ces.2014.09.025 doi GBV00000000000184A.pica (DE-627)ELV018841767 (ELSEVIER)S0009-2509(14)00529-6 DE-627 ger DE-627 rakwb eng 660 660 DE-600 570 630 VZ BIODIV DE-30 fid Terekhova, Irina verfasserin aut Specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Thermodynamics Elsevier Cyclodextrin Elsevier Complex formation Elsevier Salt effect Elsevier m-Aminobenzoic acid Elsevier Nicotinic acid Elsevier Chibunova, Ekaterina oth Kumeev, Roman oth Kruchinin, Sergey oth Fedotova, Marina oth Kozbiał, Małgorzata oth Wszelaka-Rylik, Małgorzata oth Gierycz, Pawel oth Enthalten in Elsevier Science Dong, Ran ELSEVIER Plasticity in responses to dimensional variations of soil space in 19 grassland plant species 2022 Amsterdam [u.a.] (DE-627)ELV008347182 volume:122 year:2015 day:27 month:01 pages:97-103 extent:7 https://doi.org/10.1016/j.ces.2014.09.025 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA AR 122 2015 27 0127 97-103 7 045F 660 |
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10.1016/j.ces.2014.09.025 doi GBV00000000000184A.pica (DE-627)ELV018841767 (ELSEVIER)S0009-2509(14)00529-6 DE-627 ger DE-627 rakwb eng 660 660 DE-600 570 630 VZ BIODIV DE-30 fid Terekhova, Irina verfasserin aut Specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Thermodynamics Elsevier Cyclodextrin Elsevier Complex formation Elsevier Salt effect Elsevier m-Aminobenzoic acid Elsevier Nicotinic acid Elsevier Chibunova, Ekaterina oth Kumeev, Roman oth Kruchinin, Sergey oth Fedotova, Marina oth Kozbiał, Małgorzata oth Wszelaka-Rylik, Małgorzata oth Gierycz, Pawel oth Enthalten in Elsevier Science Dong, Ran ELSEVIER Plasticity in responses to dimensional variations of soil space in 19 grassland plant species 2022 Amsterdam [u.a.] (DE-627)ELV008347182 volume:122 year:2015 day:27 month:01 pages:97-103 extent:7 https://doi.org/10.1016/j.ces.2014.09.025 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA AR 122 2015 27 0127 97-103 7 045F 660 |
| allfieldsGer |
10.1016/j.ces.2014.09.025 doi GBV00000000000184A.pica (DE-627)ELV018841767 (ELSEVIER)S0009-2509(14)00529-6 DE-627 ger DE-627 rakwb eng 660 660 DE-600 570 630 VZ BIODIV DE-30 fid Terekhova, Irina verfasserin aut Specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Thermodynamics Elsevier Cyclodextrin Elsevier Complex formation Elsevier Salt effect Elsevier m-Aminobenzoic acid Elsevier Nicotinic acid Elsevier Chibunova, Ekaterina oth Kumeev, Roman oth Kruchinin, Sergey oth Fedotova, Marina oth Kozbiał, Małgorzata oth Wszelaka-Rylik, Małgorzata oth Gierycz, Pawel oth Enthalten in Elsevier Science Dong, Ran ELSEVIER Plasticity in responses to dimensional variations of soil space in 19 grassland plant species 2022 Amsterdam [u.a.] (DE-627)ELV008347182 volume:122 year:2015 day:27 month:01 pages:97-103 extent:7 https://doi.org/10.1016/j.ces.2014.09.025 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA AR 122 2015 27 0127 97-103 7 045F 660 |
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10.1016/j.ces.2014.09.025 doi GBV00000000000184A.pica (DE-627)ELV018841767 (ELSEVIER)S0009-2509(14)00529-6 DE-627 ger DE-627 rakwb eng 660 660 DE-600 570 630 VZ BIODIV DE-30 fid Terekhova, Irina verfasserin aut Specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. Thermodynamics Elsevier Cyclodextrin Elsevier Complex formation Elsevier Salt effect Elsevier m-Aminobenzoic acid Elsevier Nicotinic acid Elsevier Chibunova, Ekaterina oth Kumeev, Roman oth Kruchinin, Sergey oth Fedotova, Marina oth Kozbiał, Małgorzata oth Wszelaka-Rylik, Małgorzata oth Gierycz, Pawel oth Enthalten in Elsevier Science Dong, Ran ELSEVIER Plasticity in responses to dimensional variations of soil space in 19 grassland plant species 2022 Amsterdam [u.a.] (DE-627)ELV008347182 volume:122 year:2015 day:27 month:01 pages:97-103 extent:7 https://doi.org/10.1016/j.ces.2014.09.025 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA AR 122 2015 27 0127 97-103 7 045F 660 |
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Enthalten in Plasticity in responses to dimensional variations of soil space in 19 grassland plant species Amsterdam [u.a.] volume:122 year:2015 day:27 month:01 pages:97-103 extent:7 |
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Enthalten in Plasticity in responses to dimensional variations of soil space in 19 grassland plant species Amsterdam [u.a.] volume:122 year:2015 day:27 month:01 pages:97-103 extent:7 |
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specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids |
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Specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids |
| abstract |
Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. |
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Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. |
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Inclusion complex formation of α- and β-cyclodextrins with zwitterionic nicotinic and m-aminobenzoic acids in water and 0.2M solutions of KCl, KBr, KH2PO4 and K2SO4 was studied by 1H NMR and UV-spectroscopy. We complemented the experiments with statistical mechanics calculations in the framework of the 3D-RISM approach to analyze the ion-binding between inorganic univalent anions and positively charged groups of the acids under study. It was detected that binding affinity of cyclodextrins to the acids is decreased in the presence of the salts. This is caused by specific and nonspecific action of the considered inorganic anions. The influence of the Cl− and SO 4 2 − was found to be nonspecific and insignificant. On the contrary, Br− and H 2 PO 4 − ions can considerably affect the inclusion complex formation. Insertion of Br− into the macrocyclic cavity and attraction between H 2 PO 4 − and the zwitterions are the main processes competing with cyclodextrin–acid binding. It has been demonstrated that the manifestation of the salt effects depends on the cyclodextrin cavity size, ionization state of the acid and other experimental conditions. |
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Specific and nonspecific effects of biologically active inorganic salts on inclusion complex formation of cyclodextrins with aromatic carboxylic acids |
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