Influence and action mechanism of pressure on pyrolysis process of a low rank Naomaohu coal at different temperatures
In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Zhu, Yao [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2022transfer abstract |
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| Schlagwörter: |
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| Übergeordnetes Werk: |
Enthalten in: Picralima nitida seeds suppress PGE2 production by interfering with multiple signalling pathways in IL-1β-stimulated SK-N-SH neuronal cells - Olajide, Olumayokun A. ELSEVIER, 2014, New York, NY [u.a.] |
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| Übergeordnetes Werk: |
volume:167 ; year:2022 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.jaap.2022.105682 |
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ELV058979697 |
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| 245 | 1 | 0 | |a Influence and action mechanism of pressure on pyrolysis process of a low rank Naomaohu coal at different temperatures |
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| 520 | |a In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. | ||
| 520 | |a In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. | ||
| 650 | 7 | |a Pressurized pyrolysis |2 Elsevier | |
| 650 | 7 | |a Promoting effect |2 Elsevier | |
| 650 | 7 | |a Action mechanism |2 Elsevier | |
| 650 | 7 | |a Char physicochemical properties |2 Elsevier | |
| 650 | 7 | |a Inhibiting effect |2 Elsevier | |
| 700 | 1 | |a Wang, Qinhui |4 oth | |
| 700 | 1 | |a Yan, Jiqing |4 oth | |
| 700 | 1 | |a Cen, Jianmeng |4 oth | |
| 700 | 1 | |a Fang, Mengxiang |4 oth | |
| 700 | 1 | |a Ye, Chao |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Science Direct |a Olajide, Olumayokun A. ELSEVIER |t Picralima nitida seeds suppress PGE2 production by interfering with multiple signalling pathways in IL-1β-stimulated SK-N-SH neuronal cells |d 2014 |g New York, NY [u.a.] |w (DE-627)ELV017524784 |
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10.1016/j.jaap.2022.105682 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001972.pica (DE-627)ELV058979697 (ELSEVIER)S0165-2370(22)00252-2 DE-627 ger DE-627 rakwb eng 610 VZ 390 VZ 300 610 VZ 44.06 bkl Zhu, Yao verfasserin aut Influence and action mechanism of pressure on pyrolysis process of a low rank Naomaohu coal at different temperatures 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. Pressurized pyrolysis Elsevier Promoting effect Elsevier Action mechanism Elsevier Char physicochemical properties Elsevier Inhibiting effect Elsevier Wang, Qinhui oth Yan, Jiqing oth Cen, Jianmeng oth Fang, Mengxiang oth Ye, Chao oth Enthalten in Science Direct Olajide, Olumayokun A. ELSEVIER Picralima nitida seeds suppress PGE2 production by interfering with multiple signalling pathways in IL-1β-stimulated SK-N-SH neuronal cells 2014 New York, NY [u.a.] (DE-627)ELV017524784 volume:167 year:2022 pages:0 https://doi.org/10.1016/j.jaap.2022.105682 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_70 44.06 Medizinsoziologie VZ AR 167 2022 0 |
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10.1016/j.jaap.2022.105682 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001972.pica (DE-627)ELV058979697 (ELSEVIER)S0165-2370(22)00252-2 DE-627 ger DE-627 rakwb eng 610 VZ 390 VZ 300 610 VZ 44.06 bkl Zhu, Yao verfasserin aut Influence and action mechanism of pressure on pyrolysis process of a low rank Naomaohu coal at different temperatures 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. Pressurized pyrolysis Elsevier Promoting effect Elsevier Action mechanism Elsevier Char physicochemical properties Elsevier Inhibiting effect Elsevier Wang, Qinhui oth Yan, Jiqing oth Cen, Jianmeng oth Fang, Mengxiang oth Ye, Chao oth Enthalten in Science Direct Olajide, Olumayokun A. ELSEVIER Picralima nitida seeds suppress PGE2 production by interfering with multiple signalling pathways in IL-1β-stimulated SK-N-SH neuronal cells 2014 New York, NY [u.a.] (DE-627)ELV017524784 volume:167 year:2022 pages:0 https://doi.org/10.1016/j.jaap.2022.105682 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_70 44.06 Medizinsoziologie VZ AR 167 2022 0 |
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10.1016/j.jaap.2022.105682 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001972.pica (DE-627)ELV058979697 (ELSEVIER)S0165-2370(22)00252-2 DE-627 ger DE-627 rakwb eng 610 VZ 390 VZ 300 610 VZ 44.06 bkl Zhu, Yao verfasserin aut Influence and action mechanism of pressure on pyrolysis process of a low rank Naomaohu coal at different temperatures 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. Pressurized pyrolysis Elsevier Promoting effect Elsevier Action mechanism Elsevier Char physicochemical properties Elsevier Inhibiting effect Elsevier Wang, Qinhui oth Yan, Jiqing oth Cen, Jianmeng oth Fang, Mengxiang oth Ye, Chao oth Enthalten in Science Direct Olajide, Olumayokun A. ELSEVIER Picralima nitida seeds suppress PGE2 production by interfering with multiple signalling pathways in IL-1β-stimulated SK-N-SH neuronal cells 2014 New York, NY [u.a.] (DE-627)ELV017524784 volume:167 year:2022 pages:0 https://doi.org/10.1016/j.jaap.2022.105682 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_70 44.06 Medizinsoziologie VZ AR 167 2022 0 |
