Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS
Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue...
Ausführliche Beschreibung
Autor*in: |
Chang, Hailong [verfasserIn] Wang, Long [verfasserIn] Huang, Chenyu [verfasserIn] Zhou, Rendan [verfasserIn] Wu, Tianqi [verfasserIn] Li, Baotong [verfasserIn] |
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E-Artikel |
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Sprache: |
Englisch |
Erschienen: |
2023 |
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Schlagwörter: |
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Übergeordnetes Werk: |
Enthalten in: Journal of food composition and analysis - Orlando, Fla. : Academic Press, 1987, 123 |
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Übergeordnetes Werk: |
volume:123 |
DOI / URN: |
10.1016/j.jfca.2023.105552 |
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Katalog-ID: |
ELV063482401 |
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245 | 1 | 0 | |a Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS |
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520 | |a Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue analysis, and dietary risk assessment. The samples were extracted with acetonitrile, cleaned up using MWCNTs, and detected by HPLC-MS. The results showed that the concentrations and peak areas of benzovindiflupyr showed a good linear correlation (R2 >0.99) in a certain concentration range, and the LOD and LOQ values ranged from 0.001 to 0.002 mg/kg and 0.004–0.008 mg/kg, respectively. The average intra-day and inter-day recovery rates of benzovindiflupyr from four blank matrices spiked at 0.01, 0.04 and 0.1 mg/kg ranged from 82.4% to 101% with a RSDr of 0.790–9.36%, and 83.6–98.7% with a RSDR of 1.61–7.24%, respectively. The dissipation half-lives of benzovindiflupyr in field soil and peanut plants were 8.53–8.56 days and 14.9–17.3 days, respectively. The residual benzovindiflupyr in peanut kernels poses no health risk to Chinese consumers. These findings can help guide the application of benzovindiflupyr in the peanut field environment and minimize the environmental risks associated with its use. | ||
650 | 4 | |a Benzovindiflupyr | |
650 | 4 | |a QuEChERS-HPLC-MS | |
650 | 4 | |a Multi-walled carbon nanotubes | |
650 | 4 | |a Peanut | |
650 | 4 | |a Residue analysis | |
650 | 4 | |a Dissipation dynamics | |
650 | 4 | |a Dietary risk assessment | |
700 | 1 | |a Wang, Long |e verfasserin |4 aut | |
700 | 1 | |a Huang, Chenyu |e verfasserin |4 aut | |
700 | 1 | |a Zhou, Rendan |e verfasserin |4 aut | |
700 | 1 | |a Wu, Tianqi |e verfasserin |4 aut | |
700 | 1 | |a Li, Baotong |e verfasserin |4 aut | |
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allfields |
10.1016/j.jfca.2023.105552 doi (DE-627)ELV063482401 (ELSEVIER)S0889-1575(23)00426-X DE-627 ger DE-627 rda eng 630 640 540 660 VZ 58.34 bkl Chang, Hailong verfasserin aut Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue analysis, and dietary risk assessment. The samples were extracted with acetonitrile, cleaned up using MWCNTs, and detected by HPLC-MS. The results showed that the concentrations and peak areas of benzovindiflupyr showed a good linear correlation (R2 >0.99) in a certain concentration range, and the LOD and LOQ values ranged from 0.001 to 0.002 mg/kg and 0.004–0.008 mg/kg, respectively. The average intra-day and inter-day recovery rates of benzovindiflupyr from four blank matrices spiked at 0.01, 0.04 and 0.1 mg/kg ranged from 82.4% to 101% with a RSDr of 0.790–9.36%, and 83.6–98.7% with a RSDR of 1.61–7.24%, respectively. The dissipation half-lives of benzovindiflupyr in field soil and peanut plants were 8.53–8.56 days and 14.9–17.3 days, respectively. The residual benzovindiflupyr in peanut kernels poses no health risk to Chinese consumers. These findings can help guide the application of benzovindiflupyr in the peanut field environment and minimize the environmental risks associated with its use. Benzovindiflupyr QuEChERS-HPLC-MS Multi-walled carbon nanotubes Peanut Residue analysis Dissipation dynamics Dietary risk assessment Wang, Long verfasserin aut Huang, Chenyu verfasserin aut Zhou, Rendan verfasserin aut Wu, Tianqi verfasserin aut Li, Baotong verfasserin aut Enthalten in Journal of food composition and analysis Orlando, Fla. : Academic Press, 1987 123 Online-Ressource (DE-627)267328400 (DE-600)1469801-8 (DE-576)259483710 0889-1575 nnns volume:123 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.34 Lebensmitteltechnologie VZ AR 123 |
