Unusual crystallization and melting behavior induced by microphase separation in MPEG-b-PLLA diblock copolymer
The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influ...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Zhou, Dongdong [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015transfer abstract |
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| Umfang: |
7 |
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| Übergeordnetes Werk: |
Enthalten in: Functional outcomes at 12 months for patients with traumatic brain injury, intracerebral haemorrhage and subarachnoid haemorrhage treated in an Australian neurocritical care unit: A prospective cohort study - Fitzgerald, Emily ELSEVIER, 2020, the international journal for the science and technology of polymers, Oxford |
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| Übergeordnetes Werk: |
volume:80 ; year:2015 ; day:2 ; month:12 ; pages:123-129 ; extent:7 |
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| DOI / URN: |
10.1016/j.polymer.2015.10.066 |
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| 245 | 1 | 0 | |a Unusual crystallization and melting behavior induced by microphase separation in MPEG-b-PLLA diblock copolymer |
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| 520 | |a The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. | ||
| 520 | |a The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. | ||
| 650 | 7 | |a Microphase separation |2 Elsevier | |
| 650 | 7 | |a Melting behaviors |2 Elsevier | |
| 650 | 7 | |a MPEG-b-PLLA diblock copolymer |2 Elsevier | |
| 700 | 1 | |a Sun, Jingru |4 oth | |
| 700 | 1 | |a Shao, Jun |4 oth | |
| 700 | 1 | |a Bian, Xinchao |4 oth | |
| 700 | 1 | |a Huang, Shaoyong |4 oth | |
| 700 | 1 | |a Li, Gao |4 oth | |
| 700 | 1 | |a Chen, Xuesi |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier Science |a Fitzgerald, Emily ELSEVIER |t Functional outcomes at 12 months for patients with traumatic brain injury, intracerebral haemorrhage and subarachnoid haemorrhage treated in an Australian neurocritical care unit: A prospective cohort study |d 2020 |d the international journal for the science and technology of polymers |g Oxford |w (DE-627)ELV005093368 |
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10.1016/j.polymer.2015.10.066 doi GBVA2015023000022.pica (DE-627)ELV024089133 (ELSEVIER)S0032-3861(15)30352-9 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.63 bkl 44.69 bkl Zhou, Dongdong verfasserin aut Unusual crystallization and melting behavior induced by microphase separation in MPEG-b-PLLA diblock copolymer 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. Microphase separation Elsevier Melting behaviors Elsevier MPEG-b-PLLA diblock copolymer Elsevier Sun, Jingru oth Shao, Jun oth Bian, Xinchao oth Huang, Shaoyong oth Li, Gao oth Chen, Xuesi oth Enthalten in Elsevier Science Fitzgerald, Emily ELSEVIER Functional outcomes at 12 months for patients with traumatic brain injury, intracerebral haemorrhage and subarachnoid haemorrhage treated in an Australian neurocritical care unit: A prospective cohort study 2020 the international journal for the science and technology of polymers Oxford (DE-627)ELV005093368 volume:80 year:2015 day:2 month:12 pages:123-129 extent:7 https://doi.org/10.1016/j.polymer.2015.10.066 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.63 Krankenpflege VZ 44.69 Intensivmedizin VZ AR 80 2015 2 1202 123-129 7 045F 540 |
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10.1016/j.polymer.2015.10.066 doi GBVA2015023000022.pica (DE-627)ELV024089133 (ELSEVIER)S0032-3861(15)30352-9 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.63 bkl 44.69 bkl Zhou, Dongdong verfasserin aut Unusual crystallization and melting behavior induced by microphase separation in MPEG-b-PLLA diblock copolymer 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. Microphase separation Elsevier Melting behaviors Elsevier MPEG-b-PLLA diblock copolymer Elsevier Sun, Jingru oth Shao, Jun oth Bian, Xinchao oth Huang, Shaoyong oth Li, Gao oth Chen, Xuesi oth Enthalten in Elsevier Science Fitzgerald, Emily ELSEVIER Functional outcomes at 12 months for patients with traumatic brain injury, intracerebral haemorrhage and subarachnoid haemorrhage treated in an Australian neurocritical care unit: A prospective cohort study 2020 the international journal for the science and technology of polymers Oxford (DE-627)ELV005093368 volume:80 year:2015 day:2 month:12 pages:123-129 extent:7 https://doi.org/10.1016/j.polymer.2015.10.066 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.63 Krankenpflege VZ 44.69 Intensivmedizin VZ AR 80 2015 2 1202 123-129 7 045F 540 |
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10.1016/j.polymer.2015.10.066 doi GBVA2015023000022.pica (DE-627)ELV024089133 (ELSEVIER)S0032-3861(15)30352-9 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.63 bkl 44.69 bkl Zhou, Dongdong verfasserin aut Unusual crystallization and melting behavior induced by microphase separation in MPEG-b-PLLA diblock copolymer 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. Microphase separation Elsevier Melting behaviors Elsevier MPEG-b-PLLA diblock copolymer Elsevier Sun, Jingru oth Shao, Jun oth Bian, Xinchao oth Huang, Shaoyong oth Li, Gao oth Chen, Xuesi oth Enthalten in Elsevier Science Fitzgerald, Emily ELSEVIER Functional outcomes at 12 months for patients with traumatic brain injury, intracerebral haemorrhage and subarachnoid haemorrhage treated in an Australian neurocritical care unit: A prospective cohort study 2020 the international journal for the science and technology of polymers Oxford (DE-627)ELV005093368 volume:80 year:2015 day:2 month:12 pages:123-129 extent:7 https://doi.org/10.1016/j.polymer.2015.10.066 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.63 Krankenpflege VZ 44.69 Intensivmedizin VZ AR 80 2015 2 1202 123-129 7 045F 540 |
