Investigation of electrochemical calcium-ion energy storage mechanism in potassium birnessite
Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. He...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Hyoung, Jooeun [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2018transfer abstract |
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| Schlagwörter: |
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| Umfang: |
7 |
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| Übergeordnetes Werk: |
Enthalten in: Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method - Xiao, Hong ELSEVIER, 2013, the international journal on the science and technology of electrochemical energy systems, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:390 ; year:2018 ; day:30 ; month:06 ; pages:127-133 ; extent:7 |
| Links: |
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| DOI / URN: |
10.1016/j.jpowsour.2018.04.050 |
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| 520 | |a Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. | ||
| 520 | |a Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. | ||
| 650 | 7 | |a Calcium-ion battery |2 Elsevier | |
| 650 | 7 | |a Multivalent-ion battery |2 Elsevier | |
| 650 | 7 | |a Potassium birnessite |2 Elsevier | |
| 650 | 7 | |a Post lithium-ion battery |2 Elsevier | |
| 650 | 7 | |a Calcium intercalation |2 Elsevier | |
| 700 | 1 | |a Heo, Jongwook W. |4 oth | |
| 700 | 1 | |a Hong, Seung-Tae |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier |a Xiao, Hong ELSEVIER |t Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method |d 2013 |d the international journal on the science and technology of electrochemical energy systems |g New York, NY [u.a.] |w (DE-627)ELV00098745X |
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10.1016/j.jpowsour.2018.04.050 doi GBV00000000000512.pica (DE-627)ELV043075703 (ELSEVIER)S0378-7753(18)30393-8 DE-627 ger DE-627 rakwb eng 690 VZ 50.92 bkl Hyoung, Jooeun verfasserin aut Investigation of electrochemical calcium-ion energy storage mechanism in potassium birnessite 2018transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion battery Elsevier Multivalent-ion battery Elsevier Potassium birnessite Elsevier Post lithium-ion battery Elsevier Calcium intercalation Elsevier Heo, Jongwook W. oth Hong, Seung-Tae oth Enthalten in Elsevier Xiao, Hong ELSEVIER Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method 2013 the international journal on the science and technology of electrochemical energy systems New York, NY [u.a.] (DE-627)ELV00098745X volume:390 year:2018 day:30 month:06 pages:127-133 extent:7 https://doi.org/10.1016/j.jpowsour.2018.04.050 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.92 Meerestechnik VZ AR 390 2018 30 0630 127-133 7 |
| spelling |
10.1016/j.jpowsour.2018.04.050 doi GBV00000000000512.pica (DE-627)ELV043075703 (ELSEVIER)S0378-7753(18)30393-8 DE-627 ger DE-627 rakwb eng 690 VZ 50.92 bkl Hyoung, Jooeun verfasserin aut Investigation of electrochemical calcium-ion energy storage mechanism in potassium birnessite 2018transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion battery Elsevier Multivalent-ion battery Elsevier Potassium birnessite Elsevier Post lithium-ion battery Elsevier Calcium intercalation Elsevier Heo, Jongwook W. oth Hong, Seung-Tae oth Enthalten in Elsevier Xiao, Hong ELSEVIER Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method 2013 the international journal on the science and technology of electrochemical energy systems New York, NY [u.a.] (DE-627)ELV00098745X volume:390 year:2018 day:30 month:06 pages:127-133 extent:7 https://doi.org/10.1016/j.jpowsour.2018.04.050 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.92 Meerestechnik VZ AR 390 2018 30 0630 127-133 7 |
| allfields_unstemmed |
10.1016/j.jpowsour.2018.04.050 doi GBV00000000000512.pica (DE-627)ELV043075703 (ELSEVIER)S0378-7753(18)30393-8 DE-627 ger DE-627 rakwb eng 690 VZ 50.92 bkl Hyoung, Jooeun verfasserin aut Investigation of electrochemical calcium-ion energy storage mechanism in potassium birnessite 2018transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion battery Elsevier Multivalent-ion battery Elsevier Potassium birnessite Elsevier Post lithium-ion battery Elsevier Calcium intercalation Elsevier Heo, Jongwook W. oth Hong, Seung-Tae oth Enthalten in Elsevier Xiao, Hong ELSEVIER Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method 2013 the international journal on the science and technology of electrochemical energy systems New York, NY [u.a.] (DE-627)ELV00098745X volume:390 year:2018 day:30 month:06 pages:127-133 extent:7 https://doi.org/10.1016/j.jpowsour.2018.04.050 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.92 Meerestechnik VZ AR 390 2018 30 0630 127-133 7 |
| allfieldsGer |
