Effect of preparation method on the performance of Pd-MnO x /γ-Al2O3 monolithic catalysts for ground-level O3 decomposition
MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coate...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Ren, Chengjun [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2014transfer abstract |
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8 |
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| Übergeordnetes Werk: |
Enthalten in: SP-0433: Imaging biobanks: challenges and opportunities - Van der Lugt, A. ELSEVIER, 2017, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:35 ; year:2014 ; number:11 ; pages:1883-1890 ; extent:8 |
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| DOI / URN: |
10.1016/S1872-2067(14)60176-5 |
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ELV028056604 |
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| 245 | 1 | 0 | |a Effect of preparation method on the performance of Pd-MnO x /γ-Al2O3 monolithic catalysts for ground-level O3 decomposition |
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| 520 | |a MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. | ||
| 520 | |a MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. | ||
| 650 | 7 | |a Ozone |2 Elsevier | |
| 650 | 7 | |a Preparation method |2 Elsevier | |
| 650 | 7 | |a Palladium |2 Elsevier | |
| 650 | 7 | |a Manganese oxide |2 Elsevier | |
| 650 | 7 | |a Catalytic decomposition |2 Elsevier | |
| 700 | 1 | |a Zhou, Lina |4 oth | |
| 700 | 1 | |a Shang, Hongyan |4 oth | |
| 700 | 1 | |a Chen, Yaoqiang |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier |a Van der Lugt, A. ELSEVIER |t SP-0433: Imaging biobanks: challenges and opportunities |d 2017 |g Amsterdam [u.a.] |w (DE-627)ELV01487606X |
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10.1016/S1872-2067(14)60176-5 doi GBVA2014009000015.pica (DE-627)ELV028056604 (ELSEVIER)S1872-2067(14)60176-5 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 570 540 VZ Ren, Chengjun verfasserin aut Effect of preparation method on the performance of Pd-MnO x /γ-Al2O3 monolithic catalysts for ground-level O3 decomposition 2014transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. Ozone Elsevier Preparation method Elsevier Palladium Elsevier Manganese oxide Elsevier Catalytic decomposition Elsevier Zhou, Lina oth Shang, Hongyan oth Chen, Yaoqiang oth Enthalten in Elsevier Van der Lugt, A. ELSEVIER SP-0433: Imaging biobanks: challenges and opportunities 2017 Amsterdam [u.a.] (DE-627)ELV01487606X volume:35 year:2014 number:11 pages:1883-1890 extent:8 https://doi.org/10.1016/S1872-2067(14)60176-5 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_40 AR 35 2014 11 1883-1890 8 045F 540 |
| spelling |
10.1016/S1872-2067(14)60176-5 doi GBVA2014009000015.pica (DE-627)ELV028056604 (ELSEVIER)S1872-2067(14)60176-5 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 570 540 VZ Ren, Chengjun verfasserin aut Effect of preparation method on the performance of Pd-MnO x /γ-Al2O3 monolithic catalysts for ground-level O3 decomposition 2014transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. Ozone Elsevier Preparation method Elsevier Palladium Elsevier Manganese oxide Elsevier Catalytic decomposition Elsevier Zhou, Lina oth Shang, Hongyan oth Chen, Yaoqiang oth Enthalten in Elsevier Van der Lugt, A. ELSEVIER SP-0433: Imaging biobanks: challenges and opportunities 2017 Amsterdam [u.a.] (DE-627)ELV01487606X volume:35 year:2014 number:11 pages:1883-1890 extent:8 https://doi.org/10.1016/S1872-2067(14)60176-5 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_40 AR 35 2014 11 1883-1890 8 045F 540 |
| allfields_unstemmed |
10.1016/S1872-2067(14)60176-5 doi GBVA2014009000015.pica (DE-627)ELV028056604 (ELSEVIER)S1872-2067(14)60176-5 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 570 540 VZ Ren, Chengjun verfasserin aut Effect of preparation method on the performance of Pd-MnO x /γ-Al2O3 monolithic catalysts for ground-level O3 decomposition 2014transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. Ozone Elsevier Preparation method Elsevier Palladium Elsevier Manganese oxide Elsevier Catalytic decomposition Elsevier Zhou, Lina oth Shang, Hongyan oth Chen, Yaoqiang oth Enthalten in Elsevier Van der Lugt, A. ELSEVIER SP-0433: Imaging biobanks: challenges and opportunities 2017 Amsterdam [u.a.] (DE-627)ELV01487606X volume:35 year:2014 number:11 pages:1883-1890 extent:8 https://doi.org/10.1016/S1872-2067(14)60176-5 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_40 AR 35 2014 11 1883-1890 8 045F 540 |
