Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements
Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state an...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Gavrilova, T.P. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021transfer abstract |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Optimism in prolonged grief and depression following loss: A three-wave longitudinal study - Boelen, Paul A. ELSEVIER, 2015transfer abstract, an international journal, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:323 ; year:2021 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.ssc.2020.114108 |
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ELV052419134 |
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| 245 | 1 | 0 | |a Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements |
| 264 | 1 | |c 2021transfer abstract | |
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| 520 | |a Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. | ||
| 520 | |a Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. | ||
| 650 | 7 | |a Magnetization |2 Elsevier | |
| 650 | 7 | |a Electron spin resonance |2 Elsevier | |
| 650 | 7 | |a Cathode material |2 Elsevier | |
| 650 | 7 | |a Li3V2(PO4)3 |2 Elsevier | |
| 700 | 1 | |a Khantimerov, S.M. |4 oth | |
| 700 | 1 | |a Fatykhov, R.R. |4 oth | |
| 700 | 1 | |a Yatsyk, I.V. |4 oth | |
| 700 | 1 | |a Cherosov, M.A. |4 oth | |
| 700 | 1 | |a Lee, H.S. |4 oth | |
| 700 | 1 | |a Vishwanathan, R. |4 oth | |
| 700 | 1 | |a Saravanan, K. |4 oth | |
| 700 | 1 | |a Suleimanov, N.M. |4 oth | |
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10.1016/j.ssc.2020.114108 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001230.pica (DE-627)ELV052419134 (ELSEVIER)S0038-1098(20)30606-2 DE-627 ger DE-627 rakwb eng Gavrilova, T.P. verfasserin aut Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Magnetization Elsevier Electron spin resonance Elsevier Cathode material Elsevier Li3V2(PO4)3 Elsevier Khantimerov, S.M. oth Fatykhov, R.R. oth Yatsyk, I.V. oth Cherosov, M.A. oth Lee, H.S. oth Vishwanathan, R. oth Saravanan, K. oth Suleimanov, N.M. oth Enthalten in Elsevier Science Boelen, Paul A. ELSEVIER Optimism in prolonged grief and depression following loss: A three-wave longitudinal study 2015transfer abstract an international journal New York, NY [u.a.] (DE-627)ELV018237444 volume:323 year:2021 pages:0 https://doi.org/10.1016/j.ssc.2020.114108 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 AR 323 2021 0 |
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10.1016/j.ssc.2020.114108 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001230.pica (DE-627)ELV052419134 (ELSEVIER)S0038-1098(20)30606-2 DE-627 ger DE-627 rakwb eng Gavrilova, T.P. verfasserin aut Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Magnetization Elsevier Electron spin resonance Elsevier Cathode material Elsevier Li3V2(PO4)3 Elsevier Khantimerov, S.M. oth Fatykhov, R.R. oth Yatsyk, I.V. oth Cherosov, M.A. oth Lee, H.S. oth Vishwanathan, R. oth Saravanan, K. oth Suleimanov, N.M. oth Enthalten in Elsevier Science Boelen, Paul A. ELSEVIER Optimism in prolonged grief and depression following loss: A three-wave longitudinal study 2015transfer abstract an international journal New York, NY [u.a.] (DE-627)ELV018237444 volume:323 year:2021 pages:0 https://doi.org/10.1016/j.ssc.2020.114108 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 AR 323 2021 0 |
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10.1016/j.ssc.2020.114108 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001230.pica (DE-627)ELV052419134 (ELSEVIER)S0038-1098(20)30606-2 DE-627 ger DE-627 rakwb eng Gavrilova, T.P. verfasserin aut Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Magnetization Elsevier Electron spin resonance Elsevier Cathode material Elsevier Li3V2(PO4)3 Elsevier Khantimerov, S.M. oth Fatykhov, R.R. oth Yatsyk, I.V. oth Cherosov, M.A. oth Lee, H.S. oth Vishwanathan, R. oth Saravanan, K. oth Suleimanov, N.M. oth Enthalten in Elsevier Science Boelen, Paul A. ELSEVIER Optimism in prolonged grief and depression following loss: A three-wave longitudinal study 2015transfer abstract an international journal New York, NY [u.a.] (DE-627)ELV018237444 volume:323 year:2021 pages:0 https://doi.org/10.1016/j.ssc.2020.114108 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 AR 323 2021 0 |
