CO2 hydrogenation to methanol over Cu/ZnO nanocatalysts prepared via a chitosan-assisted co-precipitation method
In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investig...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Witoon, Thongthai [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2013transfer abstract |
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| Umfang: |
7 |
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| Übergeordnetes Werk: |
Enthalten in: Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications - Saini, Hardev S. ELSEVIER, 2015transfer abstract, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:116 ; year:2013 ; pages:72-78 ; extent:7 |
| Links: |
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| DOI / URN: |
10.1016/j.fuproc.2013.04.024 |
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| 520 | |a In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. | ||
| 520 | |a In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. | ||
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| 700 | 1 | |a Jaree, Attasak |4 oth | |
| 700 | 1 | |a Chareonpanich, Metta |4 oth | |
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2013 |
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10.1016/j.fuproc.2013.04.024 doi GBVA2013012000014.pica (DE-627)ELV02728803X (ELSEVIER)S0378-3820(13)00193-8 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Witoon, Thongthai verfasserin aut CO2 hydrogenation to methanol over Cu/ZnO nanocatalysts prepared via a chitosan-assisted co-precipitation method 2013transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. Permsirivanich, Tinnavat oth Donphai, Waleeporn oth Jaree, Attasak oth Chareonpanich, Metta oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:116 year:2013 pages:72-78 extent:7 https://doi.org/10.1016/j.fuproc.2013.04.024 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 116 2013 72-78 7 045F 660 |
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10.1016/j.fuproc.2013.04.024 doi GBVA2013012000014.pica (DE-627)ELV02728803X (ELSEVIER)S0378-3820(13)00193-8 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Witoon, Thongthai verfasserin aut CO2 hydrogenation to methanol over Cu/ZnO nanocatalysts prepared via a chitosan-assisted co-precipitation method 2013transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. Permsirivanich, Tinnavat oth Donphai, Waleeporn oth Jaree, Attasak oth Chareonpanich, Metta oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:116 year:2013 pages:72-78 extent:7 https://doi.org/10.1016/j.fuproc.2013.04.024 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 116 2013 72-78 7 045F 660 |
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10.1016/j.fuproc.2013.04.024 doi GBVA2013012000014.pica (DE-627)ELV02728803X (ELSEVIER)S0378-3820(13)00193-8 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Witoon, Thongthai verfasserin aut CO2 hydrogenation to methanol over Cu/ZnO nanocatalysts prepared via a chitosan-assisted co-precipitation method 2013transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. Permsirivanich, Tinnavat oth Donphai, Waleeporn oth Jaree, Attasak oth Chareonpanich, Metta oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:116 year:2013 pages:72-78 extent:7 https://doi.org/10.1016/j.fuproc.2013.04.024 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 116 2013 72-78 7 045F 660 |
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10.1016/j.fuproc.2013.04.024 doi GBVA2013012000014.pica (DE-627)ELV02728803X (ELSEVIER)S0378-3820(13)00193-8 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Witoon, Thongthai verfasserin aut CO2 hydrogenation to methanol over Cu/ZnO nanocatalysts prepared via a chitosan-assisted co-precipitation method 2013transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. Permsirivanich, Tinnavat oth Donphai, Waleeporn oth Jaree, Attasak oth Chareonpanich, Metta oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:116 year:2013 pages:72-78 extent:7 https://doi.org/10.1016/j.fuproc.2013.04.024 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 116 2013 72-78 7 045F 660 |
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10.1016/j.fuproc.2013.04.024 doi GBVA2013012000014.pica (DE-627)ELV02728803X (ELSEVIER)S0378-3820(13)00193-8 DE-627 ger DE-627 rakwb eng 660 660 DE-600 670 VZ 540 VZ 630 VZ Witoon, Thongthai verfasserin aut CO2 hydrogenation to methanol over Cu/ZnO nanocatalysts prepared via a chitosan-assisted co-precipitation method 2013transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. Permsirivanich, Tinnavat oth Donphai, Waleeporn oth Jaree, Attasak oth Chareonpanich, Metta oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:116 year:2013 pages:72-78 extent:7 https://doi.org/10.1016/j.fuproc.2013.04.024 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 116 2013 72-78 7 045F 660 |
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English |
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Enthalten in Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications New York, NY [u.a.] volume:116 year:2013 pages:72-78 extent:7 |
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Enthalten in Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications New York, NY [u.a.] volume:116 year:2013 pages:72-78 extent:7 |
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Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications |
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Witoon, Thongthai @@aut@@ Permsirivanich, Tinnavat @@oth@@ Donphai, Waleeporn @@oth@@ Jaree, Attasak @@oth@@ Chareonpanich, Metta @@oth@@ |
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co2 hydrogenation to methanol over cu/zno nanocatalysts prepared via a chitosan-assisted co-precipitation method |
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CO2 hydrogenation to methanol over Cu/ZnO nanocatalysts prepared via a chitosan-assisted co-precipitation method |
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In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. |
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In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. |
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In this study, CuO–ZnO nanocomposites were prepared by chitosan-assisted co-precipitation method and performed as catalyst for CO2 hydrogenation to methanol. Effects of chitosan concentration on the physicochemical properties of the nanocomposites as well as the catalytic activity have been investigated. The obtained catalysts were characterized by means of scanning electron microscopy, X-ray diffraction, N2 adsorption–desorption, N2O chemisorption and temperature-programmed reduction. Chitosan was found to act not only as a coordination compound to produce a homogeneous combination of CuO–ZnO nanocomposite, but also as a soft template for the formation of hollow nanospheres. The CuO and ZnO crystallite sizes of the hollow nanospheres were found to be 11.5 and 18.8nm, respectively, which were smaller than those of other catalysts. The increase of chitosan concentration caused a change in catalyst morphology and a reduction in BET surface area as well as metallic copper surface area, but still higher than those of the unmodified catalyst. The catalysts prepared by using chitosan as precipitating agent exhibited a higher space time yield of methanol than the unmodified catalyst, which was attributed to a synergetic effect of the CuO nanoparticle incorporated in the CuO–ZnO nanocatalyst. However, when the reaction temperature was increased up to 533K, a decline in the space time yield of methanol was observed for the catalysts prepared at high chitosan concentration. |
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CO2 hydrogenation to methanol over Cu/ZnO nanocatalysts prepared via a chitosan-assisted co-precipitation method |
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