In situ growth of Ni/NiO on N-doped carbon spheres with excellent electrocatalytic performance for non-enzymatic glucose detection
A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Zhu, Jiajie [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2018transfer abstract |
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| Schlagwörter: |
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| Umfang: |
9 |
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| Übergeordnetes Werk: |
Enthalten in: Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners - Jacobs, Jacquelyn A. ELSEVIER, 2017, JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics, Lausanne |
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| Übergeordnetes Werk: |
volume:748 ; year:2018 ; day:5 ; month:06 ; pages:145-153 ; extent:9 |
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| DOI / URN: |
10.1016/j.jallcom.2018.03.125 |
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| 520 | |a A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. | ||
| 520 | |a A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. | ||
| 650 | 7 | |a Ni/NiO nanoparticles |2 Elsevier | |
| 650 | 7 | |a Carbon spheres |2 Elsevier | |
| 650 | 7 | |a Glucose sensor |2 Elsevier | |
| 650 | 7 | |a Nitrogen doping |2 Elsevier | |
| 700 | 1 | |a Yin, Haoyong |4 oth | |
| 700 | 1 | |a Gong, Jianying |4 oth | |
| 700 | 1 | |a Al-Furjan, M.S.H. |4 oth | |
| 700 | 1 | |a Nie, Qiulin |4 oth | |
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10.1016/j.jallcom.2018.03.125 doi GBV00000000000514.pica (DE-627)ELV04267042X (ELSEVIER)S0925-8388(18)30993-9 DE-627 ger DE-627 rakwb eng 630 VZ Zhu, Jiajie verfasserin aut In situ growth of Ni/NiO on N-doped carbon spheres with excellent electrocatalytic performance for non-enzymatic glucose detection 2018transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. Ni/NiO nanoparticles Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Yin, Haoyong oth Gong, Jianying oth Al-Furjan, M.S.H. oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:748 year:2018 day:5 month:06 pages:145-153 extent:9 https://doi.org/10.1016/j.jallcom.2018.03.125 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 748 2018 5 0605 145-153 9 |
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10.1016/j.jallcom.2018.03.125 doi GBV00000000000514.pica (DE-627)ELV04267042X (ELSEVIER)S0925-8388(18)30993-9 DE-627 ger DE-627 rakwb eng 630 VZ Zhu, Jiajie verfasserin aut In situ growth of Ni/NiO on N-doped carbon spheres with excellent electrocatalytic performance for non-enzymatic glucose detection 2018transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. Ni/NiO nanoparticles Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Yin, Haoyong oth Gong, Jianying oth Al-Furjan, M.S.H. oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:748 year:2018 day:5 month:06 pages:145-153 extent:9 https://doi.org/10.1016/j.jallcom.2018.03.125 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 748 2018 5 0605 145-153 9 |
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10.1016/j.jallcom.2018.03.125 doi GBV00000000000514.pica (DE-627)ELV04267042X (ELSEVIER)S0925-8388(18)30993-9 DE-627 ger DE-627 rakwb eng 630 VZ Zhu, Jiajie verfasserin aut In situ growth of Ni/NiO on N-doped carbon spheres with excellent electrocatalytic performance for non-enzymatic glucose detection 2018transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. Ni/NiO nanoparticles Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Yin, Haoyong oth Gong, Jianying oth Al-Furjan, M.S.H. oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:748 year:2018 day:5 month:06 pages:145-153 extent:9 https://doi.org/10.1016/j.jallcom.2018.03.125 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 748 2018 5 0605 145-153 9 |
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10.1016/j.jallcom.2018.03.125 doi GBV00000000000514.pica (DE-627)ELV04267042X (ELSEVIER)S0925-8388(18)30993-9 DE-627 ger DE-627 rakwb eng 630 VZ Zhu, Jiajie verfasserin aut In situ growth of Ni/NiO on N-doped carbon spheres with excellent electrocatalytic performance for non-enzymatic glucose detection 2018transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. Ni/NiO nanoparticles Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Yin, Haoyong oth Gong, Jianying oth Al-Furjan, M.S.H. oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:748 year:2018 day:5 month:06 pages:145-153 extent:9 https://doi.org/10.1016/j.jallcom.2018.03.125 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 748 2018 5 0605 145-153 9 |
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10.1016/j.jallcom.2018.03.125 doi GBV00000000000514.pica (DE-627)ELV04267042X (ELSEVIER)S0925-8388(18)30993-9 DE-627 ger DE-627 rakwb eng 630 VZ Zhu, Jiajie verfasserin aut In situ growth of Ni/NiO on N-doped carbon spheres with excellent electrocatalytic performance for non-enzymatic glucose detection 2018transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. Ni/NiO nanoparticles Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Yin, Haoyong oth Gong, Jianying oth Al-Furjan, M.S.H. oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:748 year:2018 day:5 month:06 pages:145-153 extent:9 https://doi.org/10.1016/j.jallcom.2018.03.125 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 748 2018 5 0605 145-153 9 |
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Enthalten in Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners Lausanne volume:748 year:2018 day:5 month:06 pages:145-153 extent:9 |
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in situ growth of ni/nio on n-doped carbon spheres with excellent electrocatalytic performance for non-enzymatic glucose detection |
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In situ growth of Ni/NiO on N-doped carbon spheres with excellent electrocatalytic performance for non-enzymatic glucose detection |
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A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. |
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A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. |
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A non-enzymatic potentiometric glucose sensor was developed by modifying a glass carbon electrode (GCD) with Ni/NiO decorated nitrogen doped carbon spheres (Ni/NiO/NCSs). The Ni/NiO/NCSs were prepared with in situ growth of Ni/NiO on the nitrogen doped carbon spheres. The morphology and composition of the materials were characterized by SEM, TEM, XRD and XPS, respectively. The Ni/NiO/NCSs modified GCD electrode exhibited higher current response than that of nitrogen free counterpart and NiO/nitrogen carbon spheres for non-enzymatic oxidation of glucose in alkaline media. The amperometric measurement revealed that the sensor had wide linear regions of 2 μM–600 μM and 800 μM-2500 μM with a sensitivity of 219.19 μA mM−1cm−2 and 87.88 μAmM−1cm−2 respectively. Moreover, the Ni/NiO/NCS composites also exhibited good selectivity by adding certain amount of urea, NaCl, l-proline, l-valine, l-Leucine and ascorbic acid into 0.1 M NaOH solution. The excellent electrocatalytic performance may be attributed to the synergistic effect of nitrogen doping and Ni loading, which may result in the increase of electron density and the enhancement of surface conductivity of the composite electrode materials. |
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In situ growth of Ni/NiO on N-doped carbon spheres with excellent electrocatalytic performance for non-enzymatic glucose detection |
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