Synthesis and properties of hydrophobically associating polymer fracturing fluid
The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl tr...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Ma, Xiping [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2021transfer abstract |
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| Übergeordnetes Werk: |
Enthalten in: Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface - Ren, Guoqing ELSEVIER, 2018, an international journal devoted to the principles and applications of colloid and interface science, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:626 ; year:2021 ; day:5 ; month:10 ; pages:0 |
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| DOI / URN: |
10.1016/j.colsurfa.2021.127013 |
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ELV054888719 |
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| 520 | |a The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. | ||
| 520 | |a The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. | ||
| 650 | 7 | |a Synthesis |2 Elsevier | |
| 650 | 7 | |a Polymer |2 Elsevier | |
| 650 | 7 | |a Crosslinking |2 Elsevier | |
| 650 | 7 | |a Hydrophobic monomer |2 Elsevier | |
| 650 | 7 | |a Fracturing fluid |2 Elsevier | |
| 650 | 7 | |a Performance |2 Elsevier | |
| 700 | 1 | |a Mu, Hongli |4 oth | |
| 700 | 1 | |a Hu, Yingying |4 oth | |
| 700 | 1 | |a Yang, Shengwen |4 oth | |
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2021 |
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10.1016/j.colsurfa.2021.127013 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001481.pica (DE-627)ELV054888719 (ELSEVIER)S0927-7757(21)00882-7 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Ma, Xiping verfasserin aut Synthesis and properties of hydrophobically associating polymer fracturing fluid 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. Synthesis Elsevier Polymer Elsevier Crosslinking Elsevier Hydrophobic monomer Elsevier Fracturing fluid Elsevier Performance Elsevier Mu, Hongli oth Hu, Yingying oth Yang, Shengwen oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:626 year:2021 day:5 month:10 pages:0 https://doi.org/10.1016/j.colsurfa.2021.127013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 626 2021 5 1005 0 |
| spelling |
10.1016/j.colsurfa.2021.127013 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001481.pica (DE-627)ELV054888719 (ELSEVIER)S0927-7757(21)00882-7 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Ma, Xiping verfasserin aut Synthesis and properties of hydrophobically associating polymer fracturing fluid 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. Synthesis Elsevier Polymer Elsevier Crosslinking Elsevier Hydrophobic monomer Elsevier Fracturing fluid Elsevier Performance Elsevier Mu, Hongli oth Hu, Yingying oth Yang, Shengwen oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:626 year:2021 day:5 month:10 pages:0 https://doi.org/10.1016/j.colsurfa.2021.127013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 626 2021 5 1005 0 |
| allfields_unstemmed |
10.1016/j.colsurfa.2021.127013 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001481.pica (DE-627)ELV054888719 (ELSEVIER)S0927-7757(21)00882-7 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Ma, Xiping verfasserin aut Synthesis and properties of hydrophobically associating polymer fracturing fluid 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. Synthesis Elsevier Polymer Elsevier Crosslinking Elsevier Hydrophobic monomer Elsevier Fracturing fluid Elsevier Performance Elsevier Mu, Hongli oth Hu, Yingying oth Yang, Shengwen oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:626 year:2021 day:5 month:10 pages:0 https://doi.org/10.1016/j.colsurfa.2021.127013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 626 2021 5 1005 0 |
| allfieldsGer |
10.1016/j.colsurfa.2021.127013 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001481.pica (DE-627)ELV054888719 (ELSEVIER)S0927-7757(21)00882-7 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Ma, Xiping verfasserin aut Synthesis and properties of hydrophobically associating polymer fracturing fluid 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. Synthesis Elsevier Polymer Elsevier Crosslinking Elsevier Hydrophobic monomer Elsevier Fracturing fluid Elsevier Performance Elsevier Mu, Hongli oth Hu, Yingying oth Yang, Shengwen oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:626 year:2021 day:5 month:10 pages:0 https://doi.org/10.1016/j.colsurfa.2021.127013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 626 2021 5 1005 0 |
| allfieldsSound |
10.1016/j.colsurfa.2021.127013 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001481.pica (DE-627)ELV054888719 (ELSEVIER)S0927-7757(21)00882-7 DE-627 ger DE-627 rakwb eng 540 VZ 35.10 bkl Ma, Xiping verfasserin aut Synthesis and properties of hydrophobically associating polymer fracturing fluid 2021transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. Synthesis Elsevier Polymer Elsevier Crosslinking Elsevier Hydrophobic monomer Elsevier Fracturing fluid Elsevier Performance Elsevier Mu, Hongli oth Hu, Yingying oth Yang, Shengwen oth Enthalten in Elsevier Science Ren, Guoqing ELSEVIER Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface 2018 an international journal devoted to the principles and applications of colloid and interface science Amsterdam [u.a.] (DE-627)ELV003763498 volume:626 year:2021 day:5 month:10 pages:0 https://doi.org/10.1016/j.colsurfa.2021.127013 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA 35.10 Physikalische Chemie: Allgemeines VZ AR 626 2021 5 1005 0 |
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Enthalten in Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface Amsterdam [u.a.] volume:626 year:2021 day:5 month:10 pages:0 |
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Reaction mechanism investigation of furfural conversion to 2-methylfuran on Cu(1 1 1) surface |
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synthesis and properties of hydrophobically associating polymer fracturing fluid |
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Synthesis and properties of hydrophobically associating polymer fracturing fluid |
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The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. |
| abstractGer |
The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. |
| abstract_unstemmed |
The double tailed hydrophobic monomer PMB-16 was synthesized by the reaction of phenylethylamine,1-bromohexadecane and methacryloyl chloride. The ternary hydrophobic association polymer (PADM) was synthesized by free radical copolymerization of PMB-16 with acrylamide (AM) and methacryloyloxyethyl trimethylammonium chloride (DMC). The optimum synthesis conditions were as follows, the mass ratio of m (AM):m (DMC):m (PMB-16) was 80:19.6:0.4, the total monomer concentration was 35.0 wt%, the amount of initiator (V50) was 0.1 wt% of the total mass of monomer, the reaction temperature was 55 °C, the reaction time was 6.0 h, the system pH was 7, and the amount of metal ion chelating agent (EDTA-4Na) was 0.01 wt% of the total mass of monomer. The results of performance evaluation showed that PADM aqueous solution had excellent temperature and salt resistance. Using zirconium acetylacetonate as crosslinking agent, the mass crosslinking ratio of PADM solution to zirconium acetylacetonate was 100:0.9, the crosslinking temperature was 60 °C, and the pH value was 6.0. The system presented good thickening, temperature resistance, shear stability and low residue content, so it was a low damage fracturing fluid. |
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Synthesis and properties of hydrophobically associating polymer fracturing fluid |
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