Reaction mechanisms of nano-sized AlN powders synthesized from dicyandiamide and its optical property
Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied....
Ausführliche Beschreibung
Autor*in: |
Cheng, Yanling [verfasserIn] |
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Englisch |
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2020transfer abstract |
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Enthalten in: Road traffic crash characteristics of drivers who take prescription medicines that carry a risk to driving - Lu, Li ELSEVIER, 2020, including materials science communications : an international, interdisciplinary journal on science characterization and processing of advanced materials : the international journal of the Chinese Society for Materials Science, New York, NY [u.a.] |
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Übergeordnetes Werk: |
volume:253 ; year:2020 ; day:1 ; month:10 ; pages:0 |
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DOI / URN: |
10.1016/j.matchemphys.2020.123376 |
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520 | |a Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. | ||
520 | |a Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. | ||
650 | 7 | |a Optical bandgap |2 Elsevier | |
650 | 7 | |a Nano-sized AlN |2 Elsevier | |
650 | 7 | |a Dicyandiamide |2 Elsevier | |
650 | 7 | |a Wet chemical route |2 Elsevier | |
650 | 7 | |a Reaction mechanism |2 Elsevier | |
700 | 1 | |a Li, Kexu |4 oth | |
700 | 1 | |a Wei, Shihong |4 oth | |
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700 | 1 | |a Huang, Xiong |4 oth | |
700 | 1 | |a Lin, Sidney |4 oth | |
700 | 1 | |a Plucknett, Kevin P. |4 oth | |
700 | 1 | |a Lin, Huatay |4 oth | |
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10.1016/j.matchemphys.2020.123376 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001130.pica (DE-627)ELV05132296X (ELSEVIER)S0254-0584(20)30746-X DE-627 ger DE-627 rakwb eng 610 VZ 44.38 bkl 44.91 bkl Cheng, Yanling verfasserin aut Reaction mechanisms of nano-sized AlN powders synthesized from dicyandiamide and its optical property 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Optical bandgap Elsevier Nano-sized AlN Elsevier Dicyandiamide Elsevier Wet chemical route Elsevier Reaction mechanism Elsevier Li, Kexu oth Wei, Shihong oth Zhang, Hainan oth Yang, Shengkai oth Huang, Xiong oth Lin, Sidney oth Plucknett, Kevin P. oth Lin, Huatay oth Enthalten in Elsevier Lu, Li ELSEVIER Road traffic crash characteristics of drivers who take prescription medicines that carry a risk to driving 2020 including materials science communications : an international, interdisciplinary journal on science characterization and processing of advanced materials : the international journal of the Chinese Society for Materials Science New York, NY [u.a.] (DE-627)ELV005250781 volume:253 year:2020 day:1 month:10 pages:0 https://doi.org/10.1016/j.matchemphys.2020.123376 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.38 Pharmakologie VZ 44.91 Psychiatrie Psychopathologie VZ AR 253 2020 1 1001 0 |
spelling |
10.1016/j.matchemphys.2020.123376 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001130.pica (DE-627)ELV05132296X (ELSEVIER)S0254-0584(20)30746-X DE-627 ger DE-627 rakwb eng 610 VZ 44.38 bkl 44.91 bkl Cheng, Yanling verfasserin aut Reaction mechanisms of nano-sized AlN powders synthesized from dicyandiamide and its optical property 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Optical bandgap Elsevier Nano-sized AlN Elsevier Dicyandiamide Elsevier Wet chemical route Elsevier Reaction mechanism Elsevier Li, Kexu oth Wei, Shihong oth Zhang, Hainan oth Yang, Shengkai oth Huang, Xiong oth Lin, Sidney oth Plucknett, Kevin P. oth Lin, Huatay oth Enthalten in Elsevier Lu, Li ELSEVIER Road traffic crash characteristics of drivers who take prescription medicines that carry a risk to driving 2020 including materials science communications : an international, interdisciplinary journal on science characterization and processing of advanced materials : the international journal of the Chinese Society for Materials Science New York, NY [u.a.] (DE-627)ELV005250781 volume:253 year:2020 day:1 month:10 pages:0 https://doi.org/10.1016/j.matchemphys.2020.123376 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.38 Pharmakologie VZ 44.91 Psychiatrie Psychopathologie VZ AR 253 2020 1 1001 0 |
allfields_unstemmed |
10.1016/j.matchemphys.2020.123376 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001130.pica (DE-627)ELV05132296X (ELSEVIER)S0254-0584(20)30746-X DE-627 ger DE-627 rakwb eng 610 VZ 44.38 bkl 44.91 bkl Cheng, Yanling verfasserin aut Reaction mechanisms of nano-sized AlN powders synthesized from dicyandiamide and its optical property 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Optical bandgap Elsevier Nano-sized AlN Elsevier Dicyandiamide Elsevier Wet chemical route Elsevier Reaction mechanism Elsevier Li, Kexu oth Wei, Shihong oth Zhang, Hainan oth Yang, Shengkai oth Huang, Xiong oth Lin, Sidney oth Plucknett, Kevin P. oth Lin, Huatay oth Enthalten in Elsevier Lu, Li ELSEVIER Road traffic crash characteristics of drivers who take prescription medicines that carry a risk to driving 2020 including materials science communications : an international, interdisciplinary journal on science characterization and processing of advanced materials : the international journal of the Chinese Society for Materials Science New York, NY [u.a.] (DE-627)ELV005250781 volume:253 year:2020 day:1 month:10 pages:0 https://doi.org/10.1016/j.matchemphys.2020.123376 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.38 Pharmakologie VZ 44.91 Psychiatrie Psychopathologie VZ AR 253 2020 1 1001 0 |
