Facile synthesis of ZSM-5 mesocrystal via novel pathway of crystallization: Fast precipitation, deconstruction and reorganization
Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods....
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Jiang, Tao [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021transfer abstract |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Impact of North Atlantic-East Asian teleconnections on extremely high January PM - Kim, Jeong-Hun ELSEVIER, 2021, the official journal of the International Zeolite Association, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:321 ; year:2021 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.micromeso.2021.111112 |
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| 520 | |a Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. | ||
| 520 | |a Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. | ||
| 650 | 7 | |a Tunable Si/Al |2 Elsevier | |
| 650 | 7 | |a Claisen‐Schmidt condensation |2 Elsevier | |
| 650 | 7 | |a Mesocrystal |2 Elsevier | |
| 650 | 7 | |a ZSM-5 |2 Elsevier | |
| 650 | 7 | |a Nonclassical crystallization |2 Elsevier | |
| 700 | 1 | |a Wang, Fumin |4 oth | |
| 700 | 1 | |a Zhang, Xubin |4 oth | |
| 700 | 1 | |a Zhai, Yi |4 oth | |
| 700 | 1 | |a Lv, Guojun |4 oth | |
| 700 | 1 | |a Shen, Yu |4 oth | |
| 700 | 1 | |a Wu, Yuzhou |4 oth | |
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10.1016/j.micromeso.2021.111112 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001397.pica (DE-627)ELV05408704X (ELSEVIER)S1387-1811(21)00238-9 DE-627 ger DE-627 rakwb eng 333.7 570 690 VZ BIODIV DE-30 fid 48.00 bkl Jiang, Tao verfasserin aut Facile synthesis of ZSM-5 mesocrystal via novel pathway of crystallization: Fast precipitation, deconstruction and reorganization 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Tunable Si/Al Elsevier Claisen‐Schmidt condensation Elsevier Mesocrystal Elsevier ZSM-5 Elsevier Nonclassical crystallization Elsevier Wang, Fumin oth Zhang, Xubin oth Zhai, Yi oth Lv, Guojun oth Shen, Yu oth Wu, Yuzhou oth Enthalten in Elsevier Kim, Jeong-Hun ELSEVIER Impact of North Atlantic-East Asian teleconnections on extremely high January PM 2021 the official journal of the International Zeolite Association Amsterdam [u.a.] (DE-627)ELV006778283 volume:321 year:2021 pages:0 https://doi.org/10.1016/j.micromeso.2021.111112 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA SSG-OPC-FOR 48.00 Land- und Forstwirtschaft: Allgemeines VZ AR 321 2021 0 |
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10.1016/j.micromeso.2021.111112 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001397.pica (DE-627)ELV05408704X (ELSEVIER)S1387-1811(21)00238-9 DE-627 ger DE-627 rakwb eng 333.7 570 690 VZ BIODIV DE-30 fid 48.00 bkl Jiang, Tao verfasserin aut Facile synthesis of ZSM-5 mesocrystal via novel pathway of crystallization: Fast precipitation, deconstruction and reorganization 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Tunable Si/Al Elsevier Claisen‐Schmidt condensation Elsevier Mesocrystal Elsevier ZSM-5 Elsevier Nonclassical crystallization Elsevier Wang, Fumin oth Zhang, Xubin oth Zhai, Yi oth Lv, Guojun oth Shen, Yu oth Wu, Yuzhou oth Enthalten in Elsevier Kim, Jeong-Hun ELSEVIER Impact of North Atlantic-East Asian teleconnections on extremely high January PM 2021 the official journal of the International Zeolite Association Amsterdam [u.a.] (DE-627)ELV006778283 volume:321 year:2021 pages:0 https://doi.org/10.1016/j.micromeso.2021.111112 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA SSG-OPC-FOR 48.00 Land- und Forstwirtschaft: Allgemeines VZ AR 321 2021 0 |
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10.1016/j.micromeso.2021.111112 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001397.pica (DE-627)ELV05408704X (ELSEVIER)S1387-1811(21)00238-9 DE-627 ger DE-627 rakwb eng 333.7 570 690 VZ BIODIV DE-30 fid 48.00 bkl Jiang, Tao verfasserin aut Facile synthesis of ZSM-5 mesocrystal via novel pathway of crystallization: Fast precipitation, deconstruction and reorganization 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Tunable Si/Al Elsevier Claisen‐Schmidt condensation Elsevier Mesocrystal Elsevier ZSM-5 Elsevier Nonclassical crystallization Elsevier Wang, Fumin oth Zhang, Xubin oth Zhai, Yi oth Lv, Guojun oth Shen, Yu oth Wu, Yuzhou oth Enthalten in Elsevier Kim, Jeong-Hun ELSEVIER Impact of North Atlantic-East Asian teleconnections on extremely high January PM 2021 the official journal of the International Zeolite Association Amsterdam [u.a.] (DE-627)ELV006778283 volume:321 year:2021 pages:0 https://doi.org/10.1016/j.micromeso.2021.111112 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA SSG-OPC-FOR 48.00 Land- und Forstwirtschaft: Allgemeines VZ AR 321 2021 0 |
