Single-molecule tracking measurement of PDMS layer during curing process
The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding...
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Gespeichert in:
| Autor*in: |
Iwao, Ryo [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021transfer abstract |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study - Dai, Jiamiao ELSEVIER, 2022, europhysics journal, Amsterdam |
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| Übergeordnetes Werk: |
volume:565 ; year:2021 ; day:1 ; month:03 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.physa.2020.125576 |
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| 520 | |a The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. | ||
| 520 | |a The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. | ||
| 650 | 7 | |a Curing process |2 Elsevier | |
| 650 | 7 | |a Single-molecule tracking |2 Elsevier | |
| 650 | 7 | |a Diffusion coefficient |2 Elsevier | |
| 650 | 7 | |a PDMS |2 Elsevier | |
| 700 | 1 | |a Yamaguchi, Hiroki |4 oth | |
| 700 | 1 | |a Niimi, Tomohide |4 oth | |
| 700 | 1 | |a Matsuda, Yu |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n North Holland Publ. Co |a Dai, Jiamiao ELSEVIER |t Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study |d 2022 |d europhysics journal |g Amsterdam |w (DE-627)ELV00892340X |
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10.1016/j.physa.2020.125576 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001839.pica (DE-627)ELV052591247 (ELSEVIER)S0378-4371(20)30874-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.91 bkl Iwao, Ryo verfasserin aut Single-molecule tracking measurement of PDMS layer during curing process 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. Curing process Elsevier Single-molecule tracking Elsevier Diffusion coefficient Elsevier PDMS Elsevier Yamaguchi, Hiroki oth Niimi, Tomohide oth Matsuda, Yu oth Enthalten in North Holland Publ. Co Dai, Jiamiao ELSEVIER Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study 2022 europhysics journal Amsterdam (DE-627)ELV00892340X volume:565 year:2021 day:1 month:03 pages:0 https://doi.org/10.1016/j.physa.2020.125576 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.91 Psychiatrie Psychopathologie VZ AR 565 2021 1 0301 0 |
| spelling |
10.1016/j.physa.2020.125576 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001839.pica (DE-627)ELV052591247 (ELSEVIER)S0378-4371(20)30874-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.91 bkl Iwao, Ryo verfasserin aut Single-molecule tracking measurement of PDMS layer during curing process 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. Curing process Elsevier Single-molecule tracking Elsevier Diffusion coefficient Elsevier PDMS Elsevier Yamaguchi, Hiroki oth Niimi, Tomohide oth Matsuda, Yu oth Enthalten in North Holland Publ. Co Dai, Jiamiao ELSEVIER Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study 2022 europhysics journal Amsterdam (DE-627)ELV00892340X volume:565 year:2021 day:1 month:03 pages:0 https://doi.org/10.1016/j.physa.2020.125576 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.91 Psychiatrie Psychopathologie VZ AR 565 2021 1 0301 0 |
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10.1016/j.physa.2020.125576 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001839.pica (DE-627)ELV052591247 (ELSEVIER)S0378-4371(20)30874-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.91 bkl Iwao, Ryo verfasserin aut Single-molecule tracking measurement of PDMS layer during curing process 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. Curing process Elsevier Single-molecule tracking Elsevier Diffusion coefficient Elsevier PDMS Elsevier Yamaguchi, Hiroki oth Niimi, Tomohide oth Matsuda, Yu oth Enthalten in North Holland Publ. Co Dai, Jiamiao ELSEVIER Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study 2022 europhysics journal Amsterdam (DE-627)ELV00892340X volume:565 year:2021 day:1 month:03 pages:0 https://doi.org/10.1016/j.physa.2020.125576 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.91 Psychiatrie Psychopathologie VZ AR 565 2021 1 0301 0 |
| allfieldsGer |
10.1016/j.physa.2020.125576 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001839.pica (DE-627)ELV052591247 (ELSEVIER)S0378-4371(20)30874-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.91 bkl Iwao, Ryo verfasserin aut Single-molecule tracking measurement of PDMS layer during curing process 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. Curing process Elsevier Single-molecule tracking Elsevier Diffusion coefficient Elsevier PDMS Elsevier Yamaguchi, Hiroki oth Niimi, Tomohide oth Matsuda, Yu oth Enthalten in North Holland Publ. Co Dai, Jiamiao ELSEVIER Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study 2022 europhysics journal Amsterdam (DE-627)ELV00892340X volume:565 year:2021 day:1 month:03 pages:0 https://doi.org/10.1016/j.physa.2020.125576 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.91 Psychiatrie Psychopathologie VZ AR 565 2021 1 0301 0 |
