Study on SERS activity of Au-Ag bimetallic nanostructures synthesized using different reducing agents
The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained u...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Das, G.M. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021transfer abstract |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Characterization of a 7 bp indel in MARCH1 promoter associated with reproductive traits in Malabari and Attappady Black goats of India - Desai, Akshatha G. ELSEVIER, 2021, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:129 ; year:2021 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.physe.2021.114656 |
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| 520 | |a The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. | ||
| 520 | |a The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. | ||
| 650 | 7 | |a SERS |2 Elsevier | |
| 650 | 7 | |a Nanoplasmonics |2 Elsevier | |
| 650 | 7 | |a Reducing agents |2 Elsevier | |
| 650 | 7 | |a Bimetallic nanostructures |2 Elsevier | |
| 650 | 7 | |a FEM |2 Elsevier | |
| 700 | 1 | |a William, R.V. |4 oth | |
| 700 | 1 | |a Dantham, V.R. |4 oth | |
| 700 | 1 | |a Laha, R. |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n North-Holland, Elsevier Science |a Desai, Akshatha G. ELSEVIER |t Characterization of a 7 bp indel in MARCH1 promoter associated with reproductive traits in Malabari and Attappady Black goats of India |d 2021 |g Amsterdam [u.a.] |w (DE-627)ELV006775543 |
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10.1016/j.physe.2021.114656 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001315.pica (DE-627)ELV053276825 (ELSEVIER)S1386-9477(21)00039-4 DE-627 ger DE-627 rakwb eng 630 640 VZ Das, G.M. verfasserin aut Study on SERS activity of Au-Ag bimetallic nanostructures synthesized using different reducing agents 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. SERS Elsevier Nanoplasmonics Elsevier Reducing agents Elsevier Bimetallic nanostructures Elsevier FEM Elsevier William, R.V. oth Dantham, V.R. oth Laha, R. oth Enthalten in North-Holland, Elsevier Science Desai, Akshatha G. ELSEVIER Characterization of a 7 bp indel in MARCH1 promoter associated with reproductive traits in Malabari and Attappady Black goats of India 2021 Amsterdam [u.a.] (DE-627)ELV006775543 volume:129 year:2021 pages:0 https://doi.org/10.1016/j.physe.2021.114656 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U AR 129 2021 0 |
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10.1016/j.physe.2021.114656 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001315.pica (DE-627)ELV053276825 (ELSEVIER)S1386-9477(21)00039-4 DE-627 ger DE-627 rakwb eng 630 640 VZ Das, G.M. verfasserin aut Study on SERS activity of Au-Ag bimetallic nanostructures synthesized using different reducing agents 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. SERS Elsevier Nanoplasmonics Elsevier Reducing agents Elsevier Bimetallic nanostructures Elsevier FEM Elsevier William, R.V. oth Dantham, V.R. oth Laha, R. oth Enthalten in North-Holland, Elsevier Science Desai, Akshatha G. ELSEVIER Characterization of a 7 bp indel in MARCH1 promoter associated with reproductive traits in Malabari and Attappady Black goats of India 2021 Amsterdam [u.a.] (DE-627)ELV006775543 volume:129 year:2021 pages:0 https://doi.org/10.1016/j.physe.2021.114656 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U AR 129 2021 0 |
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10.1016/j.physe.2021.114656 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001315.pica (DE-627)ELV053276825 (ELSEVIER)S1386-9477(21)00039-4 DE-627 ger DE-627 rakwb eng 630 640 VZ Das, G.M. verfasserin aut Study on SERS activity of Au-Ag bimetallic nanostructures synthesized using different reducing agents 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. SERS Elsevier Nanoplasmonics Elsevier Reducing agents Elsevier Bimetallic nanostructures Elsevier FEM Elsevier William, R.V. oth Dantham, V.R. oth Laha, R. oth Enthalten in North-Holland, Elsevier Science Desai, Akshatha G. ELSEVIER Characterization of a 7 bp indel in MARCH1 promoter associated with reproductive traits in Malabari and Attappady Black goats of India 2021 Amsterdam [u.a.] (DE-627)ELV006775543 volume:129 year:2021 pages:0 https://doi.org/10.1016/j.physe.2021.114656 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U AR 129 2021 0 |
