Spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives
The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroanilin...
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| Autor*in: |
Özkınalı, Sevil [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2014transfer abstract |
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| Umfang: |
9 |
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| Übergeordnetes Werk: |
Enthalten in: A multiscale analysis for free vibration of fuzzy fiber-reinforced nanocomposite conical shells - Haghgoo, M. ELSEVIER, 2020, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:107 ; year:2014 ; pages:81-89 ; extent:9 |
| Links: |
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| DOI / URN: |
10.1016/j.dyepig.2014.03.028 |
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| 520 | |a The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. | ||
| 520 | |a The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. | ||
| 650 | 7 | |a Azocalix[4]arene |2 Elsevier | |
| 650 | 7 | |a Azocalix[4]arene-ester |2 Elsevier | |
| 650 | 7 | |a Calix[4]arene |2 Elsevier | |
| 650 | 7 | |a Acryloyl ester of azocalix[4]arene |2 Elsevier | |
| 650 | 7 | |a Thermal analysis |2 Elsevier | |
| 650 | 7 | |a Acryloyl chloride |2 Elsevier | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier Science |a Haghgoo, M. ELSEVIER |t A multiscale analysis for free vibration of fuzzy fiber-reinforced nanocomposite conical shells |d 2020 |g Amsterdam [u.a.] |w (DE-627)ELV004269640 |
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10.1016/j.dyepig.2014.03.028 doi GBVA2014003000021.pica (DE-627)ELV033672237 (ELSEVIER)S0143-7208(14)00108-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 690 VZ 50.31 bkl 56.11 bkl Özkınalı, Sevil verfasserin aut Spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives 2014transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. Azocalix[4]arene Elsevier Azocalix[4]arene-ester Elsevier Calix[4]arene Elsevier Acryloyl ester of azocalix[4]arene Elsevier Thermal analysis Elsevier Acryloyl chloride Elsevier Enthalten in Elsevier Science Haghgoo, M. ELSEVIER A multiscale analysis for free vibration of fuzzy fiber-reinforced nanocomposite conical shells 2020 Amsterdam [u.a.] (DE-627)ELV004269640 volume:107 year:2014 pages:81-89 extent:9 https://doi.org/10.1016/j.dyepig.2014.03.028 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.31 Technische Mechanik VZ 56.11 Baukonstruktion VZ AR 107 2014 81-89 9 045F 660 |
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10.1016/j.dyepig.2014.03.028 doi GBVA2014003000021.pica (DE-627)ELV033672237 (ELSEVIER)S0143-7208(14)00108-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 690 VZ 50.31 bkl 56.11 bkl Özkınalı, Sevil verfasserin aut Spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives 2014transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. Azocalix[4]arene Elsevier Azocalix[4]arene-ester Elsevier Calix[4]arene Elsevier Acryloyl ester of azocalix[4]arene Elsevier Thermal analysis Elsevier Acryloyl chloride Elsevier Enthalten in Elsevier Science Haghgoo, M. ELSEVIER A multiscale analysis for free vibration of fuzzy fiber-reinforced nanocomposite conical shells 2020 Amsterdam [u.a.] (DE-627)ELV004269640 volume:107 year:2014 pages:81-89 extent:9 https://doi.org/10.1016/j.dyepig.2014.03.028 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.31 Technische Mechanik VZ 56.11 Baukonstruktion VZ AR 107 2014 81-89 9 045F 660 |
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10.1016/j.dyepig.2014.03.028 doi GBVA2014003000021.pica (DE-627)ELV033672237 (ELSEVIER)S0143-7208(14)00108-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 690 VZ 50.31 bkl 56.11 bkl Özkınalı, Sevil verfasserin aut Spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives 2014transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. Azocalix[4]arene Elsevier Azocalix[4]arene-ester Elsevier Calix[4]arene Elsevier Acryloyl ester of azocalix[4]arene Elsevier Thermal analysis Elsevier Acryloyl chloride Elsevier Enthalten in Elsevier Science Haghgoo, M. ELSEVIER A multiscale analysis for free vibration of fuzzy fiber-reinforced nanocomposite conical shells 2020 Amsterdam [u.a.] (DE-627)ELV004269640 volume:107 year:2014 pages:81-89 extent:9 https://doi.org/10.1016/j.dyepig.2014.03.028 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.31 Technische Mechanik VZ 56.11 Baukonstruktion VZ AR 107 2014 81-89 9 045F 660 |