allfieldsGer |
10.1016/j.matchemphys.2020.123376 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001130.pica (DE-627)ELV05132296X (ELSEVIER)S0254-0584(20)30746-X DE-627 ger DE-627 rakwb eng 610 VZ 44.38 bkl 44.91 bkl Cheng, Yanling verfasserin aut Reaction mechanisms of nano-sized AlN powders synthesized from dicyandiamide and its optical property 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Optical bandgap Elsevier Nano-sized AlN Elsevier Dicyandiamide Elsevier Wet chemical route Elsevier Reaction mechanism Elsevier Li, Kexu oth Wei, Shihong oth Zhang, Hainan oth Yang, Shengkai oth Huang, Xiong oth Lin, Sidney oth Plucknett, Kevin P. oth Lin, Huatay oth Enthalten in Elsevier Lu, Li ELSEVIER Road traffic crash characteristics of drivers who take prescription medicines that carry a risk to driving 2020 including materials science communications : an international, interdisciplinary journal on science characterization and processing of advanced materials : the international journal of the Chinese Society for Materials Science New York, NY [u.a.] (DE-627)ELV005250781 volume:253 year:2020 day:1 month:10 pages:0 https://doi.org/10.1016/j.matchemphys.2020.123376 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.38 Pharmakologie VZ 44.91 Psychiatrie Psychopathologie VZ AR 253 2020 1 1001 0 |
allfieldsSound |
10.1016/j.matchemphys.2020.123376 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001130.pica (DE-627)ELV05132296X (ELSEVIER)S0254-0584(20)30746-X DE-627 ger DE-627 rakwb eng 610 VZ 44.38 bkl 44.91 bkl Cheng, Yanling verfasserin aut Reaction mechanisms of nano-sized AlN powders synthesized from dicyandiamide and its optical property 2020transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. Optical bandgap Elsevier Nano-sized AlN Elsevier Dicyandiamide Elsevier Wet chemical route Elsevier Reaction mechanism Elsevier Li, Kexu oth Wei, Shihong oth Zhang, Hainan oth Yang, Shengkai oth Huang, Xiong oth Lin, Sidney oth Plucknett, Kevin P. oth Lin, Huatay oth Enthalten in Elsevier Lu, Li ELSEVIER Road traffic crash characteristics of drivers who take prescription medicines that carry a risk to driving 2020 including materials science communications : an international, interdisciplinary journal on science characterization and processing of advanced materials : the international journal of the Chinese Society for Materials Science New York, NY [u.a.] (DE-627)ELV005250781 volume:253 year:2020 day:1 month:10 pages:0 https://doi.org/10.1016/j.matchemphys.2020.123376 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.38 Pharmakologie VZ 44.91 Psychiatrie Psychopathologie VZ AR 253 2020 1 1001 0 |
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Road traffic crash characteristics of drivers who take prescription medicines that carry a risk to driving |
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The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties.</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. 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reaction mechanisms of nano-sized aln powders synthesized from dicyandiamide and its optical property |
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Reaction mechanisms of nano-sized AlN powders synthesized from dicyandiamide and its optical property |
abstract |
Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. |
abstractGer |
Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. |
abstract_unstemmed |
Nano-sized AlN powders were successfully synthesized using a wet chemical route, with dicyandiamide as the nitrogen source reagent. The influence of dicyandiamide/metal precursor molar ratio on the purity, crystallization, microstructure, and optical properties of the calcined powders were studied. The underlying reaction mechanisms, along with the intermediates formed during the reactions, were also investigated. The compositions and morphologies of the as-received and prepared powders were subsequently characterized using XPS, FTIR, XRD, SEM, and TEM. The optical properties of the prepared powders were measured by ultraviolet–visible spectroscopy (UV–Vis). The precursor components decompose, and follow a complex reaction sequence as a function of temperature, finally leading to AlN formation at 800 °C. Increasing AlN content is achieved between 800 and 890 °C. Essentially only AlN arises following calcination at 900 °C. The AlN crystallite size and degree of crystallization further increase when calcining at 1000 °C. This work demonstrates a promising route to produce nano-sized AlN powders with favorable microstructures and optical properties. |
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Reaction mechanisms of nano-sized AlN powders synthesized from dicyandiamide and its optical property |
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