Performance of Ni-rich bimetallic phosphides on simultaneous quinoline hydrodenitrogenation and dibenzothiophene hydrodesulfurization
A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% anoth...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Fang, Mengxiang [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015transfer abstract |
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| Umfang: |
9 |
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| Übergeordnetes Werk: |
Enthalten in: Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications - Saini, Hardev S. ELSEVIER, 2015transfer abstract, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:129 ; year:2015 ; pages:236-244 ; extent:9 |
| Links: |
|---|
| DOI / URN: |
10.1016/j.fuproc.2014.09.020 |
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| 520 | |a A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. | ||
| 520 | |a A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. | ||
| 700 | 1 | |a Tang, Wei |4 oth | |
| 700 | 1 | |a Yu, Chunjiang |4 oth | |
| 700 | 1 | |a Xia, Liangyan |4 oth | |
| 700 | 1 | |a Xia, Zhixiang |4 oth | |
| 700 | 1 | |a Wang, Qinhui |4 oth | |
| 700 | 1 | |a Luo, Zhongyang |4 oth | |
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10.1016/j.fuproc.2014.09.020 doi GBVA2015012000028.pica (DE-627)ELV023660996 (ELSEVIER)S0378-3820(14)00391-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Fang, Mengxiang verfasserin aut Performance of Ni-rich bimetallic phosphides on simultaneous quinoline hydrodenitrogenation and dibenzothiophene hydrodesulfurization 2015transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. Tang, Wei oth Yu, Chunjiang oth Xia, Liangyan oth Xia, Zhixiang oth Wang, Qinhui oth Luo, Zhongyang oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:129 year:2015 pages:236-244 extent:9 https://doi.org/10.1016/j.fuproc.2014.09.020 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 129 2015 236-244 9 045F 660 |
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10.1016/j.fuproc.2014.09.020 doi GBVA2015012000028.pica (DE-627)ELV023660996 (ELSEVIER)S0378-3820(14)00391-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Fang, Mengxiang verfasserin aut Performance of Ni-rich bimetallic phosphides on simultaneous quinoline hydrodenitrogenation and dibenzothiophene hydrodesulfurization 2015transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. Tang, Wei oth Yu, Chunjiang oth Xia, Liangyan oth Xia, Zhixiang oth Wang, Qinhui oth Luo, Zhongyang oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:129 year:2015 pages:236-244 extent:9 https://doi.org/10.1016/j.fuproc.2014.09.020 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 129 2015 236-244 9 045F 660 |
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10.1016/j.fuproc.2014.09.020 doi GBVA2015012000028.pica (DE-627)ELV023660996 (ELSEVIER)S0378-3820(14)00391-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Fang, Mengxiang verfasserin aut Performance of Ni-rich bimetallic phosphides on simultaneous quinoline hydrodenitrogenation and dibenzothiophene hydrodesulfurization 2015transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. Tang, Wei oth Yu, Chunjiang oth Xia, Liangyan oth Xia, Zhixiang oth Wang, Qinhui oth Luo, Zhongyang oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:129 year:2015 pages:236-244 extent:9 https://doi.org/10.1016/j.fuproc.2014.09.020 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 129 2015 236-244 9 045F 660 |
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10.1016/j.fuproc.2014.09.020 doi GBVA2015012000028.pica (DE-627)ELV023660996 (ELSEVIER)S0378-3820(14)00391-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Fang, Mengxiang verfasserin aut Performance of Ni-rich bimetallic phosphides on simultaneous quinoline hydrodenitrogenation and dibenzothiophene hydrodesulfurization 2015transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. Tang, Wei oth Yu, Chunjiang oth Xia, Liangyan oth Xia, Zhixiang oth Wang, Qinhui oth Luo, Zhongyang oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:129 year:2015 pages:236-244 extent:9 https://doi.org/10.1016/j.fuproc.2014.09.020 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 129 2015 236-244 9 045F 660 |
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10.1016/j.fuproc.2014.09.020 doi GBVA2015012000028.pica (DE-627)ELV023660996 (ELSEVIER)S0378-3820(14)00391-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Fang, Mengxiang verfasserin aut Performance of Ni-rich bimetallic phosphides on simultaneous quinoline hydrodenitrogenation and dibenzothiophene hydrodesulfurization 2015transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. Tang, Wei oth Yu, Chunjiang oth Xia, Liangyan oth Xia, Zhixiang oth Wang, Qinhui oth Luo, Zhongyang oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:129 year:2015 pages:236-244 extent:9 https://doi.org/10.1016/j.fuproc.2014.09.020 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 129 2015 236-244 9 045F 660 |
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Enthalten in Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications New York, NY [u.a.] volume:129 year:2015 pages:236-244 extent:9 |
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Enthalten in Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications New York, NY [u.a.] volume:129 year:2015 pages:236-244 extent:9 |
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Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications |
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Fang, Mengxiang @@aut@@ Tang, Wei @@oth@@ Yu, Chunjiang @@oth@@ Xia, Liangyan @@oth@@ Xia, Zhixiang @@oth@@ Wang, Qinhui @@oth@@ Luo, Zhongyang @@oth@@ |
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Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications |
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performance of ni-rich bimetallic phosphides on simultaneous quinoline hydrodenitrogenation and dibenzothiophene hydrodesulfurization |
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Performance of Ni-rich bimetallic phosphides on simultaneous quinoline hydrodenitrogenation and dibenzothiophene hydrodesulfurization |
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A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. |
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A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. |
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A series of Ni-rich bimetallic phosphides incorporating different metals were successfully prepared by initial wetness impregnation, followed by temperature-programmed reduction. Catalyst characterization indicates that the bulk structure and physical properties maintained after adding 2.5mol% another metal on Ni2P. Electron transfer from the second metal to Ni was found on Mo0.05Ni1.95P, Co0.05Ni1.95P, and Fe0.05Ni1.95P, except on W0.05Ni1.95P. Simultaneous hydrodenitrogenation (HDN) of quinoline and hydrodesulfurization (HDS) of dibenzothiophene (DBT) over phosphides and a commercial metal sulfide were studied at 320–380°C, 3MPa, weight hourly space velocity of 6h−1, and H2/feed ratio of 500:1. Metal phosphides show higher HDN of quinoline and the same HDS of dibenzothiophene activities than that of a commercial catalyst at 380°C. Mo0.05Ni1.95P shows the best performance and lowest N and S content adsorbed on the catalyst, due to the active M(2) sites. HDS conversion and product selectivities are seriously impacted by the adsorption of N-containing compounds on active sites of catalysts. Increasing temperature to 360°C or/and decreasing N content to less than 1000ppm quinoline in the feed are suggested to obtain simultaneous efficient removal of N and S. |
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Performance of Ni-rich bimetallic phosphides on simultaneous quinoline hydrodenitrogenation and dibenzothiophene hydrodesulfurization |
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