Abnormal reduction and luminescence properties of Sm2+-doped Sr5(PO4)3Cl prepared by solution combustion synthesis
Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Wei, Donglei [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022transfer abstract |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: New ablation evolution behaviors in micro-hole drilling of 2.5D C - Liu, Chang ELSEVIER, 2021, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:241 ; year:2022 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.jlumin.2021.118514 |
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ELV055951724 |
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| 245 | 1 | 0 | |a Abnormal reduction and luminescence properties of Sm2+-doped Sr5(PO4)3Cl prepared by solution combustion synthesis |
| 264 | 1 | |c 2022transfer abstract | |
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| 520 | |a Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. | ||
| 520 | |a Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. | ||
| 650 | 7 | |a Inorganic compounds |2 Elsevier | |
| 650 | 7 | |a Sm2+ |2 Elsevier | |
| 650 | 7 | |a Luminescence |2 Elsevier | |
| 650 | 7 | |a Sr5(PO4)3Cl |2 Elsevier | |
| 650 | 7 | |a Phosphor |2 Elsevier | |
| 700 | 1 | |a Yang, Xifeng |4 oth | |
| 700 | 1 | |a Liu, Yushen |4 oth | |
| 700 | 1 | |a Seo, Hyo Jin |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier |a Liu, Chang ELSEVIER |t New ablation evolution behaviors in micro-hole drilling of 2.5D C |d 2021 |g New York, NY [u.a.] |w (DE-627)ELV00662605X |
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10.1016/j.jlumin.2021.118514 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001608.pica (DE-627)ELV055951724 (ELSEVIER)S0022-2313(21)00630-X DE-627 ger DE-627 rakwb eng 670 VZ 51.60 bkl 58.45 bkl Wei, Donglei verfasserin aut Abnormal reduction and luminescence properties of Sm2+-doped Sr5(PO4)3Cl prepared by solution combustion synthesis 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Inorganic compounds Elsevier Sm2+ Elsevier Luminescence Elsevier Sr5(PO4)3Cl Elsevier Phosphor Elsevier Yang, Xifeng oth Liu, Yushen oth Seo, Hyo Jin oth Enthalten in Elsevier Liu, Chang ELSEVIER New ablation evolution behaviors in micro-hole drilling of 2.5D C 2021 New York, NY [u.a.] (DE-627)ELV00662605X volume:241 year:2022 pages:0 https://doi.org/10.1016/j.jlumin.2021.118514 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde VZ 58.45 Gesteinshüttenkunde VZ AR 241 2022 0 |
| spelling |
10.1016/j.jlumin.2021.118514 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001608.pica (DE-627)ELV055951724 (ELSEVIER)S0022-2313(21)00630-X DE-627 ger DE-627 rakwb eng 670 VZ 51.60 bkl 58.45 bkl Wei, Donglei verfasserin aut Abnormal reduction and luminescence properties of Sm2+-doped Sr5(PO4)3Cl prepared by solution combustion synthesis 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Inorganic compounds Elsevier Sm2+ Elsevier Luminescence Elsevier Sr5(PO4)3Cl Elsevier Phosphor Elsevier Yang, Xifeng oth Liu, Yushen oth Seo, Hyo Jin oth Enthalten in Elsevier Liu, Chang ELSEVIER New ablation evolution behaviors in micro-hole drilling of 2.5D C 2021 New York, NY [u.a.] (DE-627)ELV00662605X volume:241 year:2022 pages:0 https://doi.org/10.1016/j.jlumin.2021.118514 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde VZ 58.45 Gesteinshüttenkunde VZ AR 241 2022 0 |
| allfields_unstemmed |
10.1016/j.jlumin.2021.118514 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001608.pica (DE-627)ELV055951724 (ELSEVIER)S0022-2313(21)00630-X DE-627 ger DE-627 rakwb eng 670 VZ 51.60 bkl 58.45 bkl Wei, Donglei verfasserin aut Abnormal reduction and luminescence properties of Sm2+-doped Sr5(PO4)3Cl prepared by solution combustion synthesis 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Inorganic compounds Elsevier Sm2+ Elsevier Luminescence Elsevier Sr5(PO4)3Cl Elsevier Phosphor Elsevier Yang, Xifeng oth Liu, Yushen oth Seo, Hyo Jin oth Enthalten in Elsevier Liu, Chang ELSEVIER New ablation evolution behaviors in micro-hole drilling of 2.5D C 2021 New York, NY [u.a.] (DE-627)ELV00662605X volume:241 year:2022 pages:0 https://doi.org/10.1016/j.jlumin.2021.118514 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde VZ 58.45 Gesteinshüttenkunde VZ AR 241 2022 0 |
