Structural dependence of microwave dielectric performance of wolframite structured Mg1-xCaxZrNb2O8 ceramics: Crystal structure, microstructure evolution, Raman analysis and chemical bond theory
Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substit...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Wang, Gang [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021transfer abstract |
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| Schlagwörter: |
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| Umfang: |
7 |
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| Übergeordnetes Werk: |
Enthalten in: Improved differential evolution for RSSD-based localization in Gaussian mixture noise - Zhang, Yuanyuan ELSEVIER, 2023, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:41 ; year:2021 ; number:6 ; pages:3445-3451 ; extent:7 |
| Links: |
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| DOI / URN: |
10.1016/j.jeurceramsoc.2021.01.033 |
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| 245 | 1 | 0 | |a Structural dependence of microwave dielectric performance of wolframite structured Mg1-xCaxZrNb2O8 ceramics: Crystal structure, microstructure evolution, Raman analysis and chemical bond theory |
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| 520 | |a Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. | ||
| 520 | |a Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. | ||
| 650 | 7 | |a Raman vibration |2 Elsevier | |
| 650 | 7 | |a Mg1-xCaxZrNb2O8 ceramics |2 Elsevier | |
| 650 | 7 | |a Microstructure evolution |2 Elsevier | |
| 650 | 7 | |a Chemical bond theory |2 Elsevier | |
| 700 | 1 | |a Zhang, Dainan |4 oth | |
| 700 | 1 | |a Li, Jie |4 oth | |
| 700 | 1 | |a Shi, Liang |4 oth | |
| 700 | 1 | |a Yang, Yan |4 oth | |
| 700 | 1 | |a Gan, Gongwen |4 oth | |
| 700 | 1 | |a Shi, Xiaolei |4 oth | |
| 700 | 1 | |a Liu, Cheng |4 oth | |
| 700 | 1 | |a Liao, Yulong |4 oth | |
| 700 | 1 | |a Jin, Lichuan |4 oth | |
| 700 | 1 | |a Zhang, Huaiwu |4 oth | |
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10.1016/j.jeurceramsoc.2021.01.033 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001783.pica (DE-627)ELV053557255 (ELSEVIER)S0955-2219(21)00049-2 DE-627 ger DE-627 rakwb eng 004 VZ 54.00 bkl Wang, Gang verfasserin aut Structural dependence of microwave dielectric performance of wolframite structured Mg1-xCaxZrNb2O8 ceramics: Crystal structure, microstructure evolution, Raman analysis and chemical bond theory 2021transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Raman vibration Elsevier Mg1-xCaxZrNb2O8 ceramics Elsevier Microstructure evolution Elsevier Chemical bond theory Elsevier Zhang, Dainan oth Li, Jie oth Shi, Liang oth Yang, Yan oth Gan, Gongwen oth Shi, Xiaolei oth Liu, Cheng oth Liao, Yulong oth Jin, Lichuan oth Zhang, Huaiwu oth Enthalten in Elsevier Science Zhang, Yuanyuan ELSEVIER Improved differential evolution for RSSD-based localization in Gaussian mixture noise 2023 Amsterdam [u.a.] (DE-627)ELV009961755 volume:41 year:2021 number:6 pages:3445-3451 extent:7 https://doi.org/10.1016/j.jeurceramsoc.2021.01.033 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 54.00 Informatik: Allgemeines VZ AR 41 2021 6 3445-3451 7 |
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10.1016/j.jeurceramsoc.2021.01.033 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001783.pica (DE-627)ELV053557255 (ELSEVIER)S0955-2219(21)00049-2 DE-627 ger DE-627 rakwb eng 004 VZ 54.00 bkl Wang, Gang verfasserin aut Structural dependence of microwave dielectric performance of wolframite structured Mg1-xCaxZrNb2O8 ceramics: Crystal structure, microstructure evolution, Raman analysis and chemical bond theory 2021transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Raman vibration Elsevier Mg1-xCaxZrNb2O8 ceramics Elsevier Microstructure evolution Elsevier Chemical bond theory Elsevier Zhang, Dainan oth Li, Jie oth Shi, Liang oth Yang, Yan oth Gan, Gongwen oth Shi, Xiaolei oth Liu, Cheng oth Liao, Yulong oth Jin, Lichuan oth Zhang, Huaiwu oth Enthalten in Elsevier Science Zhang, Yuanyuan ELSEVIER Improved differential evolution for RSSD-based localization in Gaussian mixture noise 2023 Amsterdam [u.a.] (DE-627)ELV009961755 volume:41 year:2021 number:6 pages:3445-3451 extent:7 https://doi.org/10.1016/j.jeurceramsoc.2021.01.033 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 54.00 Informatik: Allgemeines VZ AR 41 2021 6 3445-3451 7 |
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10.1016/j.jeurceramsoc.2021.01.033 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001783.pica (DE-627)ELV053557255 (ELSEVIER)S0955-2219(21)00049-2 DE-627 ger DE-627 rakwb eng 004 VZ 54.00 bkl Wang, Gang verfasserin aut Structural dependence of microwave dielectric performance of wolframite structured Mg1-xCaxZrNb2O8 ceramics: Crystal structure, microstructure evolution, Raman analysis and chemical bond theory 2021transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Raman vibration Elsevier Mg1-xCaxZrNb2O8 ceramics Elsevier Microstructure evolution Elsevier Chemical bond theory Elsevier Zhang, Dainan oth Li, Jie oth Shi, Liang oth Yang, Yan oth Gan, Gongwen oth Shi, Xiaolei oth Liu, Cheng oth Liao, Yulong oth Jin, Lichuan oth Zhang, Huaiwu oth Enthalten in Elsevier Science Zhang, Yuanyuan ELSEVIER Improved differential evolution for RSSD-based localization in Gaussian mixture noise 2023 Amsterdam [u.a.] (DE-627)ELV009961755 volume:41 year:2021 number:6 pages:3445-3451 extent:7 https://doi.org/10.1016/j.jeurceramsoc.2021.01.033 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 54.00 Informatik: Allgemeines VZ AR 41 2021 6 3445-3451 7 |
