Synthetic and structural investigation of ZnO nano-rods, hydrothermally grown over Au coated optical fiber for evanescent field-based detection of aqueous ammonia
Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ra...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Singh, Shailendra Kr [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
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2020transfer abstract |
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| Übergeordnetes Werk: |
Enthalten in: Thermal and mechanical characterization of fly ash geopolymer with aluminium chloride and potassium hydroxide treated hemp shiv lightweight aggregate - Narattha, Chalermphan ELSEVIER, 2022, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:107 ; year:2020 ; day:1 ; month:03 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.mssp.2019.104819 |
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ELV048912336 |
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| 245 | 1 | 0 | |a Synthetic and structural investigation of ZnO nano-rods, hydrothermally grown over Au coated optical fiber for evanescent field-based detection of aqueous ammonia |
| 264 | 1 | |c 2020transfer abstract | |
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| 520 | |a Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. | ||
| 520 | |a Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. | ||
| 650 | 7 | |a Material characterization |2 Elsevier | |
| 650 | 7 | |a Hydrothermal synthesis |2 Elsevier | |
| 650 | 7 | |a Ammonia sensing |2 Elsevier | |
| 650 | 7 | |a Fiber optic sensor |2 Elsevier | |
| 650 | 7 | |a Gold coating |2 Elsevier | |
| 650 | 7 | |a ZnO hexagonal nanorod |2 Elsevier | |
| 700 | 1 | |a Dutta, Debjit |4 oth | |
| 700 | 1 | |a Das, Shyamal |4 oth | |
| 700 | 1 | |a Dhar, Anirban |4 oth | |
| 700 | 1 | |a Paul, M.C. |4 oth | |
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10.1016/j.mssp.2019.104819 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000000854.pica (DE-627)ELV048912336 (ELSEVIER)S1369-8001(19)31313-7 DE-627 ger DE-627 rakwb eng 690 VZ 56.45 bkl Singh, Shailendra Kr verfasserin aut Synthetic and structural investigation of ZnO nano-rods, hydrothermally grown over Au coated optical fiber for evanescent field-based detection of aqueous ammonia 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Material characterization Elsevier Hydrothermal synthesis Elsevier Ammonia sensing Elsevier Fiber optic sensor Elsevier Gold coating Elsevier ZnO hexagonal nanorod Elsevier Dutta, Debjit oth Das, Shyamal oth Dhar, Anirban oth Paul, M.C. oth Enthalten in Elsevier Science Narattha, Chalermphan ELSEVIER Thermal and mechanical characterization of fly ash geopolymer with aluminium chloride and potassium hydroxide treated hemp shiv lightweight aggregate 2022 Amsterdam [u.a.] (DE-627)ELV007709056 volume:107 year:2020 day:1 month:03 pages:0 https://doi.org/10.1016/j.mssp.2019.104819 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 56.45 Baustoffkunde VZ AR 107 2020 1 0301 0 |
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10.1016/j.mssp.2019.104819 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000000854.pica (DE-627)ELV048912336 (ELSEVIER)S1369-8001(19)31313-7 DE-627 ger DE-627 rakwb eng 690 VZ 56.45 bkl Singh, Shailendra Kr verfasserin aut Synthetic and structural investigation of ZnO nano-rods, hydrothermally grown over Au coated optical fiber for evanescent field-based detection of aqueous ammonia 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Material characterization Elsevier Hydrothermal synthesis Elsevier Ammonia sensing Elsevier Fiber optic sensor Elsevier Gold coating Elsevier ZnO hexagonal nanorod Elsevier Dutta, Debjit oth Das, Shyamal oth Dhar, Anirban oth Paul, M.C. oth Enthalten in Elsevier Science Narattha, Chalermphan ELSEVIER Thermal and mechanical characterization of fly ash geopolymer with aluminium chloride and potassium hydroxide treated hemp shiv lightweight aggregate 2022 Amsterdam [u.a.] (DE-627)ELV007709056 volume:107 year:2020 day:1 month:03 pages:0 https://doi.org/10.1016/j.mssp.2019.104819 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 56.45 Baustoffkunde VZ AR 107 2020 1 0301 0 |
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10.1016/j.mssp.2019.104819 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000000854.pica (DE-627)ELV048912336 (ELSEVIER)S1369-8001(19)31313-7 DE-627 ger DE-627 rakwb eng 690 VZ 56.45 bkl Singh, Shailendra Kr verfasserin aut Synthetic and structural investigation of ZnO nano-rods, hydrothermally grown over Au coated optical fiber for evanescent field-based detection of aqueous ammonia 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Material characterization Elsevier Hydrothermal synthesis Elsevier Ammonia sensing Elsevier Fiber optic sensor Elsevier Gold coating Elsevier ZnO hexagonal nanorod Elsevier Dutta, Debjit oth Das, Shyamal oth Dhar, Anirban oth Paul, M.C. oth Enthalten in Elsevier Science Narattha, Chalermphan ELSEVIER Thermal and mechanical characterization of fly ash geopolymer with aluminium chloride and potassium hydroxide treated hemp shiv lightweight aggregate 2022 Amsterdam [u.a.] (DE-627)ELV007709056 volume:107 year:2020 day:1 month:03 pages:0 https://doi.org/10.1016/j.mssp.2019.104819 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 56.45 Baustoffkunde VZ AR 107 2020 1 0301 0 |
