Metals concentrations in transitional and coastal waters by ICPMS and voltammetry analysis of spot samples and passive samplers (DGT)
This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Caetano, Miguel [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022transfer abstract |
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| Übergeordnetes Werk: |
Enthalten in: Purification and mass spectrometry study of Maillard reaction impurities in five acyclic nucleoside antiviral drugs - Lai, Xiaohong ELSEVIER, 2022, the international journal for marine environmental scientists, engineers, administrators, politicians and lawyers, Amsterdam [u.a.] |
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| Übergeordnetes Werk: |
volume:179 ; year:2022 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.marpolbul.2022.113715 |
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| 520 | |a This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. | ||
| 520 | |a This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. | ||
| 700 | 1 | |a Correia dos Santos, Margarida M. |4 oth | |
| 700 | 1 | |a Rosa, Nuno |4 oth | |
| 700 | 1 | |a Carvalho, Inês |4 oth | |
| 700 | 1 | |a Rodríguez, José Germán |4 oth | |
| 700 | 1 | |a Belzunce-Segarra, María Jesús |4 oth | |
| 700 | 1 | |a Menchaca, Iratxe |4 oth | |
| 700 | 1 | |a Larreta, Joana |4 oth | |
| 700 | 1 | |a Sanz, Marta Rodrigo |4 oth | |
| 700 | 1 | |a Millán-Gabet, Vanessa |4 oth | |
| 700 | 1 | |a Gonzalez, Jean-Louis |4 oth | |
| 700 | 1 | |a Amouroux, Isabelle |4 oth | |
| 700 | 1 | |a Guesdon, Stephane |4 oth | |
| 700 | 1 | |a Menet-Nédélec, Florence |4 oth | |
| 700 | 1 | |a White, Blánaid |4 oth | |
| 700 | 1 | |a Regan, Fiona |4 oth | |
| 700 | 1 | |a Nolan, Martin |4 oth | |
| 700 | 1 | |a McHugh, Brendan |4 oth | |
| 700 | 1 | |a Bersuder, Philippe |4 oth | |
| 700 | 1 | |a Bolam, Thi |4 oth | |
| 700 | 1 | |a Robinson, Craig D. |4 oth | |
| 700 | 1 | |a Fones, Gary R. |4 oth | |
| 700 | 1 | |a Zhang, Hao |4 oth | |
| 700 | 1 | |a Schintu, Marco |4 oth | |
| 700 | 1 | |a Montero, Natalia |4 oth | |
| 700 | 1 | |a Marras, Barbara |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier Science |a Lai, Xiaohong ELSEVIER |t Purification and mass spectrometry study of Maillard reaction impurities in five acyclic nucleoside antiviral drugs |d 2022 |d the international journal for marine environmental scientists, engineers, administrators, politicians and lawyers |g Amsterdam [u.a.] |w (DE-627)ELV007549504 |
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10.1016/j.marpolbul.2022.113715 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001951.pica (DE-627)ELV057765294 (ELSEVIER)S0025-326X(22)00397-6 DE-627 ger DE-627 rakwb eng 610 VZ 15,3 ssgn PHARM DE-84 fid 44.40 bkl Caetano, Miguel verfasserin aut Metals concentrations in transitional and coastal waters by ICPMS and voltammetry analysis of spot samples and passive samplers (DGT) 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. Correia dos Santos, Margarida M. oth Rosa, Nuno oth Carvalho, Inês oth Rodríguez, José Germán oth Belzunce-Segarra, María Jesús oth Menchaca, Iratxe oth Larreta, Joana oth Sanz, Marta Rodrigo oth Millán-Gabet, Vanessa oth Gonzalez, Jean-Louis oth Amouroux, Isabelle oth Guesdon, Stephane oth Menet-Nédélec, Florence oth White, Blánaid oth Regan, Fiona oth Nolan, Martin oth McHugh, Brendan oth Bersuder, Philippe oth Bolam, Thi oth Robinson, Craig D. oth Fones, Gary R. oth Zhang, Hao oth Schintu, Marco oth Montero, Natalia oth Marras, Barbara oth Enthalten in Elsevier Science Lai, Xiaohong ELSEVIER Purification and mass spectrometry study of Maillard reaction impurities in five acyclic nucleoside antiviral drugs 2022 the international journal for marine environmental scientists, engineers, administrators, politicians and lawyers Amsterdam [u.a.] (DE-627)ELV007549504 volume:179 year:2022 pages:0 https://doi.org/10.1016/j.marpolbul.2022.113715 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-PHARM SSG-OLC-PHA SSG-OPC-PHA 44.40 Pharmazie Pharmazeutika VZ AR 179 2022 0 |
