Direct conversion of biomass-derived carbohydrates to 5-hydroxymethylfurfural using an efficient and inexpensive manganese phosphate catalyst
Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived c...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Xu, Siquan [verfasserIn] |
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E-Artikel |
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Englisch |
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2018transfer abstract |
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8 |
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| Übergeordnetes Werk: |
Enthalten in: Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications - Saini, Hardev S. ELSEVIER, 2015transfer abstract, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:181 ; year:2018 ; day:1 ; month:12 ; pages:199-206 ; extent:8 |
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10.1016/j.fuproc.2018.09.027 |
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| 245 | 1 | 0 | |a Direct conversion of biomass-derived carbohydrates to 5-hydroxymethylfurfural using an efficient and inexpensive manganese phosphate catalyst |
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| 520 | |a Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. | ||
| 520 | |a Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. | ||
| 700 | 1 | |a Pan, Donghui |4 oth | |
| 700 | 1 | |a Li, Wenqi |4 oth | |
| 700 | 1 | |a Shen, Pengxin |4 oth | |
| 700 | 1 | |a Wu, Yuanfeng |4 oth | |
| 700 | 1 | |a Song, Xianghai |4 oth | |
| 700 | 1 | |a Zhu, Yanli |4 oth | |
| 700 | 1 | |a Xu, Ningning |4 oth | |
| 700 | 1 | |a Gao, Lijing |4 oth | |
| 700 | 1 | |a Xiao, Guomin |4 oth | |
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10.1016/j.fuproc.2018.09.027 doi GBV00000000000411.pica (DE-627)ELV044596111 (ELSEVIER)S0378-3820(18)30785-9 DE-627 ger DE-627 rakwb eng 670 VZ 540 VZ 630 VZ Xu, Siquan verfasserin aut Direct conversion of biomass-derived carbohydrates to 5-hydroxymethylfurfural using an efficient and inexpensive manganese phosphate catalyst 2018transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Pan, Donghui oth Li, Wenqi oth Shen, Pengxin oth Wu, Yuanfeng oth Song, Xianghai oth Zhu, Yanli oth Xu, Ningning oth Gao, Lijing oth Xiao, Guomin oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:181 year:2018 day:1 month:12 pages:199-206 extent:8 https://doi.org/10.1016/j.fuproc.2018.09.027 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 181 2018 1 1201 199-206 8 |
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10.1016/j.fuproc.2018.09.027 doi GBV00000000000411.pica (DE-627)ELV044596111 (ELSEVIER)S0378-3820(18)30785-9 DE-627 ger DE-627 rakwb eng 670 VZ 540 VZ 630 VZ Xu, Siquan verfasserin aut Direct conversion of biomass-derived carbohydrates to 5-hydroxymethylfurfural using an efficient and inexpensive manganese phosphate catalyst 2018transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Pan, Donghui oth Li, Wenqi oth Shen, Pengxin oth Wu, Yuanfeng oth Song, Xianghai oth Zhu, Yanli oth Xu, Ningning oth Gao, Lijing oth Xiao, Guomin oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:181 year:2018 day:1 month:12 pages:199-206 extent:8 https://doi.org/10.1016/j.fuproc.2018.09.027 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 181 2018 1 1201 199-206 8 |
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10.1016/j.fuproc.2018.09.027 doi GBV00000000000411.pica (DE-627)ELV044596111 (ELSEVIER)S0378-3820(18)30785-9 DE-627 ger DE-627 rakwb eng 670 VZ 540 VZ 630 VZ Xu, Siquan verfasserin aut Direct conversion of biomass-derived carbohydrates to 5-hydroxymethylfurfural using an efficient and inexpensive manganese phosphate catalyst 2018transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Pan, Donghui oth Li, Wenqi oth Shen, Pengxin oth Wu, Yuanfeng oth Song, Xianghai oth Zhu, Yanli oth Xu, Ningning oth Gao, Lijing oth Xiao, Guomin oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:181 year:2018 day:1 month:12 pages:199-206 extent:8 https://doi.org/10.1016/j.fuproc.2018.09.027 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 181 2018 1 1201 199-206 8 |