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10.1016/j.jeurceramsoc.2021.01.033 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001783.pica (DE-627)ELV053557255 (ELSEVIER)S0955-2219(21)00049-2 DE-627 ger DE-627 rakwb eng 004 VZ 54.00 bkl Wang, Gang verfasserin aut Structural dependence of microwave dielectric performance of wolframite structured Mg1-xCaxZrNb2O8 ceramics: Crystal structure, microstructure evolution, Raman analysis and chemical bond theory 2021transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Raman vibration Elsevier Mg1-xCaxZrNb2O8 ceramics Elsevier Microstructure evolution Elsevier Chemical bond theory Elsevier Zhang, Dainan oth Li, Jie oth Shi, Liang oth Yang, Yan oth Gan, Gongwen oth Shi, Xiaolei oth Liu, Cheng oth Liao, Yulong oth Jin, Lichuan oth Zhang, Huaiwu oth Enthalten in Elsevier Science Zhang, Yuanyuan ELSEVIER Improved differential evolution for RSSD-based localization in Gaussian mixture noise 2023 Amsterdam [u.a.] (DE-627)ELV009961755 volume:41 year:2021 number:6 pages:3445-3451 extent:7 https://doi.org/10.1016/j.jeurceramsoc.2021.01.033 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 54.00 Informatik: Allgemeines VZ AR 41 2021 6 3445-3451 7 |
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10.1016/j.jeurceramsoc.2021.01.033 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001783.pica (DE-627)ELV053557255 (ELSEVIER)S0955-2219(21)00049-2 DE-627 ger DE-627 rakwb eng 004 VZ 54.00 bkl Wang, Gang verfasserin aut Structural dependence of microwave dielectric performance of wolframite structured Mg1-xCaxZrNb2O8 ceramics: Crystal structure, microstructure evolution, Raman analysis and chemical bond theory 2021transfer abstract 7 nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. Raman vibration Elsevier Mg1-xCaxZrNb2O8 ceramics Elsevier Microstructure evolution Elsevier Chemical bond theory Elsevier Zhang, Dainan oth Li, Jie oth Shi, Liang oth Yang, Yan oth Gan, Gongwen oth Shi, Xiaolei oth Liu, Cheng oth Liao, Yulong oth Jin, Lichuan oth Zhang, Huaiwu oth Enthalten in Elsevier Science Zhang, Yuanyuan ELSEVIER Improved differential evolution for RSSD-based localization in Gaussian mixture noise 2023 Amsterdam [u.a.] (DE-627)ELV009961755 volume:41 year:2021 number:6 pages:3445-3451 extent:7 https://doi.org/10.1016/j.jeurceramsoc.2021.01.033 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 54.00 Informatik: Allgemeines VZ AR 41 2021 6 3445-3451 7 |
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structural dependence of microwave dielectric performance of wolframite structured mg1-xcaxzrnb2o8 ceramics: crystal structure, microstructure evolution, raman analysis and chemical bond theory |
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Structural dependence of microwave dielectric performance of wolframite structured Mg1-xCaxZrNb2O8 ceramics: Crystal structure, microstructure evolution, Raman analysis and chemical bond theory |
| abstract |
Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. |
| abstractGer |
Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. |
| abstract_unstemmed |
Wolframite-structured Mg1-xCaxZrNb2O8 (0−0.1) ceramics were synthesized through a solid-state procedure. Crystal refinement indicates a pure Mg1-xCaxZrNb2O8 ceramic with a wolframite structure. Ca2+ substitution led to the redshift of the Ag mode at approximately 896 cm−1. Additionally, Ca2+ substitution could promote grain growth and contribute to microstructure evolution from a polyhedral shape to a rod shape. According to chemical bond theory, an appropriate Ca2+ concentration can increase NbO bond iconicity and NbO bond lattice energy, which contributed to the great improvement in the dielectric constant and Q × f value. Additionally, the τf value was affected by the bond valence and thermal expansion coefficient of the MgO bond. The Mg1-xCaxZrNb2O8 (x = 0.04) ceramics exhibited great improvement in the Q × f value: εr = 25.21, Q × f = 116,000 GHz (7.17 GHz) and τf = −24.4 ppm/°C, which provides enormous potential for future millimeter-wave applications. |
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Structural dependence of microwave dielectric performance of wolframite structured Mg1-xCaxZrNb2O8 ceramics: Crystal structure, microstructure evolution, Raman analysis and chemical bond theory |
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Zhang, Dainan Li, Jie Shi, Liang Yang, Yan Gan, Gongwen Shi, Xiaolei Liu, Cheng Liao, Yulong Jin, Lichuan Zhang, Huaiwu |
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