| allfieldsGer |
10.1016/S1872-2067(14)60176-5 doi GBVA2014009000015.pica (DE-627)ELV028056604 (ELSEVIER)S1872-2067(14)60176-5 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 570 540 VZ Ren, Chengjun verfasserin aut Effect of preparation method on the performance of Pd-MnO x /γ-Al2O3 monolithic catalysts for ground-level O3 decomposition 2014transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. Ozone Elsevier Preparation method Elsevier Palladium Elsevier Manganese oxide Elsevier Catalytic decomposition Elsevier Zhou, Lina oth Shang, Hongyan oth Chen, Yaoqiang oth Enthalten in Elsevier Van der Lugt, A. ELSEVIER SP-0433: Imaging biobanks: challenges and opportunities 2017 Amsterdam [u.a.] (DE-627)ELV01487606X volume:35 year:2014 number:11 pages:1883-1890 extent:8 https://doi.org/10.1016/S1872-2067(14)60176-5 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_40 AR 35 2014 11 1883-1890 8 045F 540 |
| allfieldsSound |
10.1016/S1872-2067(14)60176-5 doi GBVA2014009000015.pica (DE-627)ELV028056604 (ELSEVIER)S1872-2067(14)60176-5 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 570 540 VZ Ren, Chengjun verfasserin aut Effect of preparation method on the performance of Pd-MnO x /γ-Al2O3 monolithic catalysts for ground-level O3 decomposition 2014transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. Ozone Elsevier Preparation method Elsevier Palladium Elsevier Manganese oxide Elsevier Catalytic decomposition Elsevier Zhou, Lina oth Shang, Hongyan oth Chen, Yaoqiang oth Enthalten in Elsevier Van der Lugt, A. ELSEVIER SP-0433: Imaging biobanks: challenges and opportunities 2017 Amsterdam [u.a.] (DE-627)ELV01487606X volume:35 year:2014 number:11 pages:1883-1890 extent:8 https://doi.org/10.1016/S1872-2067(14)60176-5 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_40 AR 35 2014 11 1883-1890 8 045F 540 |
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Enthalten in SP-0433: Imaging biobanks: challenges and opportunities Amsterdam [u.a.] volume:35 year:2014 number:11 pages:1883-1890 extent:8 |
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effect of preparation method on the performance of pd-mno x /γ-al2o3 monolithic catalysts for ground-level o3 decomposition |
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Effect of preparation method on the performance of Pd-MnO x /γ-Al2O3 monolithic catalysts for ground-level O3 decomposition |
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MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. |
| abstractGer |
MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. |
| abstract_unstemmed |
MnO x +γ-Al2O3 and MnO x /γ-Al2O3 catalysts were prepared by the sol-gel and sequential precipitation methods, respectively. The same amount of Pd was loaded on these catalysts by incipient wetness impregnation. The two Pd-MnO x /γ-Al2O3 catalysts with different physicochemical properties were coated on cordierite. The catalysts were characterized by X-ray diffraction, X-ray photoelectron spectroscopy, H2 temperature-programmed reduction, and N2 adsorption-desorption measurement. The preparation method and calcination temperature of MnO x have significant impact on the crystalline phase of MnO x , MnO x species and active oxygen species, and textural properties of the catalysts. The experimental results showed that 0.60 μL·L−1 of ozone was completely decomposed on these catalysts in the temperature range of 16 to 90°C at space velocities from 380000 to 580000 h−1. In particular, the activity for O3 decomposition was excellent on the Pd/MnO x +Pd/γ-Al2O3 catalyst that used MnO x prepared by the sol-gel method. Mn n+ is beneficial for O3 decomposition, and Mn2+, Mn3+, and Mn4+ were presented in a mole ratio of 1.7:1:3 on the surface of the catalyst. |
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Effect of preparation method on the performance of Pd-MnO x /γ-Al2O3 monolithic catalysts for ground-level O3 decomposition |
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