Investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>Al
Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative...
Ausführliche Beschreibung
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Pánik, Ján [verfasserIn] |
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Englisch |
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2019transfer abstract |
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Enthalten in: Editorial Comment - Unwala, Darius J. ELSEVIER, 2013, a journal on accelerators, instrumentation and techniques applied to research in nuclear and atomic physics, materials science and related fields in physics, Amsterdam [u.a.] |
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Übergeordnetes Werk: |
volume:438 ; year:2019 ; day:1 ; month:01 ; pages:101-106 ; extent:6 |
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DOI / URN: |
10.1016/j.nimb.2018.07.013 |
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ELV045091323 |
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245 | 1 | 0 | |a Investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>Al |
264 | 1 | |c 2019transfer abstract | |
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520 | |a Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. | ||
520 | |a Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. | ||
650 | 7 | |a Aluminium oxide |2 Elsevier | |
650 | 7 | |a Aluminium target |2 Elsevier | |
650 | 7 | |a AMS |2 Elsevier | |
650 | 7 | |a Aluminium nitride |2 Elsevier | |
650 | 7 | |a Ionization yield |2 Elsevier | |
700 | 1 | |a Ješkovský, Miroslav |4 oth | |
700 | 1 | |a Kaizer, Jakub |4 oth | |
700 | 1 | |a Steier, Peter |4 oth | |
700 | 1 | |a Zeman, Jakub |4 oth | |
700 | 1 | |a Povinec, Pavel P. |4 oth | |
773 | 0 | 8 | |i Enthalten in |n Elsevier |a Unwala, Darius J. ELSEVIER |t Editorial Comment |d 2013 |d a journal on accelerators, instrumentation and techniques applied to research in nuclear and atomic physics, materials science and related fields in physics |g Amsterdam [u.a.] |w (DE-627)ELV011304669 |
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856 | 4 | 0 | |u https://doi.org/10.1016/j.nimb.2018.07.013 |3 Volltext |
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10.1016/j.nimb.2018.07.013 doi GBV00000000000440.pica (DE-627)ELV045091323 (ELSEVIER)S0168-583X(18)30426-9 DE-627 ger DE-627 rakwb eng 610 VZ 610 VZ 44.85 bkl Pánik, Ján verfasserin aut Investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>Al 2019transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Aluminium oxide Elsevier Aluminium target Elsevier AMS Elsevier Aluminium nitride Elsevier Ionization yield Elsevier Ješkovský, Miroslav oth Kaizer, Jakub oth Steier, Peter oth Zeman, Jakub oth Povinec, Pavel P. oth Enthalten in Elsevier Unwala, Darius J. ELSEVIER Editorial Comment 2013 a journal on accelerators, instrumentation and techniques applied to research in nuclear and atomic physics, materials science and related fields in physics Amsterdam [u.a.] (DE-627)ELV011304669 volume:438 year:2019 day:1 month:01 pages:101-106 extent:6 https://doi.org/10.1016/j.nimb.2018.07.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_40 GBV_ILN_62 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 44.85 Kardiologie Angiologie VZ AR 438 2019 1 0101 101-106 6 |
spelling |
10.1016/j.nimb.2018.07.013 doi GBV00000000000440.pica (DE-627)ELV045091323 (ELSEVIER)S0168-583X(18)30426-9 DE-627 ger DE-627 rakwb eng 610 VZ 610 VZ 44.85 bkl Pánik, Ján verfasserin aut Investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>Al 2019transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Aluminium oxide Elsevier Aluminium target Elsevier AMS Elsevier Aluminium nitride Elsevier Ionization yield Elsevier Ješkovský, Miroslav oth Kaizer, Jakub oth Steier, Peter oth Zeman, Jakub oth Povinec, Pavel P. oth Enthalten in Elsevier Unwala, Darius J. ELSEVIER Editorial Comment 2013 a journal on accelerators, instrumentation and techniques applied to research in nuclear and atomic physics, materials science and related fields in physics Amsterdam [u.a.] (DE-627)ELV011304669 volume:438 year:2019 day:1 month:01 pages:101-106 extent:6 https://doi.org/10.1016/j.nimb.2018.07.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_40 GBV_ILN_62 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 44.85 Kardiologie Angiologie VZ AR 438 2019 1 0101 101-106 6 |
allfields_unstemmed |
10.1016/j.nimb.2018.07.013 doi GBV00000000000440.pica (DE-627)ELV045091323 (ELSEVIER)S0168-583X(18)30426-9 DE-627 ger DE-627 rakwb eng 610 VZ 610 VZ 44.85 bkl Pánik, Ján verfasserin aut Investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>Al 2019transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Aluminium oxide Elsevier Aluminium target Elsevier AMS Elsevier Aluminium nitride Elsevier Ionization yield Elsevier Ješkovský, Miroslav oth Kaizer, Jakub oth Steier, Peter oth Zeman, Jakub oth Povinec, Pavel P. oth Enthalten in Elsevier Unwala, Darius J. ELSEVIER Editorial Comment 2013 a journal on accelerators, instrumentation and techniques applied to research in nuclear and atomic physics, materials science and related fields in physics Amsterdam [u.a.] (DE-627)ELV011304669 volume:438 year:2019 day:1 month:01 pages:101-106 extent:6 https://doi.org/10.1016/j.nimb.2018.07.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_40 GBV_ILN_62 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 44.85 Kardiologie Angiologie VZ AR 438 2019 1 0101 101-106 6 |