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10.1016/j.marpolbul.2022.113715 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001951.pica (DE-627)ELV057765294 (ELSEVIER)S0025-326X(22)00397-6 DE-627 ger DE-627 rakwb eng 610 VZ 15,3 ssgn PHARM DE-84 fid 44.40 bkl Caetano, Miguel verfasserin aut Metals concentrations in transitional and coastal waters by ICPMS and voltammetry analysis of spot samples and passive samplers (DGT) 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. Correia dos Santos, Margarida M. oth Rosa, Nuno oth Carvalho, Inês oth Rodríguez, José Germán oth Belzunce-Segarra, María Jesús oth Menchaca, Iratxe oth Larreta, Joana oth Sanz, Marta Rodrigo oth Millán-Gabet, Vanessa oth Gonzalez, Jean-Louis oth Amouroux, Isabelle oth Guesdon, Stephane oth Menet-Nédélec, Florence oth White, Blánaid oth Regan, Fiona oth Nolan, Martin oth McHugh, Brendan oth Bersuder, Philippe oth Bolam, Thi oth Robinson, Craig D. oth Fones, Gary R. oth Zhang, Hao oth Schintu, Marco oth Montero, Natalia oth Marras, Barbara oth Enthalten in Elsevier Science Lai, Xiaohong ELSEVIER Purification and mass spectrometry study of Maillard reaction impurities in five acyclic nucleoside antiviral drugs 2022 the international journal for marine environmental scientists, engineers, administrators, politicians and lawyers Amsterdam [u.a.] (DE-627)ELV007549504 volume:179 year:2022 pages:0 https://doi.org/10.1016/j.marpolbul.2022.113715 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-PHARM SSG-OLC-PHA SSG-OPC-PHA 44.40 Pharmazie Pharmazeutika VZ AR 179 2022 0 |
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10.1016/j.marpolbul.2022.113715 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001951.pica (DE-627)ELV057765294 (ELSEVIER)S0025-326X(22)00397-6 DE-627 ger DE-627 rakwb eng 610 VZ 15,3 ssgn PHARM DE-84 fid 44.40 bkl Caetano, Miguel verfasserin aut Metals concentrations in transitional and coastal waters by ICPMS and voltammetry analysis of spot samples and passive samplers (DGT) 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. Correia dos Santos, Margarida M. oth Rosa, Nuno oth Carvalho, Inês oth Rodríguez, José Germán oth Belzunce-Segarra, María Jesús oth Menchaca, Iratxe oth Larreta, Joana oth Sanz, Marta Rodrigo oth Millán-Gabet, Vanessa oth Gonzalez, Jean-Louis oth Amouroux, Isabelle oth Guesdon, Stephane oth Menet-Nédélec, Florence oth White, Blánaid oth Regan, Fiona oth Nolan, Martin oth McHugh, Brendan oth Bersuder, Philippe oth Bolam, Thi oth Robinson, Craig D. oth Fones, Gary R. oth Zhang, Hao oth Schintu, Marco oth Montero, Natalia oth Marras, Barbara oth Enthalten in Elsevier Science Lai, Xiaohong ELSEVIER Purification and mass spectrometry study of Maillard reaction impurities in five acyclic nucleoside antiviral drugs 2022 the international journal for marine environmental scientists, engineers, administrators, politicians and lawyers Amsterdam [u.a.] (DE-627)ELV007549504 volume:179 year:2022 pages:0 https://doi.org/10.1016/j.marpolbul.2022.113715 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-PHARM SSG-OLC-PHA SSG-OPC-PHA 44.40 Pharmazie Pharmazeutika VZ AR 179 2022 0 |
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10.1016/j.marpolbul.2022.113715 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001951.pica (DE-627)ELV057765294 (ELSEVIER)S0025-326X(22)00397-6 DE-627 ger DE-627 rakwb eng 610 VZ 15,3 ssgn PHARM DE-84 fid 44.40 bkl Caetano, Miguel verfasserin aut Metals concentrations in transitional and coastal waters by ICPMS and voltammetry analysis of spot samples and passive samplers (DGT) 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. Correia dos Santos, Margarida M. oth Rosa, Nuno oth Carvalho, Inês oth Rodríguez, José Germán oth Belzunce-Segarra, María Jesús oth Menchaca, Iratxe oth Larreta, Joana oth Sanz, Marta Rodrigo oth Millán-Gabet, Vanessa oth Gonzalez, Jean-Louis oth Amouroux, Isabelle oth Guesdon, Stephane oth Menet-Nédélec, Florence oth White, Blánaid oth Regan, Fiona oth Nolan, Martin oth McHugh, Brendan oth Bersuder, Philippe oth Bolam, Thi oth Robinson, Craig D. oth Fones, Gary R. oth Zhang, Hao oth Schintu, Marco oth Montero, Natalia oth Marras, Barbara oth Enthalten in Elsevier Science Lai, Xiaohong ELSEVIER Purification and mass spectrometry study of Maillard reaction impurities in five acyclic nucleoside antiviral drugs 2022 the international journal for marine environmental scientists, engineers, administrators, politicians and lawyers Amsterdam [u.a.] (DE-627)ELV007549504 volume:179 year:2022 pages:0 https://doi.org/10.1016/j.marpolbul.2022.113715 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-PHARM SSG-OLC-PHA SSG-OPC-PHA 44.40 Pharmazie Pharmazeutika VZ AR 179 2022 0 |