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10.1016/j.physa.2020.125576 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001839.pica (DE-627)ELV052591247 (ELSEVIER)S0378-4371(20)30874-8 DE-627 ger DE-627 rakwb eng 610 VZ 44.91 bkl Iwao, Ryo verfasserin aut Single-molecule tracking measurement of PDMS layer during curing process 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. Curing process Elsevier Single-molecule tracking Elsevier Diffusion coefficient Elsevier PDMS Elsevier Yamaguchi, Hiroki oth Niimi, Tomohide oth Matsuda, Yu oth Enthalten in North Holland Publ. Co Dai, Jiamiao ELSEVIER Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study 2022 europhysics journal Amsterdam (DE-627)ELV00892340X volume:565 year:2021 day:1 month:03 pages:0 https://doi.org/10.1016/j.physa.2020.125576 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 44.91 Psychiatrie Psychopathologie VZ AR 565 2021 1 0301 0 |
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Enthalten in Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study Amsterdam volume:565 year:2021 day:1 month:03 pages:0 |
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Enthalten in Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study Amsterdam volume:565 year:2021 day:1 month:03 pages:0 |
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Effects of psychiatric disorders on ultrasound measurements and adverse perinatal outcomes in Chinese pregnant women: A ten-year retrospective cohort study |
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<?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01000caa a22002652 4500</leader><controlfield tag="001">ELV052591247</controlfield><controlfield tag="003">DE-627</controlfield><controlfield tag="005">20230626033455.0</controlfield><controlfield tag="007">cr uuu---uuuuu</controlfield><controlfield tag="008">210910s2021 xx |||||o 00| ||eng c</controlfield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.1016/j.physa.2020.125576</subfield><subfield code="2">doi</subfield></datafield><datafield tag="028" ind1="5" ind2="2"><subfield code="a">/cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001839.pica</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-627)ELV052591247</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(ELSEVIER)S0378-4371(20)30874-8</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-627</subfield><subfield code="b">ger</subfield><subfield code="c">DE-627</subfield><subfield code="e">rakwb</subfield></datafield><datafield tag="041" ind1=" " ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="082" ind1="0" ind2="4"><subfield code="a">610</subfield><subfield code="q">VZ</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">44.91</subfield><subfield code="2">bkl</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Iwao, Ryo</subfield><subfield code="e">verfasserin</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Single-molecule tracking measurement of PDMS layer during curing process</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2021transfer abstract</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zzz</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">z</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">nicht spezifiziert</subfield><subfield code="b">zu</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. 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The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. 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The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. |
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The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. |
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The curing process of poly(dimethylsiloxane) (PDMS) was microscopically investigated by the single-molecule tracking method based on the diffusion motion of fluorescent dye molecules adding to the PDMS layer stored at a temperature of 308K. The PDMS layer was completely cured at 900 min after adding a curing agent. We compared the time- and ensemble-averaged mean square displacements (MSDs) of the tracked molecules at 90, 510, and 900 min after adding the curing agent into the PDMS layer. The discrepancies were observed between the time- and ensemble-averaged MSDs, indicating weak ergodicity breaking. The spatially averaged diffusion coefficient exhibited a two-step decrease: first step was rapid decrease suggesting the extent of crosslinking, and second step was slow one suggesting the increase of crosslink density. The single-molecule trajectory scale analysis revealed the heterogeneous distribution of the diffusion coefficient. By calculating the heat map from the slope of moment scaling spectrum (MSS) of each single-molecule trajectory, cluster structures were recognized. The spatial correlation of the slope of MSS decreased with the time elapsed. These results suggested the existence of the heterogeneous structure in the PDMS layer during the curing process. |
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