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10.1016/j.jaap.2022.105682 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001972.pica (DE-627)ELV058979697 (ELSEVIER)S0165-2370(22)00252-2 DE-627 ger DE-627 rakwb eng 610 VZ 390 VZ 300 610 VZ 44.06 bkl Zhu, Yao verfasserin aut Influence and action mechanism of pressure on pyrolysis process of a low rank Naomaohu coal at different temperatures 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. Pressurized pyrolysis Elsevier Promoting effect Elsevier Action mechanism Elsevier Char physicochemical properties Elsevier Inhibiting effect Elsevier Wang, Qinhui oth Yan, Jiqing oth Cen, Jianmeng oth Fang, Mengxiang oth Ye, Chao oth Enthalten in Science Direct Olajide, Olumayokun A. ELSEVIER Picralima nitida seeds suppress PGE2 production by interfering with multiple signalling pathways in IL-1β-stimulated SK-N-SH neuronal cells 2014 New York, NY [u.a.] (DE-627)ELV017524784 volume:167 year:2022 pages:0 https://doi.org/10.1016/j.jaap.2022.105682 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_70 44.06 Medizinsoziologie VZ AR 167 2022 0 |
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10.1016/j.jaap.2022.105682 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001972.pica (DE-627)ELV058979697 (ELSEVIER)S0165-2370(22)00252-2 DE-627 ger DE-627 rakwb eng 610 VZ 390 VZ 300 610 VZ 44.06 bkl Zhu, Yao verfasserin aut Influence and action mechanism of pressure on pyrolysis process of a low rank Naomaohu coal at different temperatures 2022transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. Pressurized pyrolysis Elsevier Promoting effect Elsevier Action mechanism Elsevier Char physicochemical properties Elsevier Inhibiting effect Elsevier Wang, Qinhui oth Yan, Jiqing oth Cen, Jianmeng oth Fang, Mengxiang oth Ye, Chao oth Enthalten in Science Direct Olajide, Olumayokun A. ELSEVIER Picralima nitida seeds suppress PGE2 production by interfering with multiple signalling pathways in IL-1β-stimulated SK-N-SH neuronal cells 2014 New York, NY [u.a.] (DE-627)ELV017524784 volume:167 year:2022 pages:0 https://doi.org/10.1016/j.jaap.2022.105682 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_70 44.06 Medizinsoziologie VZ AR 167 2022 0 |
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Enthalten in Picralima nitida seeds suppress PGE2 production by interfering with multiple signalling pathways in IL-1β-stimulated SK-N-SH neuronal cells New York, NY [u.a.] volume:167 year:2022 pages:0 |
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Influence and action mechanism of pressure on pyrolysis process of a low rank Naomaohu coal at different temperatures |
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In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. |
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In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. |
| abstract_unstemmed |
In this study, the effect of pressure on the pyrolysis characteristics of Naomaohu coal and the physicochemical properties of char during slow pyrolysis is evaluated, and the mechanism of pressure is explored. The results show that the influences of pressure on char yield and physical properties are reflected in both promoting and inhibiting effect, and the latter is more obvious with the increasing temperature. As the pressure increases, the char yield first reduces and then improves, and at 600 °C and 800 °C the minimum yields are in 1.0 MPa and 0.1 MPa, which are 57.48% and 54.04%, respectively. The SBET of char increases first and then decreases. At 800 °C, the SBET of char increases from 7.86 m2/g at 0.1 MPa to 19.81 m2/g at 0.5 MPa and then decreases. The effect of pressure on the chemical properties of char is relatively simple. As the pressure rises, the content of functional groups in char reduces and the degree of graphitization enhances. The TG-DTG curve, XPS, BET, SEM test, experiments on the pressurized micro-fluidized bed reaction analyzer and pressurized pyrolysis-gas chromatography/mass spectrometry show that the pressure mainly affects the pyrolysis process by affecting the secondary reaction of the primary volatiles in the particle and is related to temperature. |
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