Evaluation of rheological properties of non-Newtonian fluids in micro rheology compounder: Experimental procedures for a reliable polymer melt viscosity measurement
The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow ch...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Yousfi, Mohamed [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2014transfer abstract |
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| Schlagwörter: |
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| Umfang: |
11 |
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| Übergeordnetes Werk: |
Enthalten in: USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS - Marx, Katherine A. ELSEVIER, 2016, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:40 ; year:2014 ; pages:207-217 ; extent:11 |
| Links: |
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| DOI / URN: |
10.1016/j.polymertesting.2014.09.010 |
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ELV027835685 |
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| 245 | 1 | 0 | |a Evaluation of rheological properties of non-Newtonian fluids in micro rheology compounder: Experimental procedures for a reliable polymer melt viscosity measurement |
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| 520 | |a The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. | ||
| 520 | |a The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. | ||
| 650 | 7 | |a Viscosity |2 Elsevier | |
| 650 | 7 | |a Haake minilab micro rheology compounder |2 Elsevier | |
| 650 | 7 | |a Melt flow rate |2 Elsevier | |
| 650 | 7 | |a Interfacial tension |2 Elsevier | |
| 700 | 1 | |a Alix, Sebastien |4 oth | |
| 700 | 1 | |a Lebeau, Maxime |4 oth | |
| 700 | 1 | |a Soulestin, Jeremie |4 oth | |
| 700 | 1 | |a Lacrampe, Marie-France |4 oth | |
| 700 | 1 | |a Krawczak, Patricia |4 oth | |
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10.1016/j.polymertesting.2014.09.010 doi GBVA2014003000018.pica (DE-627)ELV027835685 (ELSEVIER)S0142-9418(14)00212-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 530 VZ 52.56 bkl Yousfi, Mohamed verfasserin aut Evaluation of rheological properties of non-Newtonian fluids in micro rheology compounder: Experimental procedures for a reliable polymer melt viscosity measurement 2014transfer abstract 11 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. Viscosity Elsevier Haake minilab micro rheology compounder Elsevier Melt flow rate Elsevier Interfacial tension Elsevier Alix, Sebastien oth Lebeau, Maxime oth Soulestin, Jeremie oth Lacrampe, Marie-France oth Krawczak, Patricia oth Enthalten in Elsevier Science Marx, Katherine A. ELSEVIER USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS 2016 Amsterdam [u.a.] (DE-627)ELV013776983 volume:40 year:2014 pages:207-217 extent:11 https://doi.org/10.1016/j.polymertesting.2014.09.010 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 40 2014 207-217 11 045F 540 |
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10.1016/j.polymertesting.2014.09.010 doi GBVA2014003000018.pica (DE-627)ELV027835685 (ELSEVIER)S0142-9418(14)00212-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 530 VZ 52.56 bkl Yousfi, Mohamed verfasserin aut Evaluation of rheological properties of non-Newtonian fluids in micro rheology compounder: Experimental procedures for a reliable polymer melt viscosity measurement 2014transfer abstract 11 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. Viscosity Elsevier Haake minilab micro rheology compounder Elsevier Melt flow rate Elsevier Interfacial tension Elsevier Alix, Sebastien oth Lebeau, Maxime oth Soulestin, Jeremie oth Lacrampe, Marie-France oth Krawczak, Patricia oth Enthalten in Elsevier Science Marx, Katherine A. ELSEVIER USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS 2016 Amsterdam [u.a.] (DE-627)ELV013776983 volume:40 year:2014 pages:207-217 extent:11 https://doi.org/10.1016/j.polymertesting.2014.09.010 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 40 2014 207-217 11 045F 540 |
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10.1016/j.polymertesting.2014.09.010 doi GBVA2014003000018.pica (DE-627)ELV027835685 (ELSEVIER)S0142-9418(14)00212-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 530 VZ 52.56 bkl Yousfi, Mohamed verfasserin aut Evaluation of rheological properties of non-Newtonian fluids in micro rheology compounder: Experimental procedures for a reliable polymer melt viscosity measurement 2014transfer abstract 11 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. Viscosity Elsevier Haake minilab micro rheology compounder Elsevier Melt flow rate Elsevier Interfacial tension Elsevier Alix, Sebastien oth Lebeau, Maxime oth Soulestin, Jeremie oth Lacrampe, Marie-France oth Krawczak, Patricia oth Enthalten in Elsevier Science Marx, Katherine A. ELSEVIER USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS 2016 Amsterdam [u.a.] (DE-627)ELV013776983 volume:40 year:2014 pages:207-217 extent:11 https://doi.org/10.1016/j.polymertesting.2014.09.010 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 40 2014 207-217 11 045F 540 |