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10.1016/j.micromeso.2021.111112 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001397.pica (DE-627)ELV05408704X (ELSEVIER)S1387-1811(21)00238-9 DE-627 ger DE-627 rakwb eng 333.7 570 690 VZ BIODIV DE-30 fid 48.00 bkl Jiang, Tao verfasserin aut Facile synthesis of ZSM-5 mesocrystal via novel pathway of crystallization: Fast precipitation, deconstruction and reorganization 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Tunable Si/Al Elsevier Claisen‐Schmidt condensation Elsevier Mesocrystal Elsevier ZSM-5 Elsevier Nonclassical crystallization Elsevier Wang, Fumin oth Zhang, Xubin oth Zhai, Yi oth Lv, Guojun oth Shen, Yu oth Wu, Yuzhou oth Enthalten in Elsevier Kim, Jeong-Hun ELSEVIER Impact of North Atlantic-East Asian teleconnections on extremely high January PM 2021 the official journal of the International Zeolite Association Amsterdam [u.a.] (DE-627)ELV006778283 volume:321 year:2021 pages:0 https://doi.org/10.1016/j.micromeso.2021.111112 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA SSG-OPC-FOR 48.00 Land- und Forstwirtschaft: Allgemeines VZ AR 321 2021 0 |
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10.1016/j.micromeso.2021.111112 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001397.pica (DE-627)ELV05408704X (ELSEVIER)S1387-1811(21)00238-9 DE-627 ger DE-627 rakwb eng 333.7 570 690 VZ BIODIV DE-30 fid 48.00 bkl Jiang, Tao verfasserin aut Facile synthesis of ZSM-5 mesocrystal via novel pathway of crystallization: Fast precipitation, deconstruction and reorganization 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. Tunable Si/Al Elsevier Claisen‐Schmidt condensation Elsevier Mesocrystal Elsevier ZSM-5 Elsevier Nonclassical crystallization Elsevier Wang, Fumin oth Zhang, Xubin oth Zhai, Yi oth Lv, Guojun oth Shen, Yu oth Wu, Yuzhou oth Enthalten in Elsevier Kim, Jeong-Hun ELSEVIER Impact of North Atlantic-East Asian teleconnections on extremely high January PM 2021 the official journal of the International Zeolite Association Amsterdam [u.a.] (DE-627)ELV006778283 volume:321 year:2021 pages:0 https://doi.org/10.1016/j.micromeso.2021.111112 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-BIODIV SSG-OLC-PHA SSG-OPC-FOR 48.00 Land- und Forstwirtschaft: Allgemeines VZ AR 321 2021 0 |
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Enthalten in Impact of North Atlantic-East Asian teleconnections on extremely high January PM Amsterdam [u.a.] volume:321 year:2021 pages:0 |
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Facile synthesis of ZSM-5 mesocrystal via novel pathway of crystallization: Fast precipitation, deconstruction and reorganization |
| abstract |
Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. |
| abstractGer |
Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. |
| abstract_unstemmed |
Mesocrystal zeolite with well-defined morphology owns mesoporous channels and single crystal characteristics, which could promote diffusion efficiency, stability and catalytic activity. Thus, we performed the controllable synthesis of ZSM-5 mesocrystal without special additives and complex methods. Selected area electron diffraction (SAED) and fast Fourier transform (FFT) showed diffraction spots regardless of crystallization time, which indicated the well oriented feature of synthesized ZSM-5 zeolites. The crystallization process was further investigated. The oriented particle attachment (OPA) effectively guided the synthesis process of mesocrystals, which followed the nonclassical crystallization mechanism. The crystallinity curve exhibited valley-like shape, which manifested that the crystallization pathway went through three stages: fast precipitation, deconstruction and reorganization. The plausible formation mechanism was proposed, which might be useful for the fabrication of ZSM-5 mesocrystal. The prepared zeolites showed superior catalytic performance in aldol condensation reaction between benzaldehyde and 2-hydroxyacetophenone, obtaining 93% of the conversion. |
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