Eco-friendly solvents and their mixture for the fabrication of polysulfone ultrafiltration membranes: An investigation of doctor blade and slot die casting methods
Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as R...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Dong, Xiaobo [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2020transfer abstract |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Steering charge kinetics in W - Yue, Xin-Zheng ELSEVIER, 2019, the official journal of the North American Membrane Society, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:614 ; year:2020 ; day:15 ; month:11 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.memsci.2020.118510 |
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| 520 | |a Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. | ||
| 520 | |a Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. | ||
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| 650 | 7 | |a Polymeric membranes |2 Elsevier | |
| 650 | 7 | |a Eco-friendly solvents |2 Elsevier | |
| 650 | 7 | |a Scale-up study |2 Elsevier | |
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| 700 | 1 | |a Grulke, Eric |4 oth | |
| 700 | 1 | |a Harris, Tequila |4 oth | |
| 700 | 1 | |a Escobar, Isabel C. |4 oth | |
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10.1016/j.memsci.2020.118510 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001118.pica (DE-627)ELV051216787 (ELSEVIER)S0376-7388(20)31087-5 DE-627 ger DE-627 rakwb eng 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Dong, Xiaobo verfasserin aut Eco-friendly solvents and their mixture for the fabrication of polysulfone ultrafiltration membranes: An investigation of doctor blade and slot die casting methods 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Slot die Elsevier Polymeric membranes Elsevier Eco-friendly solvents Elsevier Scale-up study Elsevier Jeong, Tae J. oth Kline, Eric oth Banks, Lillian oth Grulke, Eric oth Harris, Tequila oth Escobar, Isabel C. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:614 year:2020 day:15 month:11 pages:0 https://doi.org/10.1016/j.memsci.2020.118510 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 614 2020 15 1115 0 |
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10.1016/j.memsci.2020.118510 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001118.pica (DE-627)ELV051216787 (ELSEVIER)S0376-7388(20)31087-5 DE-627 ger DE-627 rakwb eng 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Dong, Xiaobo verfasserin aut Eco-friendly solvents and their mixture for the fabrication of polysulfone ultrafiltration membranes: An investigation of doctor blade and slot die casting methods 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Slot die Elsevier Polymeric membranes Elsevier Eco-friendly solvents Elsevier Scale-up study Elsevier Jeong, Tae J. oth Kline, Eric oth Banks, Lillian oth Grulke, Eric oth Harris, Tequila oth Escobar, Isabel C. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:614 year:2020 day:15 month:11 pages:0 https://doi.org/10.1016/j.memsci.2020.118510 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 614 2020 15 1115 0 |
| allfields_unstemmed |
10.1016/j.memsci.2020.118510 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001118.pica (DE-627)ELV051216787 (ELSEVIER)S0376-7388(20)31087-5 DE-627 ger DE-627 rakwb eng 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Dong, Xiaobo verfasserin aut Eco-friendly solvents and their mixture for the fabrication of polysulfone ultrafiltration membranes: An investigation of doctor blade and slot die casting methods 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Slot die Elsevier Polymeric membranes Elsevier Eco-friendly solvents Elsevier Scale-up study Elsevier Jeong, Tae J. oth Kline, Eric oth Banks, Lillian oth Grulke, Eric oth Harris, Tequila oth Escobar, Isabel C. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:614 year:2020 day:15 month:11 pages:0 https://doi.org/10.1016/j.memsci.2020.118510 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 614 2020 15 1115 0 |
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10.1016/j.memsci.2020.118510 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001118.pica (DE-627)ELV051216787 (ELSEVIER)S0376-7388(20)31087-5 DE-627 ger DE-627 rakwb eng 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Dong, Xiaobo verfasserin aut Eco-friendly solvents and their mixture for the fabrication of polysulfone ultrafiltration membranes: An investigation of doctor blade and slot die casting methods 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Slot die Elsevier Polymeric membranes Elsevier Eco-friendly solvents Elsevier Scale-up study Elsevier Jeong, Tae J. oth Kline, Eric oth Banks, Lillian oth Grulke, Eric oth Harris, Tequila oth Escobar, Isabel C. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:614 year:2020 day:15 month:11 pages:0 https://doi.org/10.1016/j.memsci.2020.118510 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 614 2020 15 1115 0 |
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10.1016/j.memsci.2020.118510 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001118.pica (DE-627)ELV051216787 (ELSEVIER)S0376-7388(20)31087-5 DE-627 ger DE-627 rakwb eng 540 VZ 35.17 bkl 58.50 bkl 43.12 bkl Dong, Xiaobo verfasserin aut Eco-friendly solvents and their mixture for the fabrication of polysulfone ultrafiltration membranes: An investigation of doctor blade and slot die casting methods 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. Slot die Elsevier Polymeric membranes Elsevier Eco-friendly solvents Elsevier Scale-up study Elsevier Jeong, Tae J. oth Kline, Eric oth Banks, Lillian oth Grulke, Eric oth Harris, Tequila oth Escobar, Isabel C. oth Enthalten in Elsevier Yue, Xin-Zheng ELSEVIER Steering charge kinetics in W 2019 the official journal of the North American Membrane Society New York, NY [u.a.] (DE-627)ELV002478420 volume:614 year:2020 day:15 month:11 pages:0 https://doi.org/10.1016/j.memsci.2020.118510 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.17 Katalyse VZ 58.50 Umwelttechnik: Allgemeines VZ 43.12 Umweltchemie VZ AR 614 2020 15 1115 0 |
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eco-friendly solvents and their mixture for the fabrication of polysulfone ultrafiltration membranes: an investigation of doctor blade and slot die casting methods |
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Eco-friendly solvents and their mixture for the fabrication of polysulfone ultrafiltration membranes: An investigation of doctor blade and slot die casting methods |
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Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. |
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Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. |
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Nonsolvent induced phase separation has been widely used to fabricate polymeric membranes. Common solvents, such as dimethylacetamide (DMAc) and N-Methyl-2-pyrrolidone (NMP), are toxic and not environmentally friendly; therefore, eco-friendly alternatives are needed. Eco-friendly solvents, such as Rhodiasolv® PolarClean (PolarClean) and γ-valerolactone (GVL), have been investigated to replace DMAc and NMP at the laboratory scale; however, not extensively at the production scale. In this work, the feasibility of fabricating polysulfone (PSf) ultrafiltration membranes using eco-friendly solvents at laboratory and production scales is investigated. First, it was determined that the addition of GVL to dope solutions of PolarClean could reduce the original preparation time at a rotation speed of 450 RPM by two-thirds, and by three-quarters at 600 RPM. Furthermore, dope solutions exhibit Newtonian fluid behavior. Doctor blade extrusion and a roll-to-roll (R2R) system integrated with slot die casting are used to fabricate the PSf ultrafiltration membranes at laboratory and production scales, respectively, and the resulting membranes are compared structurally, morphologically and operationally. |
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