Platinum–Iron nanoparticles supported on reduced graphene oxide as an improved catalyst for methanol electro oxidation
Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was ch...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Eshghi, Abolfath [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2018transfer abstract |
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| Umfang: |
10 |
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| Übergeordnetes Werk: |
Enthalten in: External auditory canal: Inferior, posterior-inferior, and anterior canal wall overhangs - Dedhia, Kavita ELSEVIER, 2018, official journal of the International Association for Hydrogen Energy, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:43 ; year:2018 ; number:12 ; day:22 ; month:03 ; pages:6107-6116 ; extent:10 |
| Links: |
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| DOI / URN: |
10.1016/j.ijhydene.2018.01.206 |
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| 520 | |a Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. | ||
| 520 | |a Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. | ||
| 650 | 7 | |a Direct methanol fuel cell |2 Elsevier | |
| 650 | 7 | |a Platinum |2 Elsevier | |
| 650 | 7 | |a Iron |2 Elsevier | |
| 650 | 7 | |a Anode catalyst |2 Elsevier | |
| 650 | 7 | |a Reduced graphene oxide |2 Elsevier | |
| 700 | 1 | |a kheirmand, Mehdi |4 oth | |
| 700 | 1 | |a Sabzehmeidani, Mohammad Mehdi |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier |a Dedhia, Kavita ELSEVIER |t External auditory canal: Inferior, posterior-inferior, and anterior canal wall overhangs |d 2018 |d official journal of the International Association for Hydrogen Energy |g New York, NY [u.a.] |w (DE-627)ELV000127019 |
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10.1016/j.ijhydene.2018.01.206 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001021.pica (DE-627)ELV042270162 (ELSEVIER)S0360-3199(18)30359-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.94 bkl Eshghi, Abolfath verfasserin aut Platinum–Iron nanoparticles supported on reduced graphene oxide as an improved catalyst for methanol electro oxidation 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Direct methanol fuel cell Elsevier Platinum Elsevier Iron Elsevier Anode catalyst Elsevier Reduced graphene oxide Elsevier kheirmand, Mehdi oth Sabzehmeidani, Mohammad Mehdi oth Enthalten in Elsevier Dedhia, Kavita ELSEVIER External auditory canal: Inferior, posterior-inferior, and anterior canal wall overhangs 2018 official journal of the International Association for Hydrogen Energy New York, NY [u.a.] (DE-627)ELV000127019 volume:43 year:2018 number:12 day:22 month:03 pages:6107-6116 extent:10 https://doi.org/10.1016/j.ijhydene.2018.01.206 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.94 Hals-Nasen-Ohrenheilkunde VZ AR 43 2018 12 22 0322 6107-6116 10 |
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10.1016/j.ijhydene.2018.01.206 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001021.pica (DE-627)ELV042270162 (ELSEVIER)S0360-3199(18)30359-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.94 bkl Eshghi, Abolfath verfasserin aut Platinum–Iron nanoparticles supported on reduced graphene oxide as an improved catalyst for methanol electro oxidation 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Direct methanol fuel cell Elsevier Platinum Elsevier Iron Elsevier Anode catalyst Elsevier Reduced graphene oxide Elsevier kheirmand, Mehdi oth Sabzehmeidani, Mohammad Mehdi oth Enthalten in Elsevier Dedhia, Kavita ELSEVIER External auditory canal: Inferior, posterior-inferior, and anterior canal wall overhangs 2018 official journal of the International Association for Hydrogen Energy New York, NY [u.a.] (DE-627)ELV000127019 volume:43 year:2018 number:12 day:22 month:03 pages:6107-6116 extent:10 https://doi.org/10.1016/j.ijhydene.2018.01.206 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.94 Hals-Nasen-Ohrenheilkunde VZ AR 43 2018 12 22 0322 6107-6116 10 |
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10.1016/j.ijhydene.2018.01.206 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001021.pica (DE-627)ELV042270162 (ELSEVIER)S0360-3199(18)30359-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.94 bkl Eshghi, Abolfath verfasserin aut Platinum–Iron nanoparticles supported on reduced graphene oxide as an improved catalyst for methanol electro oxidation 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Direct methanol fuel cell Elsevier Platinum Elsevier Iron Elsevier Anode catalyst Elsevier Reduced graphene oxide Elsevier kheirmand, Mehdi oth Sabzehmeidani, Mohammad Mehdi oth Enthalten in Elsevier Dedhia, Kavita ELSEVIER External auditory canal: Inferior, posterior-inferior, and anterior canal wall overhangs 2018 official journal of the International Association for Hydrogen Energy New York, NY [u.a.] (DE-627)ELV000127019 volume:43 year:2018 number:12 day:22 month:03 pages:6107-6116 extent:10 https://doi.org/10.1016/j.ijhydene.2018.01.206 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.94 Hals-Nasen-Ohrenheilkunde VZ AR 43 2018 12 22 0322 6107-6116 10 |
