Synthesis and characterisation of new PCsp3P-supported nickel complexes
The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the s...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Jonasson, Klara J. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2014 |
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4 |
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| Übergeordnetes Werk: |
Enthalten in: The Effect of Simultaneous Renal Replacement Therapy on Extracorporeal Membrane Oxygenation Support for Postcardiotomy Patients with Cardiogenic Shock: A Pilot Randomized Controlled Trial - Li, Chenglong ELSEVIER, 2019, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:759 ; year:2014 ; day:1 ; month:06 ; pages:15-18 ; extent:4 |
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| DOI / URN: |
10.1016/j.jorganchem.2014.02.013 |
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| 520 | |a The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the solid state structures were determined by X-ray diffraction showing an unusually long Ni–Br bond in the bromo complex. A preliminary account of their reactivity is reported and they were found to be unreactive towards base and hydride sources and to be poor catalysts in Kumada coupling reactions. | ||
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10.1016/j.jorganchem.2014.02.013 doi GBVA2014022000004.pica (DE-627)ELV028505506 (ELSEVIER)S0022-328X(14)00092-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.85 bkl 44.66 bkl Jonasson, Klara J. verfasserin aut Synthesis and characterisation of new PCsp3P-supported nickel complexes 2014 4 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the solid state structures were determined by X-ray diffraction showing an unusually long Ni–Br bond in the bromo complex. A preliminary account of their reactivity is reported and they were found to be unreactive towards base and hydride sources and to be poor catalysts in Kumada coupling reactions. Cyclometalation Elsevier Coordination Elsevier Aliphatic pincer complexes Elsevier Nickel Elsevier PCP pincer ligands Elsevier Wendt, Ola F. oth Enthalten in Elsevier Li, Chenglong ELSEVIER The Effect of Simultaneous Renal Replacement Therapy on Extracorporeal Membrane Oxygenation Support for Postcardiotomy Patients with Cardiogenic Shock: A Pilot Randomized Controlled Trial 2019 New York, NY [u.a.] (DE-627)ELV002971518 volume:759 year:2014 day:1 month:06 pages:15-18 extent:4 https://doi.org/10.1016/j.jorganchem.2014.02.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.85 Kardiologie Angiologie VZ 44.66 Anästhesiologie VZ AR 759 2014 1 0601 15-18 4 045F 540 |
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10.1016/j.jorganchem.2014.02.013 doi GBVA2014022000004.pica (DE-627)ELV028505506 (ELSEVIER)S0022-328X(14)00092-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.85 bkl 44.66 bkl Jonasson, Klara J. verfasserin aut Synthesis and characterisation of new PCsp3P-supported nickel complexes 2014 4 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the solid state structures were determined by X-ray diffraction showing an unusually long Ni–Br bond in the bromo complex. A preliminary account of their reactivity is reported and they were found to be unreactive towards base and hydride sources and to be poor catalysts in Kumada coupling reactions. Cyclometalation Elsevier Coordination Elsevier Aliphatic pincer complexes Elsevier Nickel Elsevier PCP pincer ligands Elsevier Wendt, Ola F. oth Enthalten in Elsevier Li, Chenglong ELSEVIER The Effect of Simultaneous Renal Replacement Therapy on Extracorporeal Membrane Oxygenation Support for Postcardiotomy Patients with Cardiogenic Shock: A Pilot Randomized Controlled Trial 2019 New York, NY [u.a.] (DE-627)ELV002971518 volume:759 year:2014 day:1 month:06 pages:15-18 extent:4 https://doi.org/10.1016/j.jorganchem.2014.02.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.85 Kardiologie Angiologie VZ 44.66 Anästhesiologie VZ AR 759 2014 1 0601 15-18 4 045F 540 |
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10.1016/j.jorganchem.2014.02.013 doi GBVA2014022000004.pica (DE-627)ELV028505506 (ELSEVIER)S0022-328X(14)00092-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.85 bkl 44.66 bkl Jonasson, Klara J. verfasserin aut Synthesis and characterisation of new PCsp3P-supported nickel complexes 2014 4 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the solid state structures were determined by X-ray diffraction showing an unusually long Ni–Br bond in the bromo complex. A preliminary account of their reactivity is reported and they were found to be unreactive towards base and hydride sources and to be poor catalysts in Kumada coupling reactions. Cyclometalation Elsevier Coordination Elsevier Aliphatic pincer complexes Elsevier Nickel Elsevier PCP pincer ligands Elsevier Wendt, Ola F. oth Enthalten in Elsevier Li, Chenglong ELSEVIER The Effect of Simultaneous Renal Replacement Therapy on Extracorporeal Membrane Oxygenation Support for Postcardiotomy Patients with Cardiogenic Shock: A Pilot Randomized Controlled Trial 2019 New York, NY [u.a.] (DE-627)ELV002971518 volume:759 year:2014 day:1 month:06 pages:15-18 extent:4 https://doi.org/10.1016/j.jorganchem.2014.02.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.85 Kardiologie Angiologie VZ 44.66 Anästhesiologie VZ AR 759 2014 1 0601 15-18 4 045F 540 |
