Investigation of the Ionic conductivity and dielectric measurements of poly (N-vinyl pyrrolidone)-sulfamic acid polymer complexes
Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy...
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| Autor*in: |
Daries Bella, R.S. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2015transfer abstract |
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| Schlagwörter: |
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| Umfang: |
7 |
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| Übergeordnetes Werk: |
Enthalten in: Towards circular plastics: Density and MFR prediction of PE with IR spectroscopic techniques - Bredács, M. ELSEVIER, 2023, Amsterdam |
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| Übergeordnetes Werk: |
volume:458 ; year:2015 ; day:1 ; month:02 ; pages:51-57 ; extent:7 |
| Links: |
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| DOI / URN: |
10.1016/j.physb.2014.11.005 |
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| 520 | |a Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. | ||
| 520 | |a Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. | ||
| 650 | 7 | |a Poly (N-vinyl pyrrolidone) |2 Elsevier | |
| 650 | 7 | |a Differential scanning calorimetry |2 Elsevier | |
| 650 | 7 | |a Proton conductor |2 Elsevier | |
| 650 | 7 | |a Ionic conductivity |2 Elsevier | |
| 650 | 7 | |a Zwitterion |2 Elsevier | |
| 650 | 7 | |a Sulfamic acid |2 Elsevier | |
| 700 | 1 | |a Karthickprabhu, S. |4 oth | |
| 700 | 1 | |a Maheswaran, A. |4 oth | |
| 700 | 1 | |a Amibika, C. |4 oth | |
| 700 | 1 | |a Hirankumar, G. |4 oth | |
| 700 | 1 | |a Devaraj, Premanand |4 oth | |
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10.1016/j.physb.2014.11.005 doi GBVA2015015000022.pica (DE-627)ELV029107741 (ELSEVIER)S0921-4526(14)00830-8 DE-627 ger DE-627 rakwb eng 530 530 DE-600 540 VZ 51.30 bkl Daries Bella, R.S. verfasserin aut Investigation of the Ionic conductivity and dielectric measurements of poly (N-vinyl pyrrolidone)-sulfamic acid polymer complexes 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Poly (N-vinyl pyrrolidone) Elsevier Differential scanning calorimetry Elsevier Proton conductor Elsevier Ionic conductivity Elsevier Zwitterion Elsevier Sulfamic acid Elsevier Karthickprabhu, S. oth Maheswaran, A. oth Amibika, C. oth Hirankumar, G. oth Devaraj, Premanand oth Enthalten in Elsevier Bredács, M. ELSEVIER Towards circular plastics: Density and MFR prediction of PE with IR spectroscopic techniques 2023 Amsterdam (DE-627)ELV010517057 volume:458 year:2015 day:1 month:02 pages:51-57 extent:7 https://doi.org/10.1016/j.physb.2014.11.005 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_203 GBV_ILN_227 GBV_ILN_2010 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 458 2015 1 0201 51-57 7 045F 530 |
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10.1016/j.physb.2014.11.005 doi GBVA2015015000022.pica (DE-627)ELV029107741 (ELSEVIER)S0921-4526(14)00830-8 DE-627 ger DE-627 rakwb eng 530 530 DE-600 540 VZ 51.30 bkl Daries Bella, R.S. verfasserin aut Investigation of the Ionic conductivity and dielectric measurements of poly (N-vinyl pyrrolidone)-sulfamic acid polymer complexes 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Poly (N-vinyl pyrrolidone) Elsevier Differential scanning calorimetry Elsevier Proton conductor Elsevier Ionic conductivity Elsevier Zwitterion Elsevier Sulfamic acid Elsevier Karthickprabhu, S. oth Maheswaran, A. oth Amibika, C. oth Hirankumar, G. oth Devaraj, Premanand oth Enthalten in Elsevier Bredács, M. ELSEVIER Towards circular plastics: Density and MFR prediction of PE with IR spectroscopic techniques 2023 Amsterdam (DE-627)ELV010517057 volume:458 year:2015 day:1 month:02 pages:51-57 extent:7 https://doi.org/10.1016/j.physb.2014.11.005 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_203 GBV_ILN_227 GBV_ILN_2010 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 458 2015 1 0201 51-57 7 045F 530 |
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10.1016/j.physb.2014.11.005 doi GBVA2015015000022.pica (DE-627)ELV029107741 (ELSEVIER)S0921-4526(14)00830-8 DE-627 ger DE-627 rakwb eng 530 530 DE-600 540 VZ 51.30 bkl Daries Bella, R.S. verfasserin aut Investigation of the Ionic conductivity and dielectric measurements of poly (N-vinyl pyrrolidone)-sulfamic acid polymer complexes 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Poly (N-vinyl pyrrolidone) Elsevier Differential scanning calorimetry Elsevier Proton conductor Elsevier Ionic conductivity Elsevier Zwitterion Elsevier Sulfamic acid Elsevier Karthickprabhu, S. oth Maheswaran, A. oth Amibika, C. oth Hirankumar, G. oth Devaraj, Premanand oth Enthalten in Elsevier Bredács, M. ELSEVIER Towards circular plastics: Density and MFR prediction of PE with IR spectroscopic techniques 2023 Amsterdam (DE-627)ELV010517057 volume:458 year:2015 day:1 month:02 pages:51-57 extent:7 https://doi.org/10.1016/j.physb.2014.11.005 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_203 GBV_ILN_227 GBV_ILN_2010 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 458 2015 1 0201 51-57 7 045F 530 |
