Label-free electrochemical immunosensor for insulin detection by high-efficiency synergy strategy of Pd NPs3D MoSx towards H2O2
Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Gao, Zengqiang [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2019transfer abstract |
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| Schlagwörter: |
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| Umfang: |
7 |
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| Übergeordnetes Werk: |
Enthalten in: Vertical differentiation via multi-tier geographical indications and the consumer perception of quality: The case of Chianti wines - Costanigro, Marco ELSEVIER, 2019, the principal international journal devoted to research, design development and application of biosensors and bioelectronics, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:126 ; year:2019 ; day:1 ; month:02 ; pages:108-114 ; extent:7 |
| Links: |
|---|
| DOI / URN: |
10.1016/j.bios.2018.10.017 |
|---|
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ELV045372063 |
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| 245 | 1 | 0 | |a Label-free electrochemical immunosensor for insulin detection by high-efficiency synergy strategy of Pd NPs3D MoSx towards H2O2 |
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| 520 | |a Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. | ||
| 520 | |a Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. | ||
| 650 | 7 | |a Pd NPs |2 Elsevier | |
| 650 | 7 | |a Electrochemical label-free immunosensor |2 Elsevier | |
| 650 | 7 | |a Amorphous MoSx |2 Elsevier | |
| 650 | 7 | |a Insulin |2 Elsevier | |
| 650 | 7 | |a CTAB |2 Elsevier | |
| 700 | 1 | |a Li, Yueyun |4 oth | |
| 700 | 1 | |a Zhang, Chunyan |4 oth | |
| 700 | 1 | |a Zhang, Shuan |4 oth | |
| 700 | 1 | |a Li, Faying |4 oth | |
| 700 | 1 | |a Wang, Ping |4 oth | |
| 700 | 1 | |a Wang, Huan |4 oth | |
| 700 | 1 | |a Wei, Qin |4 oth | |
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10.1016/j.bios.2018.10.017 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001263.pica (DE-627)ELV045372063 (ELSEVIER)S0956-5663(18)30822-4 DE-627 ger DE-627 rakwb eng 630 640 VZ 49.00 bkl Gao, Zengqiang verfasserin aut Label-free electrochemical immunosensor for insulin detection by high-efficiency synergy strategy of Pd NPs3D MoSx towards H2O2 2019transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Pd NPs Elsevier Electrochemical label-free immunosensor Elsevier Amorphous MoSx Elsevier Insulin Elsevier CTAB Elsevier Li, Yueyun oth Zhang, Chunyan oth Zhang, Shuan oth Li, Faying oth Wang, Ping oth Wang, Huan oth Wei, Qin oth Enthalten in Elsevier Science Costanigro, Marco ELSEVIER Vertical differentiation via multi-tier geographical indications and the consumer perception of quality: The case of Chianti wines 2019 the principal international journal devoted to research, design development and application of biosensors and bioelectronics Amsterdam [u.a.] (DE-627)ELV001931067 volume:126 year:2019 day:1 month:02 pages:108-114 extent:7 https://doi.org/10.1016/j.bios.2018.10.017 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 49.00 Hauswirtschaft: Allgemeines VZ AR 126 2019 1 0201 108-114 7 |
| spelling |
10.1016/j.bios.2018.10.017 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001263.pica (DE-627)ELV045372063 (ELSEVIER)S0956-5663(18)30822-4 DE-627 ger DE-627 rakwb eng 630 640 VZ 49.00 bkl Gao, Zengqiang verfasserin aut Label-free electrochemical immunosensor for insulin detection by high-efficiency synergy strategy of Pd NPs3D MoSx towards H2O2 2019transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Pd NPs Elsevier Electrochemical label-free immunosensor Elsevier Amorphous MoSx Elsevier Insulin Elsevier CTAB Elsevier Li, Yueyun oth Zhang, Chunyan oth Zhang, Shuan oth Li, Faying oth Wang, Ping oth Wang, Huan oth Wei, Qin oth Enthalten in Elsevier Science Costanigro, Marco ELSEVIER Vertical differentiation via multi-tier geographical indications and the consumer perception of quality: The case of Chianti wines 2019 the principal international journal devoted to research, design development and application of biosensors and bioelectronics Amsterdam [u.a.] (DE-627)ELV001931067 volume:126 year:2019 day:1 month:02 pages:108-114 extent:7 https://doi.org/10.1016/j.bios.2018.10.017 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 49.00 Hauswirtschaft: Allgemeines VZ AR 126 2019 1 0201 108-114 7 |
| allfields_unstemmed |
10.1016/j.bios.2018.10.017 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001263.pica (DE-627)ELV045372063 (ELSEVIER)S0956-5663(18)30822-4 DE-627 ger DE-627 rakwb eng 630 640 VZ 49.00 bkl Gao, Zengqiang verfasserin aut Label-free electrochemical immunosensor for insulin detection by high-efficiency synergy strategy of Pd NPs3D MoSx towards H2O2 2019transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Pd NPs Elsevier Electrochemical label-free immunosensor Elsevier Amorphous MoSx Elsevier Insulin Elsevier CTAB Elsevier Li, Yueyun oth Zhang, Chunyan oth Zhang, Shuan oth Li, Faying oth Wang, Ping oth Wang, Huan oth Wei, Qin oth Enthalten in Elsevier Science Costanigro, Marco ELSEVIER Vertical differentiation via multi-tier geographical indications and the consumer perception of quality: The case of Chianti wines 2019 the principal international journal devoted to research, design development and application of biosensors and bioelectronics Amsterdam [u.a.] (DE-627)ELV001931067 volume:126 year:2019 day:1 month:02 pages:108-114 extent:7 https://doi.org/10.1016/j.bios.2018.10.017 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 49.00 Hauswirtschaft: Allgemeines VZ AR 126 2019 1 0201 108-114 7 |