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10.1016/j.polymertesting.2014.09.010 doi GBVA2014003000018.pica (DE-627)ELV027835685 (ELSEVIER)S0142-9418(14)00212-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 530 VZ 52.56 bkl Yousfi, Mohamed verfasserin aut Evaluation of rheological properties of non-Newtonian fluids in micro rheology compounder: Experimental procedures for a reliable polymer melt viscosity measurement 2014transfer abstract 11 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. Viscosity Elsevier Haake minilab micro rheology compounder Elsevier Melt flow rate Elsevier Interfacial tension Elsevier Alix, Sebastien oth Lebeau, Maxime oth Soulestin, Jeremie oth Lacrampe, Marie-France oth Krawczak, Patricia oth Enthalten in Elsevier Science Marx, Katherine A. ELSEVIER USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS 2016 Amsterdam [u.a.] (DE-627)ELV013776983 volume:40 year:2014 pages:207-217 extent:11 https://doi.org/10.1016/j.polymertesting.2014.09.010 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 40 2014 207-217 11 045F 540 |
| allfieldsSound |
10.1016/j.polymertesting.2014.09.010 doi GBVA2014003000018.pica (DE-627)ELV027835685 (ELSEVIER)S0142-9418(14)00212-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 530 VZ 52.56 bkl Yousfi, Mohamed verfasserin aut Evaluation of rheological properties of non-Newtonian fluids in micro rheology compounder: Experimental procedures for a reliable polymer melt viscosity measurement 2014transfer abstract 11 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. Viscosity Elsevier Haake minilab micro rheology compounder Elsevier Melt flow rate Elsevier Interfacial tension Elsevier Alix, Sebastien oth Lebeau, Maxime oth Soulestin, Jeremie oth Lacrampe, Marie-France oth Krawczak, Patricia oth Enthalten in Elsevier Science Marx, Katherine A. ELSEVIER USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS 2016 Amsterdam [u.a.] (DE-627)ELV013776983 volume:40 year:2014 pages:207-217 extent:11 https://doi.org/10.1016/j.polymertesting.2014.09.010 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 40 2014 207-217 11 045F 540 |
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Enthalten in USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS Amsterdam [u.a.] volume:40 year:2014 pages:207-217 extent:11 |
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Enthalten in USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS Amsterdam [u.a.] volume:40 year:2014 pages:207-217 extent:11 |
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USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS |
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Evaluation of rheological properties of non-Newtonian fluids in micro rheology compounder: Experimental procedures for a reliable polymer melt viscosity measurement |
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USE OF NOVEL OBSERVATIONAL METHODOLOGY FOR MEASURING AFFECT AND BEHAVIORS IN A BEHAVIORAL INTERVENTION FOR PERSONS WITH DEMENTIA HOSPITALIZED FOR BEHAVIORAL SYMPTOMS |
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evaluation of rheological properties of non-newtonian fluids in micro rheology compounder: experimental procedures for a reliable polymer melt viscosity measurement |
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Evaluation of rheological properties of non-Newtonian fluids in micro rheology compounder: Experimental procedures for a reliable polymer melt viscosity measurement |
| abstract |
The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. |
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The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. |
| abstract_unstemmed |
The aim of this report is to develop an experimental method which provides relevant data about the rheological behaviour of polymer melts using a Haake minilab microcompounder. A slit capillary die integrated in the recirculation channel of the microcompounder allows determination of polymer flow characteristics using two pressure transducers specially designed for this purpose. According to a specific methodology detailed in the present paper, the effective flow rate and the corresponding apparent shear rate were carefully investigated as regards the repeatability of the data. The viscosity of different commercial polymeric materials (polyolefins and polyamide 6) exhibiting different melt flow rate properties was then calculated based on the Hagen-Poiseuille theory. The results show that the melt flow data obtained from the micro-rheology compounder overlap very well with the shear data obtained using oscillatory or rod capillary rheometers according to the Cox-Merz rule. Finally, a possible application of viscosity measurements of the developed method is given. Using the morphological analysis of a PP/PA6 (80/20 w/w) sample as a polymeric blend model, a deduction of an interfacial tension factor was highlighted and a pertinent value corresponding to that found in the literature was assessed. |
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