Soft magnetic composites based on Fe fibres and powders prepared by cold sintering process
The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characteri...
Ausführliche Beschreibung
Gespeichert in:
| Autor*in: |
Neamţu, B.V. [verfasserIn] |
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| Format: |
E-Artikel |
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| Sprache: |
Englisch |
| Erschienen: |
2023transfer abstract |
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| Übergeordnetes Werk: |
Enthalten in: Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners - Jacobs, Jacquelyn A. ELSEVIER, 2017, JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics, Lausanne |
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| Übergeordnetes Werk: |
volume:933 ; year:2023 ; day:5 ; month:02 ; pages:0 |
| Links: |
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| DOI / URN: |
10.1016/j.jallcom.2022.167799 |
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ELV059522402 |
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| 520 | |a The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. | ||
| 520 | |a The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. | ||
| 650 | 7 | |a Soft magnetic composites |2 Elsevier | |
| 650 | 7 | |a Cold sintering |2 Elsevier | |
| 650 | 7 | |a Powder-based composites |2 Elsevier | |
| 650 | 7 | |a Soft magnetic properties |2 Elsevier | |
| 650 | 7 | |a Fibres-based composites |2 Elsevier | |
| 700 | 1 | |a Popa, F. |4 oth | |
| 700 | 1 | |a Marinca, T.F. |4 oth | |
| 700 | 1 | |a Chicnaş, I. |4 oth | |
| 773 | 0 | 8 | |i Enthalten in |n Elsevier |a Jacobs, Jacquelyn A. ELSEVIER |t Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners |d 2017 |d JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics |g Lausanne |w (DE-627)ELV001115774 |
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10.1016/j.jallcom.2022.167799 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001974.pica (DE-627)ELV059522402 (ELSEVIER)S0925-8388(22)04190-1 DE-627 ger DE-627 rakwb eng 630 VZ Neamţu, B.V. verfasserin aut Soft magnetic composites based on Fe fibres and powders prepared by cold sintering process 2023transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. Soft magnetic composites Elsevier Cold sintering Elsevier Powder-based composites Elsevier Soft magnetic properties Elsevier Fibres-based composites Elsevier Popa, F. oth Marinca, T.F. oth Chicnaş, I. oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:933 year:2023 day:5 month:02 pages:0 https://doi.org/10.1016/j.jallcom.2022.167799 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 933 2023 5 0205 0 |
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10.1016/j.jallcom.2022.167799 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001974.pica (DE-627)ELV059522402 (ELSEVIER)S0925-8388(22)04190-1 DE-627 ger DE-627 rakwb eng 630 VZ Neamţu, B.V. verfasserin aut Soft magnetic composites based on Fe fibres and powders prepared by cold sintering process 2023transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. Soft magnetic composites Elsevier Cold sintering Elsevier Powder-based composites Elsevier Soft magnetic properties Elsevier Fibres-based composites Elsevier Popa, F. oth Marinca, T.F. oth Chicnaş, I. oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:933 year:2023 day:5 month:02 pages:0 https://doi.org/10.1016/j.jallcom.2022.167799 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 933 2023 5 0205 0 |
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10.1016/j.jallcom.2022.167799 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001974.pica (DE-627)ELV059522402 (ELSEVIER)S0925-8388(22)04190-1 DE-627 ger DE-627 rakwb eng 630 VZ Neamţu, B.V. verfasserin aut Soft magnetic composites based on Fe fibres and powders prepared by cold sintering process 2023transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. Soft magnetic composites Elsevier Cold sintering Elsevier Powder-based composites Elsevier Soft magnetic properties Elsevier Fibres-based composites Elsevier Popa, F. oth Marinca, T.F. oth Chicnaş, I. oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:933 year:2023 day:5 month:02 pages:0 https://doi.org/10.1016/j.jallcom.2022.167799 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 933 2023 5 0205 0 |
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10.1016/j.jallcom.2022.167799 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001974.pica (DE-627)ELV059522402 (ELSEVIER)S0925-8388(22)04190-1 DE-627 ger DE-627 rakwb eng 630 VZ Neamţu, B.V. verfasserin aut Soft magnetic composites based on Fe fibres and powders prepared by cold sintering process 2023transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. Soft magnetic composites Elsevier Cold sintering Elsevier Powder-based composites Elsevier Soft magnetic properties Elsevier Fibres-based composites Elsevier Popa, F. oth Marinca, T.F. oth Chicnaş, I. oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:933 year:2023 day:5 month:02 pages:0 https://doi.org/10.1016/j.jallcom.2022.167799 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 933 2023 5 0205 0 |
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10.1016/j.jallcom.2022.167799 doi /cbs_pica/cbs_olc/import_discovery/elsevier/einzuspielen/GBV00000000001974.pica (DE-627)ELV059522402 (ELSEVIER)S0925-8388(22)04190-1 DE-627 ger DE-627 rakwb eng 630 VZ Neamţu, B.V. verfasserin aut Soft magnetic composites based on Fe fibres and powders prepared by cold sintering process 2023transfer abstract nicht spezifiziert zzz rdacontent nicht spezifiziert z rdamedia nicht spezifiziert zu rdacarrier The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. Soft magnetic composites Elsevier Cold sintering Elsevier Powder-based composites Elsevier Soft magnetic properties Elsevier Fibres-based composites Elsevier Popa, F. oth Marinca, T.F. oth Chicnaş, I. oth Enthalten in Elsevier Jacobs, Jacquelyn A. ELSEVIER Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners 2017 JAL : an interdisciplinary journal of materials science and solid-state chemistry and physics Lausanne (DE-627)ELV001115774 volume:933 year:2023 day:5 month:02 pages:0 https://doi.org/10.1016/j.jallcom.2022.167799 Volltext GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA AR 933 2023 5 0205 0 |
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Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners |
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Factors associated with canine resource guarding behaviour in the presence of people: A cross-sectional survey of dog owners |
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Soft magnetic composites based on Fe fibres and powders prepared by cold sintering process |
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The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. |
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The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. |
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The manuscript provides a new strategy for preparation of soft magnetic composites that involves the consolidation of the ferromagnetic phase (fibres or powders), which is first covered with an insulating layer, via the cold sintering process. The manuscript reports on the preparation and characterisation of cold sintered compacts based on Fe fibres and Fe powders coated with ZnO and sintered at the temperature of 200 °C for 60 min under the pressure of 600 MPa. The amount of ZnO used as dielectric phase was 10 and 20 wt%. The absence of any reaction between phases that compose the compacts (Fe fibres or powders and ZnO) during the cold sintering process was proved by X-ray diffraction (XRD). Electron microscopy and X-ray micro-analysis (SEM-EDX) were used for morphology and chemical analysis of the cold sintered compacts. The influence of the type of ferromagnetic phase (fibres or particles), as well as the influence of the amount of dielectric phase on the saturation induction (Bs), the coercive field (Hc), and the maximum relative permeability (µrmax) of the cold sintered magnetic cores, was investigated and discussed. The effect of the same factors on the total core power losses (P) and the initial relative permeability (µri) of the cold sintered compacts, upon increasing the frequency of the magnetising field up to 10 kHz, was analysed. The feasibility of applying a heat treatment at the temperature of 450 °C for 1 h was investigated, leading to the enhancement of both DC and AC magnetic properties of the cold sintered compacts. |
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