10.1016/j.jpowsour.2018.04.050 doi GBV00000000000512.pica (DE-627)ELV043075703 (ELSEVIER)S0378-7753(18)30393-8 DE-627 ger DE-627 rakwb eng 690 VZ 50.92 bkl Hyoung, Jooeun verfasserin aut Investigation of electrochemical calcium-ion energy storage mechanism in potassium birnessite 2018transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion battery Elsevier Multivalent-ion battery Elsevier Potassium birnessite Elsevier Post lithium-ion battery Elsevier Calcium intercalation Elsevier Heo, Jongwook W. oth Hong, Seung-Tae oth Enthalten in Elsevier Xiao, Hong ELSEVIER Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method 2013 the international journal on the science and technology of electrochemical energy systems New York, NY [u.a.] (DE-627)ELV00098745X volume:390 year:2018 day:30 month:06 pages:127-133 extent:7 https://doi.org/10.1016/j.jpowsour.2018.04.050 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.92 Meerestechnik VZ AR 390 2018 30 0630 127-133 7 |
| allfieldsSound |
10.1016/j.jpowsour.2018.04.050 doi GBV00000000000512.pica (DE-627)ELV043075703 (ELSEVIER)S0378-7753(18)30393-8 DE-627 ger DE-627 rakwb eng 690 VZ 50.92 bkl Hyoung, Jooeun verfasserin aut Investigation of electrochemical calcium-ion energy storage mechanism in potassium birnessite 2018transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. Calcium-ion battery Elsevier Multivalent-ion battery Elsevier Potassium birnessite Elsevier Post lithium-ion battery Elsevier Calcium intercalation Elsevier Heo, Jongwook W. oth Hong, Seung-Tae oth Enthalten in Elsevier Xiao, Hong ELSEVIER Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method 2013 the international journal on the science and technology of electrochemical energy systems New York, NY [u.a.] (DE-627)ELV00098745X volume:390 year:2018 day:30 month:06 pages:127-133 extent:7 https://doi.org/10.1016/j.jpowsour.2018.04.050 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 50.92 Meerestechnik VZ AR 390 2018 30 0630 127-133 7 |
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Enthalten in Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method New York, NY [u.a.] volume:390 year:2018 day:30 month:06 pages:127-133 extent:7 |
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Enthalten in Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method New York, NY [u.a.] volume:390 year:2018 day:30 month:06 pages:127-133 extent:7 |
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Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method |
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Numerical modeling of wave–current forces acting on horizontal cylinder of marine structures by VOF method |
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investigation of electrochemical calcium-ion energy storage mechanism in potassium birnessite |
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Investigation of electrochemical calcium-ion energy storage mechanism in potassium birnessite |
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Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. |
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Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. |
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Calcium-ion intercalation-based batteries receive attention as one type of post lithium-ion battery because of their potential advantages in terms of cost and capacity. A birnessite-type manganese oxide, K0.31MnO2·0.25H2O, is characterized by a layered structure with interlayer distances of ∼7 Å. Here, we demonstrate for the first time the electrochemical Ca2+ ion intercalation capability of K-bir, and elucidate the calcium-ion storage mechanism. A reversible electrochemical reaction is observed in cyclic voltammograms and galvanostatic cycles. The initial specific discharge capacity is 153 mAh g−1 at 25.8 mA g−1 (0.1 C) in a 1 M Ca(NO3)2 aqueous electrolyte, with the average discharge voltage of 2.8 V (vs. Ca/Ca2+). X-ray diffraction, transmission electron microscopy, and elemental analyses confirm that Ca2+ ion transport is mainly responsible for the electrochemical reaction. A kinetic analysis using CVs with various scan rates indicates that the reaction mechanism can be described as a combined reaction of a surface-limited capacitance and a diffusion-controlled intercalation. In addition, 3D bond valence sum difference maps show the 2D network for conduction pathways of calcium ions in the structure. This work demonstrates that birnessite-type manganese oxide could be a potential cathode material for calcium-ion batteries. |
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Investigation of electrochemical calcium-ion energy storage mechanism in potassium birnessite |
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