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10.1016/j.jorganchem.2014.02.013 doi GBVA2014022000004.pica (DE-627)ELV028505506 (ELSEVIER)S0022-328X(14)00092-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.85 bkl 44.66 bkl Jonasson, Klara J. verfasserin aut Synthesis and characterisation of new PCsp3P-supported nickel complexes 2014 4 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the solid state structures were determined by X-ray diffraction showing an unusually long Ni–Br bond in the bromo complex. A preliminary account of their reactivity is reported and they were found to be unreactive towards base and hydride sources and to be poor catalysts in Kumada coupling reactions. Cyclometalation Elsevier Coordination Elsevier Aliphatic pincer complexes Elsevier Nickel Elsevier PCP pincer ligands Elsevier Wendt, Ola F. oth Enthalten in Elsevier Li, Chenglong ELSEVIER The Effect of Simultaneous Renal Replacement Therapy on Extracorporeal Membrane Oxygenation Support for Postcardiotomy Patients with Cardiogenic Shock: A Pilot Randomized Controlled Trial 2019 New York, NY [u.a.] (DE-627)ELV002971518 volume:759 year:2014 day:1 month:06 pages:15-18 extent:4 https://doi.org/10.1016/j.jorganchem.2014.02.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.85 Kardiologie Angiologie VZ 44.66 Anästhesiologie VZ AR 759 2014 1 0601 15-18 4 045F 540 |
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10.1016/j.jorganchem.2014.02.013 doi GBVA2014022000004.pica (DE-627)ELV028505506 (ELSEVIER)S0022-328X(14)00092-8 DE-627 ger DE-627 rakwb eng 540 540 DE-600 610 VZ 44.85 bkl 44.66 bkl Jonasson, Klara J. verfasserin aut Synthesis and characterisation of new PCsp3P-supported nickel complexes 2014 4 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the solid state structures were determined by X-ray diffraction showing an unusually long Ni–Br bond in the bromo complex. A preliminary account of their reactivity is reported and they were found to be unreactive towards base and hydride sources and to be poor catalysts in Kumada coupling reactions. Cyclometalation Elsevier Coordination Elsevier Aliphatic pincer complexes Elsevier Nickel Elsevier PCP pincer ligands Elsevier Wendt, Ola F. oth Enthalten in Elsevier Li, Chenglong ELSEVIER The Effect of Simultaneous Renal Replacement Therapy on Extracorporeal Membrane Oxygenation Support for Postcardiotomy Patients with Cardiogenic Shock: A Pilot Randomized Controlled Trial 2019 New York, NY [u.a.] (DE-627)ELV002971518 volume:759 year:2014 day:1 month:06 pages:15-18 extent:4 https://doi.org/10.1016/j.jorganchem.2014.02.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.85 Kardiologie Angiologie VZ 44.66 Anästhesiologie VZ AR 759 2014 1 0601 15-18 4 045F 540 |
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synthesis and characterisation of new pcsp3p-supported nickel complexes |
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Synthesis and characterisation of new PCsp3P-supported nickel complexes |
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The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the solid state structures were determined by X-ray diffraction showing an unusually long Ni–Br bond in the bromo complex. A preliminary account of their reactivity is reported and they were found to be unreactive towards base and hydride sources and to be poor catalysts in Kumada coupling reactions. |
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The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the solid state structures were determined by X-ray diffraction showing an unusually long Ni–Br bond in the bromo complex. A preliminary account of their reactivity is reported and they were found to be unreactive towards base and hydride sources and to be poor catalysts in Kumada coupling reactions. |
| abstract_unstemmed |
The coordination behaviour of the aliphatic pincer ligand cis-1,3-bis-((di-tert-butylphosphino)methyl)cyclohexane with NiCl2 and NiBr2 was studied. Reflux in toluene afforded cyclometalated, tridentate PCsp3P pincer complexes, that were characterised by elemental analysis and NMR spectroscopy; the solid state structures were determined by X-ray diffraction showing an unusually long Ni–Br bond in the bromo complex. A preliminary account of their reactivity is reported and they were found to be unreactive towards base and hydride sources and to be poor catalysts in Kumada coupling reactions. |
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| title_short |
Synthesis and characterisation of new PCsp3P-supported nickel complexes |
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https://doi.org/10.1016/j.jorganchem.2014.02.013 |
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Wendt, Ola F. |
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10.1016/j.jorganchem.2014.02.013 |
| up_date |
2024-07-06T18:59:27.648Z |
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