allfieldsGer |
10.1016/j.nimb.2018.07.013 doi GBV00000000000440.pica (DE-627)ELV045091323 (ELSEVIER)S0168-583X(18)30426-9 DE-627 ger DE-627 rakwb eng 610 VZ 610 VZ 44.85 bkl Pánik, Ján verfasserin aut Investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>Al 2019transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Aluminium oxide Elsevier Aluminium target Elsevier AMS Elsevier Aluminium nitride Elsevier Ionization yield Elsevier Ješkovský, Miroslav oth Kaizer, Jakub oth Steier, Peter oth Zeman, Jakub oth Povinec, Pavel P. oth Enthalten in Elsevier Unwala, Darius J. ELSEVIER Editorial Comment 2013 a journal on accelerators, instrumentation and techniques applied to research in nuclear and atomic physics, materials science and related fields in physics Amsterdam [u.a.] (DE-627)ELV011304669 volume:438 year:2019 day:1 month:01 pages:101-106 extent:6 https://doi.org/10.1016/j.nimb.2018.07.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_40 GBV_ILN_62 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 44.85 Kardiologie Angiologie VZ AR 438 2019 1 0101 101-106 6 |
allfieldsSound |
10.1016/j.nimb.2018.07.013 doi GBV00000000000440.pica (DE-627)ELV045091323 (ELSEVIER)S0168-583X(18)30426-9 DE-627 ger DE-627 rakwb eng 610 VZ 610 VZ 44.85 bkl Pánik, Ján verfasserin aut Investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>Al 2019transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. Aluminium oxide Elsevier Aluminium target Elsevier AMS Elsevier Aluminium nitride Elsevier Ionization yield Elsevier Ješkovský, Miroslav oth Kaizer, Jakub oth Steier, Peter oth Zeman, Jakub oth Povinec, Pavel P. oth Enthalten in Elsevier Unwala, Darius J. ELSEVIER Editorial Comment 2013 a journal on accelerators, instrumentation and techniques applied to research in nuclear and atomic physics, materials science and related fields in physics Amsterdam [u.a.] (DE-627)ELV011304669 volume:438 year:2019 day:1 month:01 pages:101-106 extent:6 https://doi.org/10.1016/j.nimb.2018.07.013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_21 GBV_ILN_22 GBV_ILN_24 GBV_ILN_40 GBV_ILN_62 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2005 GBV_ILN_2007 44.85 Kardiologie Angiologie VZ AR 438 2019 1 0101 101-106 6 |
language |
English |
source |
Enthalten in Editorial Comment Amsterdam [u.a.] volume:438 year:2019 day:1 month:01 pages:101-106 extent:6 |
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investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>al |
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Investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>Al |
abstract |
Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. |
abstractGer |
Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. |
abstract_unstemmed |
Accelerator Mass Spectrometry (AMS) has been a frequently used technique for analysis of low-level concentrations of 26Al in environmental, biological and space samples with detection limits down to 0.01 fg. Al2O3 targets have been mostly used in ion sources for the production of aluminium negative ions because of high-temperature stability, non-toxicity, in-air stability, and relatively easy production procedures. It is well known, however, that aluminium does not yield as intense negative ion beams as other elements used in tandem AMS accelerators. An alternative solution could be to use as the target material AlN, which can yield higher Al− currents. On the other hand, the AlN targets are more difficult to synthesize, and they decompose with water in the air to form Al(OH)3 and ammonia. Commercially available compounds of Al2O3 and AlN were mixed with copper, silver and iron high-purity powders and sputtered in a MC-SNICS ion source for studying ionization yields. Since the production of magnesium and nitrogen negative ions is negligible, a production of MgN− molecules has been questionable. Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. The AMS measurements of 26Al using AlN− as injected ions from the AlN matrix, similar to AlO− ions from Al2O3 matrix, have shown that further isobar suppression due to a high 26Mg3+ production rate will be needed. |
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title_short |
Investigation of suitable targets for accelerator mass spectrometry of <ce:sup loc="pre">26</ce:sup>Al |
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Obtained results indicate that the aluminium nitride matrix could be a suitable material for AMS measurements as the production of 27Al− is higher by a factor of 1.8 from the aluminium oxide matrix, while aluminium sulphate and aluminium fluoride showed a very low sputtering efficiency. The formation probability of the MgN− was tested using AlN and Mg3N2 matrices. 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