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10.1016/j.ssc.2020.114108 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001230.pica (DE-627)ELV052419134 (ELSEVIER)S0038-1098(20)30606-2 DE-627 ger DE-627 rakwb eng Gavrilova, T.P. verfasserin aut Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Magnetization Elsevier Electron spin resonance Elsevier Cathode material Elsevier Li3V2(PO4)3 Elsevier Khantimerov, S.M. oth Fatykhov, R.R. oth Yatsyk, I.V. oth Cherosov, M.A. oth Lee, H.S. oth Vishwanathan, R. oth Saravanan, K. oth Suleimanov, N.M. oth Enthalten in Elsevier Science Boelen, Paul A. ELSEVIER Optimism in prolonged grief and depression following loss: A three-wave longitudinal study 2015transfer abstract an international journal New York, NY [u.a.] (DE-627)ELV018237444 volume:323 year:2021 pages:0 https://doi.org/10.1016/j.ssc.2020.114108 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 AR 323 2021 0 |
| allfieldsSound |
10.1016/j.ssc.2020.114108 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001230.pica (DE-627)ELV052419134 (ELSEVIER)S0038-1098(20)30606-2 DE-627 ger DE-627 rakwb eng Gavrilova, T.P. verfasserin aut Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. Magnetization Elsevier Electron spin resonance Elsevier Cathode material Elsevier Li3V2(PO4)3 Elsevier Khantimerov, S.M. oth Fatykhov, R.R. oth Yatsyk, I.V. oth Cherosov, M.A. oth Lee, H.S. oth Vishwanathan, R. oth Saravanan, K. oth Suleimanov, N.M. oth Enthalten in Elsevier Science Boelen, Paul A. ELSEVIER Optimism in prolonged grief and depression following loss: A three-wave longitudinal study 2015transfer abstract an international journal New York, NY [u.a.] (DE-627)ELV018237444 volume:323 year:2021 pages:0 https://doi.org/10.1016/j.ssc.2020.114108 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_40 AR 323 2021 0 |
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Enthalten in Optimism in prolonged grief and depression following loss: A three-wave longitudinal study New York, NY [u.a.] volume:323 year:2021 pages:0 |
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Enthalten in Optimism in prolonged grief and depression following loss: A three-wave longitudinal study New York, NY [u.a.] volume:323 year:2021 pages:0 |
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Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite.</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). 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Gavrilova, T.P. Elsevier Magnetization Elsevier Electron spin resonance Elsevier Cathode material Elsevier Li3V2(PO4)3 Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements |
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magnetic properties and vanadium oxidation state in α-li3v2(po4)3/c composite: magnetization and esr measurements |
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Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements |
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Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. |
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Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. |
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Here we present the magnetization and electron spin resonance (ESR) measurements of α-Li3V2(PO4)3/C composite, which can be potentially used as a cathode material in a lithium ion battery. Magnetization measurements of α-Li3V2(PO4)3/C indicate that the investigated sample is in paramagnetic state and exhibits Curie-Weiss like behavior above T = 50K. The negative value of the Curie-Weiss temperature θC W = −22 K suggests the presence of the antiferromagnetic interactions between magnetic spins of V3+ ions (3 d2, S = 1). At the same time, the presence of the magnetic phase transition was not observed in the investigated temperature range from 2 K up to room temperature. The nonlinear behavior of the field dependence of the magnetization was observed only at T = 2 K suggesting the possible magnetic ordering below this temperature. ESR measurements were performed both for as-prepared α-Li3V2(PO4)3/C composite and for α-Li3V2(PO4)3/C sample after Li deintercalation and intercalation processes. The complete reduction of vanadium ions to the initial valence state V3+ after the first charge/discharge cycle was determined indicating the reversible intercalation of all lithium ions to the structure during the first delithiation/lithiation cycle in the investigated α-Li3V2(PO4)3/C composite. |
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Magnetic properties and vanadium oxidation state in α-Li3V2(PO4)3/C composite: Magnetization and ESR measurements |
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