Determination of multi-mycotoxins in cereals and of total fumonisins in maize products using isotope labeled internal standard and liquid chromatography/tandem mass spectrometry with positive ionization
• A LC-ESI+-MS/MS multi-mycotoxin method was successfully validated. • Total fumonisins were determined through analysis of bound/hidden fumonisins. • Bound/hidden fumonisins were obtained after alkaline hydrolysis and SLE-LTP. • Isotope internal standards were essential for maize and wheat products...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Andrade, Patrícia Diniz [verfasserIn] |
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E-Artikel |
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Englisch |
| Erschienen: |
2017 |
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| Schlagwörter: |
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| Umfang: |
10 |
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| Übergeordnetes Werk: |
Enthalten in: Defense development: The role of co-creation in filling the gap between policy-makers and technology development - Liwång, Hans ELSEVIER, 2022, including electrophoresis, mass spectrometry and other separation and detection methods, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:1490 ; year:2017 ; day:24 ; month:03 ; pages:138-147 ; extent:10 |
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| DOI / URN: |
10.1016/j.chroma.2017.02.027 |
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determination of multi-mycotoxins in cereals and of total fumonisins in maize products using isotope labeled internal standard and liquid chromatography/tandem mass spectrometry with positive ionization |
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Determination of multi-mycotoxins in cereals and of total fumonisins in maize products using isotope labeled internal standard and liquid chromatography/tandem mass spectrometry with positive ionization |
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• A LC-ESI+-MS/MS multi-mycotoxin method was successfully validated. • Total fumonisins were determined through analysis of bound/hidden fumonisins. • Bound/hidden fumonisins were obtained after alkaline hydrolysis and SLE-LTP. • Isotope internal standards were essential for maize and wheat products analysis. • Wheat-based products were contaminated with at least one mycotoxin. |
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• A LC-ESI+-MS/MS multi-mycotoxin method was successfully validated. • Total fumonisins were determined through analysis of bound/hidden fumonisins. • Bound/hidden fumonisins were obtained after alkaline hydrolysis and SLE-LTP. • Isotope internal standards were essential for maize and wheat products analysis. • Wheat-based products were contaminated with at least one mycotoxin. |
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• A LC-ESI+-MS/MS multi-mycotoxin method was successfully validated. • Total fumonisins were determined through analysis of bound/hidden fumonisins. • Bound/hidden fumonisins were obtained after alkaline hydrolysis and SLE-LTP. • Isotope internal standards were essential for maize and wheat products analysis. • Wheat-based products were contaminated with at least one mycotoxin. |
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Determination of multi-mycotoxins in cereals and of total fumonisins in maize products using isotope labeled internal standard and liquid chromatography/tandem mass spectrometry with positive ionization |
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https://doi.org/10.1016/j.chroma.2017.02.027 |
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Dantas, Rebecca Rodrigues Moura-Alves, Tatiana Loureiro da Silva de Caldas, Eloisa Dutra |
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10.1016/j.chroma.2017.02.027 |
| up_date |
2024-07-06T18:30:32.972Z |
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