| allfieldsGer |
10.1016/j.polymer.2015.10.066 doi GBVA2015023000022.pica (DE-627)ELV024089133 (ELSEVIER)S0032-3861(15)30352-9 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.63 bkl 44.69 bkl Zhou, Dongdong verfasserin aut Unusual crystallization and melting behavior induced by microphase separation in MPEG-b-PLLA diblock copolymer 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. Microphase separation Elsevier Melting behaviors Elsevier MPEG-b-PLLA diblock copolymer Elsevier Sun, Jingru oth Shao, Jun oth Bian, Xinchao oth Huang, Shaoyong oth Li, Gao oth Chen, Xuesi oth Enthalten in Elsevier Science Fitzgerald, Emily ELSEVIER Functional outcomes at 12 months for patients with traumatic brain injury, intracerebral haemorrhage and subarachnoid haemorrhage treated in an Australian neurocritical care unit: A prospective cohort study 2020 the international journal for the science and technology of polymers Oxford (DE-627)ELV005093368 volume:80 year:2015 day:2 month:12 pages:123-129 extent:7 https://doi.org/10.1016/j.polymer.2015.10.066 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.63 Krankenpflege VZ 44.69 Intensivmedizin VZ AR 80 2015 2 1202 123-129 7 045F 540 |
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10.1016/j.polymer.2015.10.066 doi GBVA2015023000022.pica (DE-627)ELV024089133 (ELSEVIER)S0032-3861(15)30352-9 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.63 bkl 44.69 bkl Zhou, Dongdong verfasserin aut Unusual crystallization and melting behavior induced by microphase separation in MPEG-b-PLLA diblock copolymer 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. Microphase separation Elsevier Melting behaviors Elsevier MPEG-b-PLLA diblock copolymer Elsevier Sun, Jingru oth Shao, Jun oth Bian, Xinchao oth Huang, Shaoyong oth Li, Gao oth Chen, Xuesi oth Enthalten in Elsevier Science Fitzgerald, Emily ELSEVIER Functional outcomes at 12 months for patients with traumatic brain injury, intracerebral haemorrhage and subarachnoid haemorrhage treated in an Australian neurocritical care unit: A prospective cohort study 2020 the international journal for the science and technology of polymers Oxford (DE-627)ELV005093368 volume:80 year:2015 day:2 month:12 pages:123-129 extent:7 https://doi.org/10.1016/j.polymer.2015.10.066 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.63 Krankenpflege VZ 44.69 Intensivmedizin VZ AR 80 2015 2 1202 123-129 7 045F 540 |
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Enthalten in Functional outcomes at 12 months for patients with traumatic brain injury, intracerebral haemorrhage and subarachnoid haemorrhage treated in an Australian neurocritical care unit: A prospective cohort study Oxford volume:80 year:2015 day:2 month:12 pages:123-129 extent:7 |
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Functional outcomes at 12 months for patients with traumatic brain injury, intracerebral haemorrhage and subarachnoid haemorrhage treated in an Australian neurocritical care unit: A prospective cohort study |
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Unusual crystallization and melting behavior induced by microphase separation in MPEG-b-PLLA diblock copolymer |
| abstract |
The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. |
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The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. |
| abstract_unstemmed |
The crystallization and melting behaviors of weakly segregated diblock copolymer (MPEG-b-PLLA) have been investigated by differential scanning calorimetry (DSC), wide-angle X-ray diffraction (WAXD), and small-angle X-ray scattering (SAXS). The microphase separation of MPEG-b-PLLA significantly influenced the crystallization behavior of PEG and the melting behavior of PLLA block, which formed during the two-step crystallization process. PLLA block crystallized from melt under various cooling rates (R c, PLLA s) in the first step, and PEG sequentially crystallized in the second process as the temperature cooled from 60 °C to −70 °C at 10 °C/min. With R c, PLLA decreasing, PEG was more excluded out of the interlamellar regions of PLLA crystals, and concentrated into the interfibrillar regions, and formed the different microphase separation formed, which may attribute to the fractional crystallization and homogeneous nucleation. Then the melting peak of PLLA at lower temperature enhanced with the micro-domains of PEG growing, which could be ascribed to that PEG block could accelerate the melting of PLLA near these micro-domains. |
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Unusual crystallization and melting behavior induced by microphase separation in MPEG-b-PLLA diblock copolymer |
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