The direct determination of HgS by thermal desorption coupled with atomic absorption spectrometry
This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as wel...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Coufalík, Pavel [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2016transfer abstract |
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| Umfang: |
5 |
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| Übergeordnetes Werk: |
Enthalten in: Dual stimuli-responsive polypeptide-calcium phosphate hybrid nanoparticles for co-delivery of multiple drugs in cancer therapy - Li, Qiang ELSEVIER, 2021, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:118 ; year:2016 ; day:1 ; month:04 ; pages:1-5 ; extent:5 |
| Links: |
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| DOI / URN: |
10.1016/j.sab.2016.01.004 |
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| 520 | |a This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. | ||
| 520 | |a This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. | ||
| 700 | 1 | |a Zvěřina, Ondřej |4 oth | |
| 700 | 1 | |a Komárek, Josef |4 oth | |
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10.1016/j.sab.2016.01.004 doi GBV00000000000207A.pica (DE-627)ELV029817226 (ELSEVIER)S0584-8547(16)00013-6 DE-627 ger DE-627 rakwb eng 540 530 540 DE-600 530 DE-600 540 VZ 42.15 bkl Coufalík, Pavel verfasserin aut The direct determination of HgS by thermal desorption coupled with atomic absorption spectrometry 2016transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. Zvěřina, Ondřej oth Komárek, Josef oth Enthalten in Elsevier Li, Qiang ELSEVIER Dual stimuli-responsive polypeptide-calcium phosphate hybrid nanoparticles for co-delivery of multiple drugs in cancer therapy 2021 Amsterdam [u.a.] (DE-627)ELV005740053 volume:118 year:2016 day:1 month:04 pages:1-5 extent:5 https://doi.org/10.1016/j.sab.2016.01.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 42.15 Zellbiologie VZ AR 118 2016 1 0401 1-5 5 045F 540 |
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10.1016/j.sab.2016.01.004 doi GBV00000000000207A.pica (DE-627)ELV029817226 (ELSEVIER)S0584-8547(16)00013-6 DE-627 ger DE-627 rakwb eng 540 530 540 DE-600 530 DE-600 540 VZ 42.15 bkl Coufalík, Pavel verfasserin aut The direct determination of HgS by thermal desorption coupled with atomic absorption spectrometry 2016transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. Zvěřina, Ondřej oth Komárek, Josef oth Enthalten in Elsevier Li, Qiang ELSEVIER Dual stimuli-responsive polypeptide-calcium phosphate hybrid nanoparticles for co-delivery of multiple drugs in cancer therapy 2021 Amsterdam [u.a.] (DE-627)ELV005740053 volume:118 year:2016 day:1 month:04 pages:1-5 extent:5 https://doi.org/10.1016/j.sab.2016.01.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 42.15 Zellbiologie VZ AR 118 2016 1 0401 1-5 5 045F 540 |
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10.1016/j.sab.2016.01.004 doi GBV00000000000207A.pica (DE-627)ELV029817226 (ELSEVIER)S0584-8547(16)00013-6 DE-627 ger DE-627 rakwb eng 540 530 540 DE-600 530 DE-600 540 VZ 42.15 bkl Coufalík, Pavel verfasserin aut The direct determination of HgS by thermal desorption coupled with atomic absorption spectrometry 2016transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. Zvěřina, Ondřej oth Komárek, Josef oth Enthalten in Elsevier Li, Qiang ELSEVIER Dual stimuli-responsive polypeptide-calcium phosphate hybrid nanoparticles for co-delivery of multiple drugs in cancer therapy 2021 Amsterdam [u.a.] (DE-627)ELV005740053 volume:118 year:2016 day:1 month:04 pages:1-5 extent:5 https://doi.org/10.1016/j.sab.2016.01.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 42.15 Zellbiologie VZ AR 118 2016 1 0401 1-5 5 045F 540 |
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10.1016/j.sab.2016.01.004 doi GBV00000000000207A.pica (DE-627)ELV029817226 (ELSEVIER)S0584-8547(16)00013-6 DE-627 ger DE-627 rakwb eng 540 530 540 DE-600 530 DE-600 540 VZ 42.15 bkl Coufalík, Pavel verfasserin aut The direct determination of HgS by thermal desorption coupled with atomic absorption spectrometry 2016transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. Zvěřina, Ondřej oth Komárek, Josef oth Enthalten in Elsevier Li, Qiang ELSEVIER Dual stimuli-responsive polypeptide-calcium phosphate hybrid nanoparticles for co-delivery of multiple drugs in cancer therapy 2021 Amsterdam [u.a.] (DE-627)ELV005740053 volume:118 year:2016 day:1 month:04 pages:1-5 extent:5 https://doi.org/10.1016/j.sab.2016.01.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 42.15 Zellbiologie VZ AR 118 2016 1 0401 1-5 5 045F 540 |
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10.1016/j.sab.2016.01.004 doi GBV00000000000207A.pica (DE-627)ELV029817226 (ELSEVIER)S0584-8547(16)00013-6 DE-627 ger DE-627 rakwb eng 540 530 540 DE-600 530 DE-600 540 VZ 42.15 bkl Coufalík, Pavel verfasserin aut The direct determination of HgS by thermal desorption coupled with atomic absorption spectrometry 2016transfer abstract 5 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. Zvěřina, Ondřej oth Komárek, Josef oth Enthalten in Elsevier Li, Qiang ELSEVIER Dual stimuli-responsive polypeptide-calcium phosphate hybrid nanoparticles for co-delivery of multiple drugs in cancer therapy 2021 Amsterdam [u.a.] (DE-627)ELV005740053 volume:118 year:2016 day:1 month:04 pages:1-5 extent:5 https://doi.org/10.1016/j.sab.2016.01.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 42.15 Zellbiologie VZ AR 118 2016 1 0401 1-5 5 045F 540 |
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| author-letter |
Coufalík, Pavel |
| doi_str_mv |
10.1016/j.sab.2016.01.004 |
| dewey-full |
540 530 |
| title_sort |
direct determination of hgs by thermal desorption coupled with atomic absorption spectrometry |
| title_auth |
The direct determination of HgS by thermal desorption coupled with atomic absorption spectrometry |
| abstract |
This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. |
| abstractGer |
This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. |
| abstract_unstemmed |
This research was aimed at the direct determination of HgS in environmental samples by means of thermal desorption coupled with atomic absorption spectrometry. Operating parameters of the apparatus used for thermal desorption (including a prototype desorption unit) are described in this work, as well as the procedure for measuring mercury release curves together with an evaluation of the analytical signal including two methods of peak integration. The results of thermal desorption were compared with HgS contents obtained by sequential extraction. The limits of quantification of the proposed method for the selective determination of the black and red forms of HgS were 4μgkg−1 and 5μgkg−1, respectively. The limit of quantification of red HgS in soils was 35μgkg−1. The developed analytical procedure was applied to soil and sediment samples from historical mining areas. |
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GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA |
| title_short |
The direct determination of HgS by thermal desorption coupled with atomic absorption spectrometry |
| url |
https://doi.org/10.1016/j.sab.2016.01.004 |
| remote_bool |
true |
| author2 |
Zvěřina, Ondřej Komárek, Josef |
| author2Str |
Zvěřina, Ondřej Komárek, Josef |
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| doi_str |
10.1016/j.sab.2016.01.004 |
| up_date |
2024-07-06T22:27:10.613Z |
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7.3993254 |