Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties
Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) str...
Ausführliche Beschreibung
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| Autor*in: |
Basilio, L.A.L. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2020transfer abstract |
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| Umfang: |
6 |
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| Übergeordnetes Werk: |
Enthalten in: Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration - Rey, F. ELSEVIER, 2018, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:46 ; year:2020 ; number:15 ; day:15 ; month:10 ; pages:23834-23839 ; extent:6 |
| Links: |
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| DOI / URN: |
10.1016/j.ceramint.2020.06.160 |
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ELV051105233 |
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| 245 | 1 | 0 | |a Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties |
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| 520 | |a Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. | ||
| 520 | |a Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. | ||
| 650 | 7 | |a Na2Ti3O7/Na2Ti6O13 |2 Elsevier | |
| 650 | 7 | |a dc conductivity |2 Elsevier | |
| 650 | 7 | |a Microwave synthesis |2 Elsevier | |
| 700 | 1 | |a Xavier, F. |4 oth | |
| 700 | 1 | |a Sales, J.C.C. |4 oth | |
| 700 | 1 | |a Andrade, J.C.S. |4 oth | |
| 700 | 1 | |a Anglada- Rivera, J. |4 oth | |
| 700 | 1 | |a Aguilera, L. |4 oth | |
| 700 | 1 | |a Silva, R.S. |4 oth | |
| 700 | 1 | |a Rodriguez-Hernandez, J. |4 oth | |
| 700 | 1 | |a Pérez de la Cruz, J. |4 oth | |
| 700 | 1 | |a Leyet, Y. |4 oth | |
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10.1016/j.ceramint.2020.06.160 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001109.pica (DE-627)ELV051105233 (ELSEVIER)S0272-8842(20)31819-8 DE-627 ger DE-627 rakwb eng 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Basilio, L.A.L. verfasserin aut Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties 2020transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Na2Ti3O7/Na2Ti6O13 Elsevier dc conductivity Elsevier Microwave synthesis Elsevier Xavier, F. oth Sales, J.C.C. oth Andrade, J.C.S. oth Anglada- Rivera, J. oth Aguilera, L. oth Silva, R.S. oth Rodriguez-Hernandez, J. oth Pérez de la Cruz, J. oth Leyet, Y. oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:46 year:2020 number:15 day:15 month:10 pages:23834-23839 extent:6 https://doi.org/10.1016/j.ceramint.2020.06.160 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 46 2020 15 15 1015 23834-23839 6 |
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10.1016/j.ceramint.2020.06.160 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001109.pica (DE-627)ELV051105233 (ELSEVIER)S0272-8842(20)31819-8 DE-627 ger DE-627 rakwb eng 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Basilio, L.A.L. verfasserin aut Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties 2020transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Na2Ti3O7/Na2Ti6O13 Elsevier dc conductivity Elsevier Microwave synthesis Elsevier Xavier, F. oth Sales, J.C.C. oth Andrade, J.C.S. oth Anglada- Rivera, J. oth Aguilera, L. oth Silva, R.S. oth Rodriguez-Hernandez, J. oth Pérez de la Cruz, J. oth Leyet, Y. oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:46 year:2020 number:15 day:15 month:10 pages:23834-23839 extent:6 https://doi.org/10.1016/j.ceramint.2020.06.160 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 46 2020 15 15 1015 23834-23839 6 |
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10.1016/j.ceramint.2020.06.160 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001109.pica (DE-627)ELV051105233 (ELSEVIER)S0272-8842(20)31819-8 DE-627 ger DE-627 rakwb eng 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Basilio, L.A.L. verfasserin aut Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties 2020transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Na2Ti3O7/Na2Ti6O13 Elsevier dc conductivity Elsevier Microwave synthesis Elsevier Xavier, F. oth Sales, J.C.C. oth Andrade, J.C.S. oth Anglada- Rivera, J. oth Aguilera, L. oth Silva, R.S. oth Rodriguez-Hernandez, J. oth Pérez de la Cruz, J. oth Leyet, Y. oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:46 year:2020 number:15 day:15 month:10 pages:23834-23839 extent:6 https://doi.org/10.1016/j.ceramint.2020.06.160 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 46 2020 15 15 1015 23834-23839 6 |
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10.1016/j.ceramint.2020.06.160 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001109.pica (DE-627)ELV051105233 (ELSEVIER)S0272-8842(20)31819-8 DE-627 ger DE-627 rakwb eng 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Basilio, L.A.L. verfasserin aut Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties 2020transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Na2Ti3O7/Na2Ti6O13 Elsevier dc conductivity Elsevier Microwave synthesis Elsevier Xavier, F. oth Sales, J.C.C. oth Andrade, J.C.S. oth Anglada- Rivera, J. oth Aguilera, L. oth Silva, R.S. oth Rodriguez-Hernandez, J. oth Pérez de la Cruz, J. oth Leyet, Y. oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:46 year:2020 number:15 day:15 month:10 pages:23834-23839 extent:6 https://doi.org/10.1016/j.ceramint.2020.06.160 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 46 2020 15 15 1015 23834-23839 6 |
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10.1016/j.ceramint.2020.06.160 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001109.pica (DE-627)ELV051105233 (ELSEVIER)S0272-8842(20)31819-8 DE-627 ger DE-627 rakwb eng 333.7 610 VZ 43.12 bkl 43.13 bkl 44.13 bkl Basilio, L.A.L. verfasserin aut Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties 2020transfer abstract 6 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. Na2Ti3O7/Na2Ti6O13 Elsevier dc conductivity Elsevier Microwave synthesis Elsevier Xavier, F. oth Sales, J.C.C. oth Andrade, J.C.S. oth Anglada- Rivera, J. oth Aguilera, L. oth Silva, R.S. oth Rodriguez-Hernandez, J. oth Pérez de la Cruz, J. oth Leyet, Y. oth Enthalten in Elsevier Science Rey, F. ELSEVIER Soil and water bioengineering: Practice and research needs for reconciling natural hazard control and ecological restoration 2018 Amsterdam [u.a.] (DE-627)ELV000899798 volume:46 year:2020 number:15 day:15 month:10 pages:23834-23839 extent:6 https://doi.org/10.1016/j.ceramint.2020.06.160 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA SSG-OPC-GGO 43.12 Umweltchemie VZ 43.13 Umwelttoxikologie VZ 44.13 Medizinische Ökologie VZ AR 46 2020 15 15 1015 23834-23839 6 |
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fast synthesis of na2ti3o7 system synthesized by microwave-assisted hydrothermal method: electrical properties |
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Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties |
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Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. |
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Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. |
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Sodium titanate Na2TinO2n+1 (2 ≤ n ≤ 9) is a well-known semiconductor that exhibits interesting electrical properties allowing numerous applications, such as: electrodes for solid-state batteries. In this work, we reported a novel, fast and simple route to produce sodium titanate (Na2Ti3O7 - NT) structures at low temperature and short time, by using microwave-assisted hydrothermal method. The NT powder synthesis was performed at 200 °C for 1 h and 4 h. Afterward, the as-synthetized powders were sintered to 900 °C for 1 h. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and complex impedance spectroscopy. It was identified a phase mixture of the polymorphs Na2Ti3O7 and Na2Ti6O13 with elongated rod-like morphology. Both samples showed a majority Na2Ti3O7 (≥95%) crystalline phase, as confirmed by Rietveld refinement. After ceramics sintering the total dc conductivity values between of 10-6 S/cm and 10-7 S/cm were achieved. |
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Fast synthesis of Na2Ti3O7 system synthesized by microwave-assisted hydrothermal method: Electrical properties |
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