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10.1016/j.jlumin.2021.118514 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001608.pica (DE-627)ELV055951724 (ELSEVIER)S0022-2313(21)00630-X DE-627 ger DE-627 rakwb eng 670 VZ 51.60 bkl 58.45 bkl Wei, Donglei verfasserin aut Abnormal reduction and luminescence properties of Sm2+-doped Sr5(PO4)3Cl prepared by solution combustion synthesis 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Inorganic compounds Elsevier Sm2+ Elsevier Luminescence Elsevier Sr5(PO4)3Cl Elsevier Phosphor Elsevier Yang, Xifeng oth Liu, Yushen oth Seo, Hyo Jin oth Enthalten in Elsevier Liu, Chang ELSEVIER New ablation evolution behaviors in micro-hole drilling of 2.5D C 2021 New York, NY [u.a.] (DE-627)ELV00662605X volume:241 year:2022 pages:0 https://doi.org/10.1016/j.jlumin.2021.118514 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde VZ 58.45 Gesteinshüttenkunde VZ AR 241 2022 0 |
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10.1016/j.jlumin.2021.118514 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001608.pica (DE-627)ELV055951724 (ELSEVIER)S0022-2313(21)00630-X DE-627 ger DE-627 rakwb eng 670 VZ 51.60 bkl 58.45 bkl Wei, Donglei verfasserin aut Abnormal reduction and luminescence properties of Sm2+-doped Sr5(PO4)3Cl prepared by solution combustion synthesis 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. Inorganic compounds Elsevier Sm2+ Elsevier Luminescence Elsevier Sr5(PO4)3Cl Elsevier Phosphor Elsevier Yang, Xifeng oth Liu, Yushen oth Seo, Hyo Jin oth Enthalten in Elsevier Liu, Chang ELSEVIER New ablation evolution behaviors in micro-hole drilling of 2.5D C 2021 New York, NY [u.a.] (DE-627)ELV00662605X volume:241 year:2022 pages:0 https://doi.org/10.1016/j.jlumin.2021.118514 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U 51.60 Keramische Werkstoffe Hartstoffe Werkstoffkunde VZ 58.45 Gesteinshüttenkunde VZ AR 241 2022 0 |
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abnormal reduction and luminescence properties of sm2+-doped sr5(po4)3cl prepared by solution combustion synthesis |
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Abnormal reduction and luminescence properties of Sm2+-doped Sr5(PO4)3Cl prepared by solution combustion synthesis |
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Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. |
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Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. |
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Sm-doped Sr5(PO4)3Cl was prepared by a solution combustion synthesis in the air atmosphere. The pure hexagonal phases of the samples were confirmed via the XRD, Raman, and FT-IR measurements. The typical microrod shape of the products was also demonstrated by SEM, TEM, and HRTEM images. The spectral properties and lifetimes were applied to characterize the luminescence of the samples as-prepared and subsequently heated in the air atmosphere. The luminescence of as-prepared Sm-doped Sr5(PO4)3Cl contains a broad emission band and a group of narrow lines, which are ascribed to the radiative transitions of 4f5d→4f and 5D0→7FJ (J = 0, 1, 2) of Sm2+ ions, respectively. It indicates that the Sm3+ can be successfully reduced to Sm2+ ions in hexagonal Sr5(PO4)3Cl prepared by combustion synthesis. The temperature dependent luminescence spectra and decay curves of Sm2+ were measured in a very wide temperature region from 10 K to 300 K. The thermal quenching and activation energy of Sm2+ doped Sr5(PO4)3Cl were reported. The crystal field energy level diagram and excitation mechanism of Sm2+ ions-doped Sr5(PO4)3Cl were characterized by the high resolution luminescence at low temperature. The luminescence of Sm2+ in Sr5(PO4)3Cl shows a great dependence on heating temperature in the air atmosphere (50–700 °C). The heating treatments at the elevated temperature depress Sm2+ emission along with the appearance of Sm3+ ions. The temperature-induced changes in the modification of the spectral components could be applied as potential luminescence thermometry. |
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