Study on strain stiffening of non-colloidal suspension in oscillating shear by a subsequent steady shear test
Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Zhang, Anqi [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021transfer abstract |
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| Übergeordnetes Werk: |
Enthalten in: Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface - Ren, Guoqing ELSEVIER, 2018, an international journal devoted to the principles and applications of colloid and interface science, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:618 ; year:2021 ; day:5 ; month:06 ; pages:0 |
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| DOI / URN: |
10.1016/j.colsurfa.2021.126401 |
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| 520 | |a Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. | ||
| 520 | |a Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. | ||
| 650 | 7 | |a Non-colloidal suspension |2 Elsevier | |
| 650 | 7 | |a Strain stiffening |2 Elsevier | |
| 650 | 7 | |a Microstructure |2 Elsevier | |
| 650 | 7 | |a Oscillating and steady shear |2 Elsevier | |
| 700 | 1 | |a Zhu, Chenlin |4 oth | |
| 700 | 1 | |a Pan, Dingyi |4 oth | |
| 700 | 1 | |a Lin, Yuan |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier Science |a Ren, Guoqing ELSEVIER |t Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface |d 2018 |d an international journal devoted to the principles and applications of colloid and interface science |g Amsterdam [u.a.] |w (DE-627)ELV003763498 |
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10.1016/j.colsurfa.2021.126401 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001366.pica (DE-627)ELV05372612X (ELSEVIER)S0927-7757(21)00270-3 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Zhang, Anqi verfasserin aut Study on strain stiffening of non-colloidal suspension in oscillating shear by a subsequent steady shear test 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Non-colloidal suspension Elsevier Strain stiffening Elsevier Microstructure Elsevier Oscillating and steady shear Elsevier Zhu, Chenlin oth Pan, Dingyi oth Lin, Yuan oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:618 year:2021 day:5 month:06 pages:0 https://doi.org/10.1016/j.colsurfa.2021.126401 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 618 2021 5 0605 0 |
| spelling |
10.1016/j.colsurfa.2021.126401 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001366.pica (DE-627)ELV05372612X (ELSEVIER)S0927-7757(21)00270-3 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Zhang, Anqi verfasserin aut Study on strain stiffening of non-colloidal suspension in oscillating shear by a subsequent steady shear test 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Non-colloidal suspension Elsevier Strain stiffening Elsevier Microstructure Elsevier Oscillating and steady shear Elsevier Zhu, Chenlin oth Pan, Dingyi oth Lin, Yuan oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:618 year:2021 day:5 month:06 pages:0 https://doi.org/10.1016/j.colsurfa.2021.126401 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 618 2021 5 0605 0 |
| allfields_unstemmed |
10.1016/j.colsurfa.2021.126401 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001366.pica (DE-627)ELV05372612X (ELSEVIER)S0927-7757(21)00270-3 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Zhang, Anqi verfasserin aut Study on strain stiffening of non-colloidal suspension in oscillating shear by a subsequent steady shear test 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Non-colloidal suspension Elsevier Strain stiffening Elsevier Microstructure Elsevier Oscillating and steady shear Elsevier Zhu, Chenlin oth Pan, Dingyi oth Lin, Yuan oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:618 year:2021 day:5 month:06 pages:0 https://doi.org/10.1016/j.colsurfa.2021.126401 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 618 2021 5 0605 0 |
| allfieldsGer |
10.1016/j.colsurfa.2021.126401 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001366.pica (DE-627)ELV05372612X (ELSEVIER)S0927-7757(21)00270-3 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Zhang, Anqi verfasserin aut Study on strain stiffening of non-colloidal suspension in oscillating shear by a subsequent steady shear test 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Non-colloidal suspension Elsevier Strain stiffening Elsevier Microstructure Elsevier Oscillating and steady shear Elsevier Zhu, Chenlin oth Pan, Dingyi oth Lin, Yuan oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:618 year:2021 day:5 month:06 pages:0 https://doi.org/10.1016/j.colsurfa.2021.126401 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 618 2021 5 0605 0 |
| allfieldsSound |
10.1016/j.colsurfa.2021.126401 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001366.pica (DE-627)ELV05372612X (ELSEVIER)S0927-7757(21)00270-3 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Zhang, Anqi verfasserin aut Study on strain stiffening of non-colloidal suspension in oscillating shear by a subsequent steady shear test 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. Non-colloidal suspension Elsevier Strain stiffening Elsevier Microstructure Elsevier Oscillating and steady shear Elsevier Zhu, Chenlin oth Pan, Dingyi oth Lin, Yuan oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:618 year:2021 day:5 month:06 pages:0 https://doi.org/10.1016/j.colsurfa.2021.126401 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 618 2021 5 0605 0 |
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Enthalten in Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface Amsterdam [u.a.] volume:618 year:2021 day:5 month:06 pages:0 |
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With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear.</subfield></datafield><datafield tag="520" ind1=" " ind2=" "><subfield code="a">Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. 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Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface |
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study on strain stiffening of non-colloidal suspension in oscillating shear by a subsequent steady shear test |
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Study on strain stiffening of non-colloidal suspension in oscillating shear by a subsequent steady shear test |
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Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. |
| abstractGer |
Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. |
| abstract_unstemmed |
Rheological behavior of non-colloidal suspensions in oscillatory shear has been studied experimentally. With increase of strain amplitude, both storage and loss moduli first decrease and then increase at a critical point, which is called strain stiffening. Our experiment results show that suspension with small particles exhibit a larger modulus before the critical strain amplitude, and additional steady shear tests also show similar phenomenon. According to particle size distribution measurement, there is certain amount of small size particles which may have significant Brownian motion, and play a crucial role in shear thinning. Special experiment procedure is designed to investigate strain stiffening, two different tests of oscillating shear are parallel conducted and they are stopped at the strain amplitude corresponding to the critical point and peak point respectively. Both of them are further tested by a subsequent steady shear test (with constant shear rate) to inspect the internal particle structures. Samples with oscillating tests stopped at the critical point and peak point show similar magnitudes of shear viscosity in the steady shear tests. It is conjectured that particles in non-colloidal suspension exist as a metastable structure during strain stiffening, which can maintain a relatively stable configuration in oscillatory shear, but the structure will be broken rapidly in steady shear with the increase of shear rate. As a result of this, the metastable structure only affects the modulus in oscillatory shear, but does not affect the viscosity of steady shear. |
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Study on strain stiffening of non-colloidal suspension in oscillating shear by a subsequent steady shear test |
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