Synthesis, characterization, corrosion and bioactivity investigation of nano-HA coating deposited on biodegradable Mg-Zn-Mn alloy
Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to de...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Prakash, Chander [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2018transfer abstract |
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| Umfang: |
10 |
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| Übergeordnetes Werk: |
Enthalten in: A high efficiency solar steam generation system with using residual heat to enhance steam escape - Bai, Binglin ELSEVIER, 2020, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:346 ; year:2018 ; day:25 ; month:07 ; pages:9-18 ; extent:10 |
| Links: |
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| DOI / URN: |
10.1016/j.surfcoat.2018.04.035 |
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ELV043013082 |
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| 520 | |a Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. | ||
| 520 | |a Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. | ||
| 700 | 1 | |a Singh, Sunpreet |4 oth | |
| 700 | 1 | |a Pabla, B.S. |4 oth | |
| 700 | 1 | |a Uddin, M.S. |4 oth | |
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10.1016/j.surfcoat.2018.04.035 doi GBV00000000000229A.pica (DE-627)ELV043013082 (ELSEVIER)S0257-8972(18)30396-7 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Prakash, Chander verfasserin aut Synthesis, characterization, corrosion and bioactivity investigation of nano-HA coating deposited on biodegradable Mg-Zn-Mn alloy 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Singh, Sunpreet oth Pabla, B.S. oth Uddin, M.S. oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:346 year:2018 day:25 month:07 pages:9-18 extent:10 https://doi.org/10.1016/j.surfcoat.2018.04.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 346 2018 25 0725 9-18 10 045F 620 |
| spelling |
10.1016/j.surfcoat.2018.04.035 doi GBV00000000000229A.pica (DE-627)ELV043013082 (ELSEVIER)S0257-8972(18)30396-7 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Prakash, Chander verfasserin aut Synthesis, characterization, corrosion and bioactivity investigation of nano-HA coating deposited on biodegradable Mg-Zn-Mn alloy 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Singh, Sunpreet oth Pabla, B.S. oth Uddin, M.S. oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:346 year:2018 day:25 month:07 pages:9-18 extent:10 https://doi.org/10.1016/j.surfcoat.2018.04.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 346 2018 25 0725 9-18 10 045F 620 |
| allfields_unstemmed |
10.1016/j.surfcoat.2018.04.035 doi GBV00000000000229A.pica (DE-627)ELV043013082 (ELSEVIER)S0257-8972(18)30396-7 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Prakash, Chander verfasserin aut Synthesis, characterization, corrosion and bioactivity investigation of nano-HA coating deposited on biodegradable Mg-Zn-Mn alloy 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Singh, Sunpreet oth Pabla, B.S. oth Uddin, M.S. oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:346 year:2018 day:25 month:07 pages:9-18 extent:10 https://doi.org/10.1016/j.surfcoat.2018.04.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 346 2018 25 0725 9-18 10 045F 620 |
| allfieldsGer |
10.1016/j.surfcoat.2018.04.035 doi GBV00000000000229A.pica (DE-627)ELV043013082 (ELSEVIER)S0257-8972(18)30396-7 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Prakash, Chander verfasserin aut Synthesis, characterization, corrosion and bioactivity investigation of nano-HA coating deposited on biodegradable Mg-Zn-Mn alloy 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Singh, Sunpreet oth Pabla, B.S. oth Uddin, M.S. oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:346 year:2018 day:25 month:07 pages:9-18 extent:10 https://doi.org/10.1016/j.surfcoat.2018.04.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 346 2018 25 0725 9-18 10 045F 620 |
| allfieldsSound |
10.1016/j.surfcoat.2018.04.035 doi GBV00000000000229A.pica (DE-627)ELV043013082 (ELSEVIER)S0257-8972(18)30396-7 DE-627 ger DE-627 rakwb eng 620 670 620 DE-600 670 DE-600 570 690 VZ 58.51 bkl Prakash, Chander verfasserin aut Synthesis, characterization, corrosion and bioactivity investigation of nano-HA coating deposited on biodegradable Mg-Zn-Mn alloy 2018transfer abstract 10 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. Singh, Sunpreet oth Pabla, B.S. oth Uddin, M.S. oth Enthalten in Elsevier Science Bai, Binglin ELSEVIER A high efficiency solar steam generation system with using residual heat to enhance steam escape 2020 Amsterdam [u.a.] (DE-627)ELV004415906 volume:346 year:2018 day:25 month:07 pages:9-18 extent:10 https://doi.org/10.1016/j.surfcoat.2018.04.035 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 58.51 Abwassertechnik Wasseraufbereitung VZ AR 346 2018 25 0725 9-18 10 045F 620 |
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Synthesis, characterization, corrosion and bioactivity investigation of nano-HA coating deposited on biodegradable Mg-Zn-Mn alloy |
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Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. |
| abstractGer |
Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. |
| abstract_unstemmed |
Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells. |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">ELV043013082</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230626002837.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">180726s2018 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1016/j.surfcoat.2018.04.035</subfield><subfield code="2">doi</subfield></datafield><datafield tag="028" ind1="5" ind2="2"><subfield code="a">GBV00000000000229A.pica</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)ELV043013082</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(ELSEVIER)S0257-8972(18)30396-7</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">620</subfield><subfield code="a">670</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">620</subfield><subfield code="q">DE-600</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">670</subfield><subfield code="q">DE-600</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">570</subfield><subfield code="a">690</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">58.51</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Prakash, Chander</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Synthesis, characterization, corrosion and bioactivity investigation of nano-HA coating deposited on biodegradable Mg-Zn-Mn alloy</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2018transfer abstract</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">10</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zzz</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">z</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zu</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells.</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Electric discharge machining (EDM) is widely used to cut and shape the biomedical device substrates, following often a separate coating process to deposit another barrier layer to improve the corrosion performance. This paper presents an innovative single in-situ surface modification technique to deposit nano-hydroxyapatite (nHA) coating on biodegradable Mg-Zn-Mn alloy while shaping the device substrate via electric discharge machining (EDM). The key benefit of the technique is to carry out the whole process in a single setup, hence saving time and cost. The aim of the coating is to control implant's degradation rate and to improve in-vitro bioactivity with human cells. Morphology, elemental, and chemical composition of the nHA coated Mg-Zn-Mn surface were characterized by FE-SEM, EDS, and XRD, respectively, while microhardness is measured by a Vickers hardness tester. Corrosion tests were performed via potentiodynamic polarization measurements in a SBF (simulated body fluid) to evaluate the degradation kinetics. In-vitro cell culture study was carried out to evaluate biocompatibility and cell attachment onto the modified surface. Surface characterization results revealed that a biomimetic nHA containing interconnected nano-porosities of size 5-10 μm had been yielded on the substrate surface, which is beneficial for the apatite growth and osseo-integration. The deposited coating layer has comprised of Mg, Zn, Mn, O, Ca and P elements and formed intermetallic oxide phases, such as CaMg, Mg-Zn, Mn-CaO, Mn-P, and Ca-Mn-O, which improved the in-vitro corrosion performance. The degradation rate of Mg-Zn-Mn alloy was reduced by 90.85% from 0.82 mm/year to 0.07 mm/year by the deposition of nHA-coating layer. The microhardness of the modified surface was measured as 234 HV, which was 1.5 fold higher than the untreated surface. The corroded surface analysis showed that the dense intermetallic phases of nHA coating acted as a stable barrier layer, thus prohibiting the surface from degradation, and hence, improving the corrosion resistance. The in-vitro bioactivity analysis revealed that the nHA containing layer exhibited the superior bioactivity and promotes adhesion, growth, and proliferation of human osteoblastic MG-63 cells.</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Singh, Sunpreet</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Pabla, B.S.</subfield><subfield code="4">oth</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Uddin, M.S.</subfield><subfield code="4">oth</subfield></datafield><datafield tag="773" ind1="0" ind2="8"><subfield code="i">Enthalten in</subfield><subfield code="n">Elsevier Science</subfield><subfield code="a">Bai, Binglin ELSEVIER</subfield><subfield code="t">A high efficiency solar steam generation system with using residual heat to enhance steam escape</subfield><subfield code="d">2020</subfield><subfield code="g">Amsterdam [u.a.]</subfield><subfield code="w">(DE-627)ELV004415906</subfield></datafield><datafield tag="773" ind1="1" ind2="8"><subfield code="g">volume:346</subfield><subfield code="g">year:2018</subfield><subfield code="g">day:25</subfield><subfield code="g">month:07</subfield><subfield code="g">pages:9-18</subfield><subfield code="g">extent:10</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="u">https://doi.org/10.1016/j.surfcoat.2018.04.035</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_USEFLAG_U</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">GBV_ELV</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SYSFLAG_U</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">SSG-OLC-PHA</subfield></datafield><datafield tag="936" ind1="b" ind2="k"><subfield code="a">58.51</subfield><subfield code="j">Abwassertechnik</subfield><subfield code="j">Wasseraufbereitung</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="951" ind1=" " ind2=" "><subfield code="a">AR</subfield></datafield><datafield tag="952" ind1=" " ind2=" "><subfield code="d">346</subfield><subfield code="j">2018</subfield><subfield code="b">25</subfield><subfield code="c">0725</subfield><subfield code="h">9-18</subfield><subfield code="g">10</subfield></datafield><datafield tag="953" ind1=" " ind2=" "><subfield code="2">045F</subfield><subfield code="a">620</subfield></datafield></record></collection>
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