| allfieldsGer |
10.1016/j.bios.2018.10.017 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001263.pica (DE-627)ELV045372063 (ELSEVIER)S0956-5663(18)30822-4 DE-627 ger DE-627 rakwb eng 630 640 VZ 49.00 bkl Gao, Zengqiang verfasserin aut Label-free electrochemical immunosensor for insulin detection by high-efficiency synergy strategy of Pd NPs3D MoSx towards H2O2 2019transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Pd NPs Elsevier Electrochemical label-free immunosensor Elsevier Amorphous MoSx Elsevier Insulin Elsevier CTAB Elsevier Li, Yueyun oth Zhang, Chunyan oth Zhang, Shuan oth Li, Faying oth Wang, Ping oth Wang, Huan oth Wei, Qin oth Enthalten in Elsevier Science Costanigro, Marco ELSEVIER Vertical differentiation via multi-tier geographical indications and the consumer perception of quality: The case of Chianti wines 2019 the principal international journal devoted to research, design development and application of biosensors and bioelectronics Amsterdam [u.a.] (DE-627)ELV001931067 volume:126 year:2019 day:1 month:02 pages:108-114 extent:7 https://doi.org/10.1016/j.bios.2018.10.017 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 49.00 Hauswirtschaft: Allgemeines VZ AR 126 2019 1 0201 108-114 7 |
| allfieldsSound |
10.1016/j.bios.2018.10.017 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001263.pica (DE-627)ELV045372063 (ELSEVIER)S0956-5663(18)30822-4 DE-627 ger DE-627 rakwb eng 630 640 VZ 49.00 bkl Gao, Zengqiang verfasserin aut Label-free electrochemical immunosensor for insulin detection by high-efficiency synergy strategy of Pd NPs3D MoSx towards H2O2 2019transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. Pd NPs Elsevier Electrochemical label-free immunosensor Elsevier Amorphous MoSx Elsevier Insulin Elsevier CTAB Elsevier Li, Yueyun oth Zhang, Chunyan oth Zhang, Shuan oth Li, Faying oth Wang, Ping oth Wang, Huan oth Wei, Qin oth Enthalten in Elsevier Science Costanigro, Marco ELSEVIER Vertical differentiation via multi-tier geographical indications and the consumer perception of quality: The case of Chianti wines 2019 the principal international journal devoted to research, design development and application of biosensors and bioelectronics Amsterdam [u.a.] (DE-627)ELV001931067 volume:126 year:2019 day:1 month:02 pages:108-114 extent:7 https://doi.org/10.1016/j.bios.2018.10.017 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 49.00 Hauswirtschaft: Allgemeines VZ AR 126 2019 1 0201 108-114 7 |
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Enthalten in Vertical differentiation via multi-tier geographical indications and the consumer perception of quality: The case of Chianti wines Amsterdam [u.a.] volume:126 year:2019 day:1 month:02 pages:108-114 extent:7 |
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Enthalten in Vertical differentiation via multi-tier geographical indications and the consumer perception of quality: The case of Chianti wines Amsterdam [u.a.] volume:126 year:2019 day:1 month:02 pages:108-114 extent:7 |
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Vertical differentiation via multi-tier geographical indications and the consumer perception of quality: The case of Chianti wines |
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Gao, Zengqiang @@aut@@ Li, Yueyun @@oth@@ Zhang, Chunyan @@oth@@ Zhang, Shuan @@oth@@ Li, Faying @@oth@@ Wang, Ping @@oth@@ Wang, Huan @@oth@@ Wei, Qin @@oth@@ |
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Label-free electrochemical immunosensor for insulin detection by high-efficiency synergy strategy of Pd NPs3D MoSx towards H2O2 |
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Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. |
| abstractGer |
Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. |
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Here, a novel H2O2-based electrochemical immunosensor utilizing Pd nanoparticles functionalized three-dimensional wrinkly amorphous MoSx composites (Pd NPs3D MoSx) as the platform was developed for the determination of insulin. In this work, Pd NPs@3D MoSx prepared in the presence of CTAB possessed an excellent catalytic activity for the reduction of H2O2. Furthermore, Pd NPs@3D MoSx with favorable biological compatibility can conjugate a great many antibodies to capture insulin. Attributed to the excellent property, electrochemical signals could be greatly amplified, contributing to improving detection sensitivity. Especially, SEM, TEM, and XPS information further confirmed nanomaterial's surface morphology and amorphous structure. Under the optimal conditions, the proposed immunosensor exhibited a sensitively linear relation with logarithmic insulin concentrations from 0.01 to 100 ng/mL with a low detection limit of 3.0 pg/mL (S/N = 3). Characterized by good reproducibility, specificity, and stability, the fabricated immunosensor may blaze a path for insulin detection in a real sample. |
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Li, Yueyun Zhang, Chunyan Zhang, Shuan Li, Faying Wang, Ping Wang, Huan Wei, Qin |
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