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10.1016/j.marpolbul.2022.113715 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001951.pica (DE-627)ELV057765294 (ELSEVIER)S0025-326X(22)00397-6 DE-627 ger DE-627 rakwb eng 610 VZ 15,3 ssgn PHARM DE-84 fid 44.40 bkl Caetano, Miguel verfasserin aut Metals concentrations in transitional and coastal waters by ICPMS and voltammetry analysis of spot samples and passive samplers (DGT) 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. Correia dos Santos, Margarida M. oth Rosa, Nuno oth Carvalho, Inês oth Rodríguez, José Germán oth Belzunce-Segarra, María Jesús oth Menchaca, Iratxe oth Larreta, Joana oth Sanz, Marta Rodrigo oth Millán-Gabet, Vanessa oth Gonzalez, Jean-Louis oth Amouroux, Isabelle oth Guesdon, Stephane oth Menet-Nédélec, Florence oth White, Blánaid oth Regan, Fiona oth Nolan, Martin oth McHugh, Brendan oth Bersuder, Philippe oth Bolam, Thi oth Robinson, Craig D. oth Fones, Gary R. oth Zhang, Hao oth Schintu, Marco oth Montero, Natalia oth Marras, Barbara oth Enthalten in Elsevier Science Lai, Xiaohong ELSEVIER Purification and mass spectrometry study of Maillard reaction impurities in five acyclic nucleoside antiviral drugs 2022 the international journal for marine environmental scientists, engineers, administrators, politicians and lawyers Amsterdam [u.a.] (DE-627)ELV007549504 volume:179 year:2022 pages:0 https://doi.org/10.1016/j.marpolbul.2022.113715 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U FID-PHARM SSG-OLC-PHA SSG-OPC-PHA 44.40 Pharmazie Pharmazeutika VZ AR 179 2022 0 |
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Purification and mass spectrometry study of Maillard reaction impurities in five acyclic nucleoside antiviral drugs |
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Caetano, Miguel @@aut@@ Correia dos Santos, Margarida M. @@oth@@ Rosa, Nuno @@oth@@ Carvalho, Inês @@oth@@ Rodríguez, José Germán @@oth@@ Belzunce-Segarra, María Jesús @@oth@@ Menchaca, Iratxe @@oth@@ Larreta, Joana @@oth@@ Sanz, Marta Rodrigo @@oth@@ Millán-Gabet, Vanessa @@oth@@ Gonzalez, Jean-Louis @@oth@@ Amouroux, Isabelle @@oth@@ Guesdon, Stephane @@oth@@ Menet-Nédélec, Florence @@oth@@ White, Blánaid @@oth@@ Regan, Fiona @@oth@@ Nolan, Martin @@oth@@ McHugh, Brendan @@oth@@ Bersuder, Philippe @@oth@@ Bolam, Thi @@oth@@ Robinson, Craig D. @@oth@@ Fones, Gary R. @@oth@@ Zhang, Hao @@oth@@ Schintu, Marco @@oth@@ Montero, Natalia @@oth@@ Marras, Barbara @@oth@@ |
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Metals concentrations in transitional and coastal waters by ICPMS and voltammetry analysis of spot samples and passive samplers (DGT) |
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This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. |
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This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. |
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This study investigates the relationships among Ni, Cd and Pb's different chemical forms determined by different methodologies in coastal and transitional waters across a broad geographical scale. Concentrations were measured in spot samples and through passive sampling (DGT). High variability of metal concentrations was found among sampling sites and methodologies due to natural water fluctuations rather than to a given metal or method. Total dissolved metal concentrations in spot samples were lower than the EQS-WFD values. The labile fractions of Cd and Pb, measured in spot samples by Anodic Stripping Voltammetry and by DGT-ICPMS, were highly correlated. Similar labilities were found for Cd, while for Pb, the ASV labile fraction was ≈50% lower. These results reflect the pool of mobile and labile species available towards each technique kinetic window, and they seem not to be affected by discrete sampling flaws. |
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Metals concentrations in transitional and coastal waters by ICPMS and voltammetry analysis of spot samples and passive samplers (DGT) |
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