Nebulized spray pyrolysis: a new method for synthesis of graphene film and their characteristics
A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited...
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| Autor*in: |
Illakkiya, J. Tamil [verfasserIn] |
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E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2016transfer abstract |
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| Umfang: |
8 |
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| Übergeordnetes Werk: |
Enthalten in: A high efficiency solar steam generation system with using residual heat to enhance steam escape - Bai, Binglin ELSEVIER, 2020, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:307 ; year:2016 ; day:15 ; month:12 ; pages:65-72 ; extent:8 |
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| DOI / URN: |
10.1016/j.surfcoat.2016.08.051 |
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| 520 | |a A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. | ||
| 520 | |a A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. | ||
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10.1016/j.surfcoat.2016.08.051 doi GBV00000000000077A.pica (DE-627)ELV019255233 (ELSEVIER)S0257-8972(16)30805-2 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Illakkiya, J. Tamil verfasserin aut Nebulized spray pyrolysis: a new method for synthesis of graphene film and their characteristics 2016transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. Rajalakshmi, P. Usha oth Oommen, Rachel oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:307 year:2016 day:15 month:12 pages:65-72 extent:8 https://doi.org/10.1016/j.surfcoat.2016.08.051 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 307 2016 15 1215 65-72 8 045F 620 |
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10.1016/j.surfcoat.2016.08.051 doi GBV00000000000077A.pica (DE-627)ELV019255233 (ELSEVIER)S0257-8972(16)30805-2 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Illakkiya, J. Tamil verfasserin aut Nebulized spray pyrolysis: a new method for synthesis of graphene film and their characteristics 2016transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. Rajalakshmi, P. Usha oth Oommen, Rachel oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:307 year:2016 day:15 month:12 pages:65-72 extent:8 https://doi.org/10.1016/j.surfcoat.2016.08.051 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 307 2016 15 1215 65-72 8 045F 620 |
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10.1016/j.surfcoat.2016.08.051 doi GBV00000000000077A.pica (DE-627)ELV019255233 (ELSEVIER)S0257-8972(16)30805-2 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Illakkiya, J. Tamil verfasserin aut Nebulized spray pyrolysis: a new method for synthesis of graphene film and their characteristics 2016transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. Rajalakshmi, P. Usha oth Oommen, Rachel oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:307 year:2016 day:15 month:12 pages:65-72 extent:8 https://doi.org/10.1016/j.surfcoat.2016.08.051 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 307 2016 15 1215 65-72 8 045F 620 |
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10.1016/j.surfcoat.2016.08.051 doi GBV00000000000077A.pica (DE-627)ELV019255233 (ELSEVIER)S0257-8972(16)30805-2 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Illakkiya, J. Tamil verfasserin aut Nebulized spray pyrolysis: a new method for synthesis of graphene film and their characteristics 2016transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. Rajalakshmi, P. Usha oth Oommen, Rachel oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:307 year:2016 day:15 month:12 pages:65-72 extent:8 https://doi.org/10.1016/j.surfcoat.2016.08.051 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 307 2016 15 1215 65-72 8 045F 620 |
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10.1016/j.surfcoat.2016.08.051 doi GBV00000000000077A.pica (DE-627)ELV019255233 (ELSEVIER)S0257-8972(16)30805-2 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Illakkiya, J. Tamil verfasserin aut Nebulized spray pyrolysis: a new method for synthesis of graphene film and their characteristics 2016transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. Rajalakshmi, P. Usha oth Oommen, Rachel oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:307 year:2016 day:15 month:12 pages:65-72 extent:8 https://doi.org/10.1016/j.surfcoat.2016.08.051 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 307 2016 15 1215 65-72 8 045F 620 |
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Nebulized spray pyrolysis: a new method for synthesis of graphene film and their characteristics |
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A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. |
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A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. |
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A simple way to synthesis phase pure graphene film from graphene oxide is demonstrated. Dextrose and hydrazine hydrate are used as reducing agents to convert graphene oxide to graphene. The as-synthesized graphene was deposited on glass substrate by nebulized spray pyrolysis technique. The deposited film was characterized by Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), Raman spectroscopy, UV–visible spectroscopy, Scanning electron microscopy and Hall measurement. The electrochemical characteristics of the film are analyzed by electrochemical impedance spectroscopy. The de-oxygenation of graphene oxide is confirmed by XRD, XPS, FTIR and Raman studies. The optical absorption of graphene layers is observed at 290nm suggesting the transformation of graphene oxide to graphene. The majority carrier in graphene film is found to be holes, indicating p-type conductivity. The carrier mobility and carrier density of the as-deposited graphene are found to be 2.21×102 cm2/Vs and 1.98×1016 cm−3. The acceptor density and flat band potential are found to be 9.045×1022 cm−3 and 600mV respectively. The charge transfer resistance (Rct), series resistance (Rs) and double layer capacitance (Cdl) of graphene/polysulfide system are found to be 6.57Ω, 862Ω and 151μF respectively. |
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