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10.1016/j.ijhydene.2018.01.206 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001021.pica (DE-627)ELV042270162 (ELSEVIER)S0360-3199(18)30359-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.94 bkl Eshghi, Abolfath verfasserin aut Platinum–Iron nanoparticles supported on reduced graphene oxide as an improved catalyst for methanol electro oxidation 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Direct methanol fuel cell Elsevier Platinum Elsevier Iron Elsevier Anode catalyst Elsevier Reduced graphene oxide Elsevier kheirmand, Mehdi oth Sabzehmeidani, Mohammad Mehdi oth Enthalten in Elsevier Dedhia, Kavita ELSEVIER External auditory canal: Inferior, posterior-inferior, and anterior canal wall overhangs 2018 official journal of the International Association for Hydrogen Energy New York, NY [u.a.] (DE-627)ELV000127019 volume:43 year:2018 number:12 day:22 month:03 pages:6107-6116 extent:10 https://doi.org/10.1016/j.ijhydene.2018.01.206 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.94 Hals-Nasen-Ohrenheilkunde VZ AR 43 2018 12 22 0322 6107-6116 10 |
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10.1016/j.ijhydene.2018.01.206 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001021.pica (DE-627)ELV042270162 (ELSEVIER)S0360-3199(18)30359-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.94 bkl Eshghi, Abolfath verfasserin aut Platinum–Iron nanoparticles supported on reduced graphene oxide as an improved catalyst for methanol electro oxidation 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. Direct methanol fuel cell Elsevier Platinum Elsevier Iron Elsevier Anode catalyst Elsevier Reduced graphene oxide Elsevier kheirmand, Mehdi oth Sabzehmeidani, Mohammad Mehdi oth Enthalten in Elsevier Dedhia, Kavita ELSEVIER External auditory canal: Inferior, posterior-inferior, and anterior canal wall overhangs 2018 official journal of the International Association for Hydrogen Energy New York, NY [u.a.] (DE-627)ELV000127019 volume:43 year:2018 number:12 day:22 month:03 pages:6107-6116 extent:10 https://doi.org/10.1016/j.ijhydene.2018.01.206 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.94 Hals-Nasen-Ohrenheilkunde VZ AR 43 2018 12 22 0322 6107-6116 10 |
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Enthalten in External auditory canal: Inferior, posterior-inferior, and anterior canal wall overhangs New York, NY [u.a.] volume:43 year:2018 number:12 day:22 month:03 pages:6107-6116 extent:10 |
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Enthalten in External auditory canal: Inferior, posterior-inferior, and anterior canal wall overhangs New York, NY [u.a.] volume:43 year:2018 number:12 day:22 month:03 pages:6107-6116 extent:10 |
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The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. 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Platinum–Iron nanoparticles supported on reduced graphene oxide as an improved catalyst for methanol electro oxidation |
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Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. |
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Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. |
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Platinum–Iron nanoparticles supported on reduced graphene oxide powder are synthesized by chemical reduction method as an anode catalyst for the methanol electro oxidation. The characterization of the catalyst has been investigated using physical and electrochemical methods. Prepared catalyst was characterized by scanning electron microscopy (SEM), TEM (Transmission electron microscopy), FT-IR (Fourier-transform infrared spectroscopy), Raman spectroscopy and, X-ray diffraction (XRD) and energy dispersive analysis of X-ray (EDX). Pt and Pt-Fe nanoparticles are uniformly dispersed on the surface of reduced graphene oxide (rGO) powder nanocomposite support. The catalytic properties of the catalyst for methanol electro-oxidation were thoroughly studied by electrochemical methods that involved in the cyclic voltammetry, linear sweep voltammetry (LSV), chronoamperometry and electrochemical impedance spectroscopy (EIS). The Pt-Fe/rGo exhibits high electrocatalytic activity, catalyst tolerance for the CO poisoning and catalyst durability for electro-oxidation of methanol compared to the Pt/rGo and commercial Pt/C catalyst. Therefore, the Pt-Fe/rGo catalyst is a good choice for application in direct methanol fuel cells. |
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