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10.1016/j.physe.2021.114656 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001315.pica (DE-627)ELV053276825 (ELSEVIER)S1386-9477(21)00039-4 DE-627 ger DE-627 rakwb eng 630 640 VZ Das, G.M. verfasserin aut Study on SERS activity of Au-Ag bimetallic nanostructures synthesized using different reducing agents 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. SERS Elsevier Nanoplasmonics Elsevier Reducing agents Elsevier Bimetallic nanostructures Elsevier FEM Elsevier William, R.V. oth Dantham, V.R. oth Laha, R. oth Enthalten in North-Holland, Elsevier Science Desai, Akshatha G. ELSEVIER Characterization of a 7 bp indel in MARCH1 promoter associated with reproductive traits in Malabari and Attappady Black goats of India 2021 Amsterdam [u.a.] (DE-627)ELV006775543 volume:129 year:2021 pages:0 https://doi.org/10.1016/j.physe.2021.114656 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U AR 129 2021 0 |
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10.1016/j.physe.2021.114656 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001315.pica (DE-627)ELV053276825 (ELSEVIER)S1386-9477(21)00039-4 DE-627 ger DE-627 rakwb eng 630 640 VZ Das, G.M. verfasserin aut Study on SERS activity of Au-Ag bimetallic nanostructures synthesized using different reducing agents 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. SERS Elsevier Nanoplasmonics Elsevier Reducing agents Elsevier Bimetallic nanostructures Elsevier FEM Elsevier William, R.V. oth Dantham, V.R. oth Laha, R. oth Enthalten in North-Holland, Elsevier Science Desai, Akshatha G. ELSEVIER Characterization of a 7 bp indel in MARCH1 promoter associated with reproductive traits in Malabari and Attappady Black goats of India 2021 Amsterdam [u.a.] (DE-627)ELV006775543 volume:129 year:2021 pages:0 https://doi.org/10.1016/j.physe.2021.114656 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U AR 129 2021 0 |
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Characterization of a 7 bp indel in MARCH1 promoter associated with reproductive traits in Malabari and Attappady Black goats of India |
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study on sers activity of au-ag bimetallic nanostructures synthesized using different reducing agents |
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Study on SERS activity of Au-Ag bimetallic nanostructures synthesized using different reducing agents |
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The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. |
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The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. |
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The Au-Ag bimetallic nanostructures were synthesized independently using three different reducing agents [ascorbic acid (C6H8O6), sodium borohydride (NaBH4) and tri-sodium citrate dihydrate (C6H9Na3O9)] to understand their effect on the morphology of the nanostructures. The nanostructures obtained using the reducing agents mentioned in above order, were found in sprouted potato, cubical, and prolate spheroid (PS) shapes. All the synthesized nanostructures were characterized using energy-dispersive X-ray spectroscopy and extinction spectroscopy. The surface enhanced Raman scattering (SERS) activity of all these nanostructures was studied using Raman probe solutions with micro and nanomolar concentrations. Relatively, the PS shaped nanostructures were found to be more stable and better for SERS studies. Therefore, these nanostructures were further characterized by Transmission electron microscopy and X-ray photoelectron spectroscopy. The usefulness of PS shaped Au-Ag nanostructures was also demonstrated by recording the spectra of both methylene blue (MB) and 4-Aminothiophenol (4-ATP) solutions with femtomolar concentration. The experimental enhancement factor (EEF) was found to be around 1.1 × 1011 in case of MB solution with femtomolar concentration. The possible origin for the EEF is explained using quasi-static theory and Finite Element Method (FEM) based simulations. |
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