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10.1016/j.fuproc.2018.09.027 doi GBV00000000000411.pica (DE-627)ELV044596111 (ELSEVIER)S0378-3820(18)30785-9 DE-627 ger DE-627 rakwb eng 670 VZ 540 VZ 630 VZ Xu, Siquan verfasserin aut Direct conversion of biomass-derived carbohydrates to 5-hydroxymethylfurfural using an efficient and inexpensive manganese phosphate catalyst 2018transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Pan, Donghui oth Li, Wenqi oth Shen, Pengxin oth Wu, Yuanfeng oth Song, Xianghai oth Zhu, Yanli oth Xu, Ningning oth Gao, Lijing oth Xiao, Guomin oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:181 year:2018 day:1 month:12 pages:199-206 extent:8 https://doi.org/10.1016/j.fuproc.2018.09.027 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 181 2018 1 1201 199-206 8 |
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10.1016/j.fuproc.2018.09.027 doi GBV00000000000411.pica (DE-627)ELV044596111 (ELSEVIER)S0378-3820(18)30785-9 DE-627 ger DE-627 rakwb eng 670 VZ 540 VZ 630 VZ Xu, Siquan verfasserin aut Direct conversion of biomass-derived carbohydrates to 5-hydroxymethylfurfural using an efficient and inexpensive manganese phosphate catalyst 2018transfer abstract 8 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. Pan, Donghui oth Li, Wenqi oth Shen, Pengxin oth Wu, Yuanfeng oth Song, Xianghai oth Zhu, Yanli oth Xu, Ningning oth Gao, Lijing oth Xiao, Guomin oth Enthalten in Science Direct Saini, Hardev S. ELSEVIER Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications 2015transfer abstract New York, NY [u.a.] (DE-627)ELV01324101X volume:181 year:2018 day:1 month:12 pages:199-206 extent:8 https://doi.org/10.1016/j.fuproc.2018.09.027 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_24 GBV_ILN_40 AR 181 2018 1 1201 199-206 8 |
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Enthalten in Generating magnetic response and half-metallicity in GaP via dilute Ti-doping for spintronic applications New York, NY [u.a.] volume:181 year:2018 day:1 month:12 pages:199-206 extent:8 |
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With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. 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direct conversion of biomass-derived carbohydrates to 5-hydroxymethylfurfural using an efficient and inexpensive manganese phosphate catalyst |
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Direct conversion of biomass-derived carbohydrates to 5-hydroxymethylfurfural using an efficient and inexpensive manganese phosphate catalyst |
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Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. |
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Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. |
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Achieving high yields of 5-hydroxymethylfurfural (HMF) from carbohydrates remains a challenge today. With the aim of developing an efficient and inexpensive catalyst for the production of HMF, manganese phosphate (MnPO4) was used as the sole catalyst for the catalytic conversion of biomass-derived carbohydrates into HMF in the H2O/tetrahydrofuran (THF) biphasic reaction system. The effects of various factors, including reaction temperature, reaction time, system, and catalyst dosage on the conversion of carbohydrates to HMF were explored. An impressing HMF yield of 59% was achieved with glucose as a feedstock at 160 °C for 90 min. Meanwhile, up to 44% of HMF was also obtained with microcrystalline cellulose as a feedstock at 170 °C for 120 min. In addition, MnPO4 catalyst also displayed outstanding catalytic activities for the conversion of other biomass-derived carbohydrates including monosaccharides and disaccharides. Combined with the dissolution characteristics of the MnPO4, a possible catalytic mechanism for the conversion of carbohydrates into HMF catalyzed by MnPO4 was proposed. The catalytic approach proposed in this paper exhibited a promising potential for HMF production via optimizing the catalytic process. |
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