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10.1016/j.physb.2014.11.005 doi GBVA2015015000022.pica (DE-627)ELV029107741 (ELSEVIER)S0921-4526(14)00830-8 DE-627 ger DE-627 rakwb eng 530 530 DE-600 540 VZ 51.30 bkl Daries Bella, R.S. verfasserin aut Investigation of the Ionic conductivity and dielectric measurements of poly (N-vinyl pyrrolidone)-sulfamic acid polymer complexes 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Poly (N-vinyl pyrrolidone) Elsevier Differential scanning calorimetry Elsevier Proton conductor Elsevier Ionic conductivity Elsevier Zwitterion Elsevier Sulfamic acid Elsevier Karthickprabhu, S. oth Maheswaran, A. oth Amibika, C. oth Hirankumar, G. oth Devaraj, Premanand oth Enthalten in Elsevier Bredács, M. ELSEVIER Towards circular plastics: Density and MFR prediction of PE with IR spectroscopic techniques 2023 Amsterdam (DE-627)ELV010517057 volume:458 year:2015 day:1 month:02 pages:51-57 extent:7 https://doi.org/10.1016/j.physb.2014.11.005 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_203 GBV_ILN_227 GBV_ILN_2010 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 458 2015 1 0201 51-57 7 045F 530 |
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10.1016/j.physb.2014.11.005 doi GBVA2015015000022.pica (DE-627)ELV029107741 (ELSEVIER)S0921-4526(14)00830-8 DE-627 ger DE-627 rakwb eng 530 530 DE-600 540 VZ 51.30 bkl Daries Bella, R.S. verfasserin aut Investigation of the Ionic conductivity and dielectric measurements of poly (N-vinyl pyrrolidone)-sulfamic acid polymer complexes 2015transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. Poly (N-vinyl pyrrolidone) Elsevier Differential scanning calorimetry Elsevier Proton conductor Elsevier Ionic conductivity Elsevier Zwitterion Elsevier Sulfamic acid Elsevier Karthickprabhu, S. oth Maheswaran, A. oth Amibika, C. oth Hirankumar, G. oth Devaraj, Premanand oth Enthalten in Elsevier Bredács, M. ELSEVIER Towards circular plastics: Density and MFR prediction of PE with IR spectroscopic techniques 2023 Amsterdam (DE-627)ELV010517057 volume:458 year:2015 day:1 month:02 pages:51-57 extent:7 https://doi.org/10.1016/j.physb.2014.11.005 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_203 GBV_ILN_227 GBV_ILN_2010 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 458 2015 1 0201 51-57 7 045F 530 |
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investigation of the ionic conductivity and dielectric measurements of poly (n-vinyl pyrrolidone)-sulfamic acid polymer complexes |
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Investigation of the Ionic conductivity and dielectric measurements of poly (N-vinyl pyrrolidone)-sulfamic acid polymer complexes |
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Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. |
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Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. |
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Polymer electrolyte complexes of poly (N-vinyl pyrrolidone) (PVP)-sulfamic acid (NH2SO3H) were prepared by a familiar solution casting method with different molar concentrations of PVP and sulfamic acid. The interaction between PVP and NH2SO3H was confirmed by Fourier transform infrared spectroscopy analysis. Laser microscopy analysis was used to study the surface morphology of the polymer complexes. The glass transition temperature (T g) and the melting temperature (T m) of polymer complexes were computed from Differential scanning calorimetric studies. AC impedance spectroscopic measurements revealed that the polymer complex, 97mol% PVP-3mol% NH2SO3H shows higher ionic conductivity with two different activation energies above and below the glass transition temperature (T g). Dielectric studies confirmed that the dc conduction mechanism has dominated in the polymer complexes. The value of power law exponent (n) confirmed the translational motion of ions from one site to another vacant site in these complexes. |
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Investigation of the Ionic conductivity and dielectric measurements of poly (N-vinyl pyrrolidone)-sulfamic acid polymer complexes |
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