| allfieldsGer |
10.1016/j.mssp.2019.104819 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000000854.pica (DE-627)ELV048912336 (ELSEVIER)S1369-8001(19)31313-7 DE-627 ger DE-627 rakwb eng 690 VZ 56.45 bkl Singh, Shailendra Kr verfasserin aut Synthetic and structural investigation of ZnO nano-rods, hydrothermally grown over Au coated optical fiber for evanescent field-based detection of aqueous ammonia 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Material characterization Elsevier Hydrothermal synthesis Elsevier Ammonia sensing Elsevier Fiber optic sensor Elsevier Gold coating Elsevier ZnO hexagonal nanorod Elsevier Dutta, Debjit oth Das, Shyamal oth Dhar, Anirban oth Paul, M.C. oth Enthalten in Elsevier Science Narattha, Chalermphan ELSEVIER Thermal and mechanical characterization of fly ash geopolymer with aluminium chloride and potassium hydroxide treated hemp shiv lightweight aggregate 2022 Amsterdam [u.a.] (DE-627)ELV007709056 volume:107 year:2020 day:1 month:03 pages:0 https://doi.org/10.1016/j.mssp.2019.104819 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 56.45 Baustoffkunde VZ AR 107 2020 1 0301 0 |
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10.1016/j.mssp.2019.104819 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000000854.pica (DE-627)ELV048912336 (ELSEVIER)S1369-8001(19)31313-7 DE-627 ger DE-627 rakwb eng 690 VZ 56.45 bkl Singh, Shailendra Kr verfasserin aut Synthetic and structural investigation of ZnO nano-rods, hydrothermally grown over Au coated optical fiber for evanescent field-based detection of aqueous ammonia 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. Material characterization Elsevier Hydrothermal synthesis Elsevier Ammonia sensing Elsevier Fiber optic sensor Elsevier Gold coating Elsevier ZnO hexagonal nanorod Elsevier Dutta, Debjit oth Das, Shyamal oth Dhar, Anirban oth Paul, M.C. oth Enthalten in Elsevier Science Narattha, Chalermphan ELSEVIER Thermal and mechanical characterization of fly ash geopolymer with aluminium chloride and potassium hydroxide treated hemp shiv lightweight aggregate 2022 Amsterdam [u.a.] (DE-627)ELV007709056 volume:107 year:2020 day:1 month:03 pages:0 https://doi.org/10.1016/j.mssp.2019.104819 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 56.45 Baustoffkunde VZ AR 107 2020 1 0301 0 |
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Enthalten in Thermal and mechanical characterization of fly ash geopolymer with aluminium chloride and potassium hydroxide treated hemp shiv lightweight aggregate Amsterdam [u.a.] volume:107 year:2020 day:1 month:03 pages:0 |
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Thermal and mechanical characterization of fly ash geopolymer with aluminium chloride and potassium hydroxide treated hemp shiv lightweight aggregate |
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Synthetic and structural investigation of ZnO nano-rods, hydrothermally grown over Au coated optical fiber for evanescent field-based detection of aqueous ammonia |
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Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. |
| abstractGer |
Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. |
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Fabrication of modified clad optical fiber consisting of ZnO-nanorod deposited over a thin film of gold (Au), employing hydrothermal technique within an autoclave is presented. The deposited ZnO material was analyzed using X-Ray Diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, Photoluminescence (PL) spectra, Thermogravimetric analysis (TGA), Differential thermal analysis (DTA), Brunauer Emmett Teller (BET) and Field Emission Scanning Electron Microscope (FESEM) which confirms the ZnO hexagonal nimrod formation in as-synthesized material. The developed sensor was tested with ethanol, ammonia, acetone, and 2-propanol to measure the selectivity of the sensor. The response time, as well as recovery time of ZnO doped fiber-based sensor with and without Au coating, was measured 25 s, 360 s and 30 s, 240 s respectively. This ZnO-nanorod coated modified clad optical fiber exhibit good sensing performance towards ammonium ions in aqueous solution with improved sensitivity (%) ∼ 0.638 compared to pure ZnO doped modified clad optical fiber at room temperature. |
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Synthetic and structural investigation of ZnO nano-rods, hydrothermally grown over Au coated optical fiber for evanescent field-based detection of aqueous ammonia |
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