Non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (Ni<ce:inf loc="post">3</ce:inf>N/NCS) via facile one pot nitridation process
Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with ave...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Chen, Junli [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
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2019transfer abstract |
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| Umfang: |
9 |
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| Übergeordnetes Werk: |
Enthalten in: Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners - Jacobs, Jacquelyn A. ELSEVIER, 2017, JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics, Lausanne |
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| Übergeordnetes Werk: |
volume:797 ; year:2019 ; day:15 ; month:08 ; pages:922-930 ; extent:9 |
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| DOI / URN: |
10.1016/j.jallcom.2019.05.234 |
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ELV047108622 |
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| 245 | 1 | 0 | |a Non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (Ni<ce:inf loc="post">3</ce:inf>N/NCS) via facile one pot nitridation process |
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| 520 | |a Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. | ||
| 520 | |a Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. | ||
| 650 | 7 | |a Nickel nitride |2 Elsevier | |
| 650 | 7 | |a Carbon spheres |2 Elsevier | |
| 650 | 7 | |a Glucose sensor |2 Elsevier | |
| 650 | 7 | |a Nitrogen doping |2 Elsevier | |
| 650 | 7 | |a Non-enzymatic |2 Elsevier | |
| 700 | 1 | |a Yin, Haoyong |4 oth | |
| 700 | 1 | |a Zhou, Jielin |4 oth | |
| 700 | 1 | |a Gong, Jianying |4 oth | |
| 700 | 1 | |a Wang, Ling |4 oth | |
| 700 | 1 | |a Zheng, Yifan |4 oth | |
| 700 | 1 | |a Nie, Qiulin |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier |a Jacobs, Jacquelyn A. ELSEVIER |t Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners |d 2017 |d JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics |g Lausanne |w (DE-627)ELV001115774 |
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10.1016/j.jallcom.2019.05.234 doi GBV00000000000653.pica (DE-627)ELV047108622 (ELSEVIER)S0925-8388(19)31916-4 DE-627 ger DE-627 rakwb eng 630 VZ Chen, Junli verfasserin aut Non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (Ni<ce:inf loc="post">3</ce:inf>N/NCS) via facile one pot nitridation process 2019transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Non-enzymatic Elsevier Yin, Haoyong oth Zhou, Jielin oth Gong, Jianying oth Wang, Ling oth Zheng, Yifan oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:797 year:2019 day:15 month:08 pages:922-930 extent:9 https://doi.org/10.1016/j.jallcom.2019.05.234 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 797 2019 15 0815 922-930 9 |
| spelling |
10.1016/j.jallcom.2019.05.234 doi GBV00000000000653.pica (DE-627)ELV047108622 (ELSEVIER)S0925-8388(19)31916-4 DE-627 ger DE-627 rakwb eng 630 VZ Chen, Junli verfasserin aut Non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (Ni<ce:inf loc="post">3</ce:inf>N/NCS) via facile one pot nitridation process 2019transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Non-enzymatic Elsevier Yin, Haoyong oth Zhou, Jielin oth Gong, Jianying oth Wang, Ling oth Zheng, Yifan oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:797 year:2019 day:15 month:08 pages:922-930 extent:9 https://doi.org/10.1016/j.jallcom.2019.05.234 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 797 2019 15 0815 922-930 9 |
| allfields_unstemmed |
10.1016/j.jallcom.2019.05.234 doi GBV00000000000653.pica (DE-627)ELV047108622 (ELSEVIER)S0925-8388(19)31916-4 DE-627 ger DE-627 rakwb eng 630 VZ Chen, Junli verfasserin aut Non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (Ni<ce:inf loc="post">3</ce:inf>N/NCS) via facile one pot nitridation process 2019transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Non-enzymatic Elsevier Yin, Haoyong oth Zhou, Jielin oth Gong, Jianying oth Wang, Ling oth Zheng, Yifan oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:797 year:2019 day:15 month:08 pages:922-930 extent:9 https://doi.org/10.1016/j.jallcom.2019.05.234 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 797 2019 15 0815 922-930 9 |
| allfieldsGer |
10.1016/j.jallcom.2019.05.234 doi GBV00000000000653.pica (DE-627)ELV047108622 (ELSEVIER)S0925-8388(19)31916-4 DE-627 ger DE-627 rakwb eng 630 VZ Chen, Junli verfasserin aut Non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (Ni<ce:inf loc="post">3</ce:inf>N/NCS) via facile one pot nitridation process 2019transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Non-enzymatic Elsevier Yin, Haoyong oth Zhou, Jielin oth Gong, Jianying oth Wang, Ling oth Zheng, Yifan oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:797 year:2019 day:15 month:08 pages:922-930 extent:9 https://doi.org/10.1016/j.jallcom.2019.05.234 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 797 2019 15 0815 922-930 9 |
| allfieldsSound |
10.1016/j.jallcom.2019.05.234 doi GBV00000000000653.pica (DE-627)ELV047108622 (ELSEVIER)S0925-8388(19)31916-4 DE-627 ger DE-627 rakwb eng 630 VZ Chen, Junli verfasserin aut Non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (Ni<ce:inf loc="post">3</ce:inf>N/NCS) via facile one pot nitridation process 2019transfer abstract 9 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. Nickel nitride Elsevier Carbon spheres Elsevier Glucose sensor Elsevier Nitrogen doping Elsevier Non-enzymatic Elsevier Yin, Haoyong oth Zhou, Jielin oth Gong, Jianying oth Wang, Ling oth Zheng, Yifan oth Nie, Qiulin oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:797 year:2019 day:15 month:08 pages:922-930 extent:9 https://doi.org/10.1016/j.jallcom.2019.05.234 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 797 2019 15 0815 922-930 9 |
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non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (ni<ce:inf loc="post">3</ce:inf>n/ncs) via facile one pot nitridation process |
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Non-enzymatic glucose sensor based on nickel nitride decorated nitrogen doped carbon spheres (Ni<ce:inf loc="post">3</ce:inf>N/NCS) via facile one pot nitridation process |
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Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. |
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Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. |
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Nickel nitride decorated nitrogen doped carbon spheres (Ni3N/NCS) were synthesized via an eco-friendly one pot nitridation process. The morphology and structure, chemical composition, and electrochemical properties of Ni3N/NCS were characterized vie different methods. The Ni3N nanoparticles with average diameter of 20 nm were uniformly decorated on the surface of nitrogen doped carbon spheres. The constructed Ni3N/NCS sensor exhibited excellent performance for non-enzymatic glucose sensing, which included two wide linear ranges of 1 μM–3000 μM and 3000 μM - 7000 μM with high sensitivity of 2024.18 μAmM−1cm−2 and 1256.98 μAmM−1cm−2. The corresponding detection limits in lower and higher concentration ranges were 0.1 μM and 0.35 μM respectively. The significantly improved electrochemical performance of Ni3N/NCS may be due to the rapid charge transfer and high conductivity of Ni3N/NCS/GCE, originating from the synergistic effect of Ni3N and nitrogen doped carbon spheres. Moreover, the Ni3N/NCS sensor also displayed satisfactory recovery results for glucose detection in serum samples. The kinetics of glucose oxidation on the Ni3N/NCS electrode were also studied to understand the electrochemical reaction on the surface of the materials. Moreover, the possible mechanisms about the glucose sensing and the formation of Ni3N/NCS were also discussed. The present study may provide a rational strategy to eco-friendly prepare highly efficient electrocatalysts for non-enzymatic glucose sensing applications. |
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