Structural study and phase transition investigation in a simple synthesis of porous architected-ZnO nanopowder
In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additiv...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Shang, C. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2013transfer abstract |
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| Umfang: |
6 |
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| Übergeordnetes Werk: |
Enthalten in: Genotype-by-environment interactions and sexual selection - Shuker, David M. ELSEVIER, 2015, an international journal on materials structure and behavior, New York, NY |
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| Übergeordnetes Werk: |
volume:86 ; year:2013 ; pages:206-211 ; extent:6 |
| Links: |
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| DOI / URN: |
10.1016/j.matchar.2013.10.004 |
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| 520 | |a In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. | ||
| 520 | |a In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. | ||
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10.1016/j.matchar.2013.10.004 doi GBVA2013017000001.pica (DE-627)ELV033362033 (ELSEVIER)S1044-5803(13)00299-4 DE-627 ger DE-627 rakwb eng 670 670 DE-600 150 VZ 620 VZ 52.56 bkl Shang, C. verfasserin aut Structural study and phase transition investigation in a simple synthesis of porous architected-ZnO nanopowder 2013transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. Barnabé, A. oth Enthalten in Science Direct Shuker, David M. ELSEVIER Genotype-by-environment interactions and sexual selection 2015 an international journal on materials structure and behavior New York, NY (DE-627)ELV018863809 volume:86 year:2013 pages:206-211 extent:6 https://doi.org/10.1016/j.matchar.2013.10.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_22 GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 86 2013 206-211 6 045F 670 |
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10.1016/j.matchar.2013.10.004 doi GBVA2013017000001.pica (DE-627)ELV033362033 (ELSEVIER)S1044-5803(13)00299-4 DE-627 ger DE-627 rakwb eng 670 670 DE-600 150 VZ 620 VZ 52.56 bkl Shang, C. verfasserin aut Structural study and phase transition investigation in a simple synthesis of porous architected-ZnO nanopowder 2013transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. Barnabé, A. oth Enthalten in Science Direct Shuker, David M. ELSEVIER Genotype-by-environment interactions and sexual selection 2015 an international journal on materials structure and behavior New York, NY (DE-627)ELV018863809 volume:86 year:2013 pages:206-211 extent:6 https://doi.org/10.1016/j.matchar.2013.10.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_22 GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 86 2013 206-211 6 045F 670 |
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10.1016/j.matchar.2013.10.004 doi GBVA2013017000001.pica (DE-627)ELV033362033 (ELSEVIER)S1044-5803(13)00299-4 DE-627 ger DE-627 rakwb eng 670 670 DE-600 150 VZ 620 VZ 52.56 bkl Shang, C. verfasserin aut Structural study and phase transition investigation in a simple synthesis of porous architected-ZnO nanopowder 2013transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. Barnabé, A. oth Enthalten in Science Direct Shuker, David M. ELSEVIER Genotype-by-environment interactions and sexual selection 2015 an international journal on materials structure and behavior New York, NY (DE-627)ELV018863809 volume:86 year:2013 pages:206-211 extent:6 https://doi.org/10.1016/j.matchar.2013.10.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_22 GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 86 2013 206-211 6 045F 670 |
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10.1016/j.matchar.2013.10.004 doi GBVA2013017000001.pica (DE-627)ELV033362033 (ELSEVIER)S1044-5803(13)00299-4 DE-627 ger DE-627 rakwb eng 670 670 DE-600 150 VZ 620 VZ 52.56 bkl Shang, C. verfasserin aut Structural study and phase transition investigation in a simple synthesis of porous architected-ZnO nanopowder 2013transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. Barnabé, A. oth Enthalten in Science Direct Shuker, David M. ELSEVIER Genotype-by-environment interactions and sexual selection 2015 an international journal on materials structure and behavior New York, NY (DE-627)ELV018863809 volume:86 year:2013 pages:206-211 extent:6 https://doi.org/10.1016/j.matchar.2013.10.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_22 GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 86 2013 206-211 6 045F 670 |
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10.1016/j.matchar.2013.10.004 doi GBVA2013017000001.pica (DE-627)ELV033362033 (ELSEVIER)S1044-5803(13)00299-4 DE-627 ger DE-627 rakwb eng 670 670 DE-600 150 VZ 620 VZ 52.56 bkl Shang, C. verfasserin aut Structural study and phase transition investigation in a simple synthesis of porous architected-ZnO nanopowder 2013transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. Barnabé, A. oth Enthalten in Science Direct Shuker, David M. ELSEVIER Genotype-by-environment interactions and sexual selection 2015 an international journal on materials structure and behavior New York, NY (DE-627)ELV018863809 volume:86 year:2013 pages:206-211 extent:6 https://doi.org/10.1016/j.matchar.2013.10.004 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_22 GBV_ILN_40 52.56 Regenerative Energieformen alternative Energieformen VZ AR 86 2013 206-211 6 045F 670 |
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A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. 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In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. |
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In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. |
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In this work, zinc oxide powder with a rectangular-shaped porous architecture, made of numerous spherical nanometric particles, was obtained. A simple precipitation/decomposition procedure was used comprising a zinc oxalate intermediate, obtained from zinc sulfate and oxalic acid without any additives. Detailed studies on zinc oxalate dehydration, decomposition and zinc oxide formation, were carried out using in-situ temperature X-ray diffraction and thermogravimetric analysis. During the investigation, the temperature dependence of particle sizes, lattice parameters and crystal structures of ZnC2O4·2H2O, ZnC2O4 and ZnO nanopowders were analyzed from room temperature to 450°C. Structural transitions were also discussed. The structure and morphology of the as-prepared ZnO nanopowder were investigated by electron microscopy and compared to the crystalline rectangular shape of ZnC2O4·2H2O. The calcination temperature, counter ion and precipitate agent were found to be related to the product's shape and diameter. Spherical ZnO nanoparticles with diameters of less than 20nm and a maximum specific surface of 53m2/g were obtained using this method. |
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