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10.1016/j.dyepig.2014.03.028 doi GBVA2014003000021.pica (DE-627)ELV033672237 (ELSEVIER)S0143-7208(14)00108-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 690 VZ 50.31 bkl 56.11 bkl Özkınalı, Sevil verfasserin aut Spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives 2014transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. Azocalix[4]arene Elsevier Azocalix[4]arene-ester Elsevier Calix[4]arene Elsevier Acryloyl ester of azocalix[4]arene Elsevier Thermal analysis Elsevier Acryloyl chloride Elsevier Enthalten in Elsevier Science Haghgoo, M. ELSEVIER A multiscale analysis for free vibration of fuzzy fiber-reinforced nanocomposite conical shells 2020 Amsterdam [u.a.] (DE-627)ELV004269640 volume:107 year:2014 pages:81-89 extent:9 https://doi.org/10.1016/j.dyepig.2014.03.028 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.31 Technische Mechanik VZ 56.11 Baukonstruktion VZ AR 107 2014 81-89 9 045F 660 |
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10.1016/j.dyepig.2014.03.028 doi GBVA2014003000021.pica (DE-627)ELV033672237 (ELSEVIER)S0143-7208(14)00108-9 DE-627 ger DE-627 rakwb eng 660 660 DE-600 690 VZ 50.31 bkl 56.11 bkl Özkınalı, Sevil verfasserin aut Spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives 2014transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. Azocalix[4]arene Elsevier Azocalix[4]arene-ester Elsevier Calix[4]arene Elsevier Acryloyl ester of azocalix[4]arene Elsevier Thermal analysis Elsevier Acryloyl chloride Elsevier Enthalten in Elsevier Science Haghgoo, M. ELSEVIER A multiscale analysis for free vibration of fuzzy fiber-reinforced nanocomposite conical shells 2020 Amsterdam [u.a.] (DE-627)ELV004269640 volume:107 year:2014 pages:81-89 extent:9 https://doi.org/10.1016/j.dyepig.2014.03.028 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.31 Technische Mechanik VZ 56.11 Baukonstruktion VZ AR 107 2014 81-89 9 045F 660 |
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Enthalten in A multiscale analysis for free vibration of fuzzy fiber-reinforced nanocomposite conical shells Amsterdam [u.a.] volume:107 year:2014 pages:81-89 extent:9 |
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Enthalten in A multiscale analysis for free vibration of fuzzy fiber-reinforced nanocomposite conical shells Amsterdam [u.a.] volume:107 year:2014 pages:81-89 extent:9 |
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Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). 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spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives |
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Spectroscopic and thermal properties of newly mixed azocalix[4]arene ester derivatives |
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The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. |
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The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. |
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The mono-, di-, tri-, and tetra-acryloyl esters of p-chloroazocalix[4]arene which include the first examples of mixed azo ester dyes were synthesized by reacting acryloyl chloride with sodium salts of p-chloroazocalix[4]arene in tetrahydrofuran with inert atmosphere. Diazonium salt of p-chloroaniline was synthesized by using n-amlynitrite and coupled with calix[4]arene in anhydrous condition. This is the diazo coupling reactions used for the first time for synthesized azocalix[4]arene. The characterization of synthesized compounds by spectroscopic methods revealed that azocalix[4]arenes adopt a cone conformation if they contain at least one free phenolic group. The structures of these compounds have been characterized by infrared (IR), ultraviolet–visible (UV–VIS), proton nuclear magnetic resonance (1H NMR) and carbon nuclear magnetic resonance (13C NMR). Differential thermal analysis (DTA), thermogravimetry (TG) and derivative thermogravimetry (DTG) were used to determine the thermal behaviors of the compounds. |
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