spelling |
10.1016/j.jfca.2023.105552 doi (DE-627)ELV063482401 (ELSEVIER)S0889-1575(23)00426-X DE-627 ger DE-627 rda eng 630 640 540 660 VZ 58.34 bkl Chang, Hailong verfasserin aut Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue analysis, and dietary risk assessment. The samples were extracted with acetonitrile, cleaned up using MWCNTs, and detected by HPLC-MS. The results showed that the concentrations and peak areas of benzovindiflupyr showed a good linear correlation (R2 >0.99) in a certain concentration range, and the LOD and LOQ values ranged from 0.001 to 0.002 mg/kg and 0.004–0.008 mg/kg, respectively. The average intra-day and inter-day recovery rates of benzovindiflupyr from four blank matrices spiked at 0.01, 0.04 and 0.1 mg/kg ranged from 82.4% to 101% with a RSDr of 0.790–9.36%, and 83.6–98.7% with a RSDR of 1.61–7.24%, respectively. The dissipation half-lives of benzovindiflupyr in field soil and peanut plants were 8.53–8.56 days and 14.9–17.3 days, respectively. The residual benzovindiflupyr in peanut kernels poses no health risk to Chinese consumers. These findings can help guide the application of benzovindiflupyr in the peanut field environment and minimize the environmental risks associated with its use. Benzovindiflupyr QuEChERS-HPLC-MS Multi-walled carbon nanotubes Peanut Residue analysis Dissipation dynamics Dietary risk assessment Wang, Long verfasserin aut Huang, Chenyu verfasserin aut Zhou, Rendan verfasserin aut Wu, Tianqi verfasserin aut Li, Baotong verfasserin aut Enthalten in Journal of food composition and analysis Orlando, Fla. : Academic Press, 1987 123 Online-Ressource (DE-627)267328400 (DE-600)1469801-8 (DE-576)259483710 0889-1575 nnns volume:123 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.34 Lebensmitteltechnologie VZ AR 123 |
allfields_unstemmed |
10.1016/j.jfca.2023.105552 doi (DE-627)ELV063482401 (ELSEVIER)S0889-1575(23)00426-X DE-627 ger DE-627 rda eng 630 640 540 660 VZ 58.34 bkl Chang, Hailong verfasserin aut Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue analysis, and dietary risk assessment. The samples were extracted with acetonitrile, cleaned up using MWCNTs, and detected by HPLC-MS. The results showed that the concentrations and peak areas of benzovindiflupyr showed a good linear correlation (R2 >0.99) in a certain concentration range, and the LOD and LOQ values ranged from 0.001 to 0.002 mg/kg and 0.004–0.008 mg/kg, respectively. The average intra-day and inter-day recovery rates of benzovindiflupyr from four blank matrices spiked at 0.01, 0.04 and 0.1 mg/kg ranged from 82.4% to 101% with a RSDr of 0.790–9.36%, and 83.6–98.7% with a RSDR of 1.61–7.24%, respectively. The dissipation half-lives of benzovindiflupyr in field soil and peanut plants were 8.53–8.56 days and 14.9–17.3 days, respectively. The residual benzovindiflupyr in peanut kernels poses no health risk to Chinese consumers. These findings can help guide the application of benzovindiflupyr in the peanut field environment and minimize the environmental risks associated with its use. Benzovindiflupyr QuEChERS-HPLC-MS Multi-walled carbon nanotubes Peanut Residue analysis Dissipation dynamics Dietary risk assessment Wang, Long verfasserin aut Huang, Chenyu verfasserin aut Zhou, Rendan verfasserin aut Wu, Tianqi verfasserin aut Li, Baotong verfasserin aut Enthalten in Journal of food composition and analysis Orlando, Fla. : Academic Press, 1987 123 Online-Ressource (DE-627)267328400 (DE-600)1469801-8 (DE-576)259483710 0889-1575 nnns volume:123 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.34 Lebensmitteltechnologie VZ AR 123 |
allfieldsGer |
10.1016/j.jfca.2023.105552 doi (DE-627)ELV063482401 (ELSEVIER)S0889-1575(23)00426-X DE-627 ger DE-627 rda eng 630 640 540 660 VZ 58.34 bkl Chang, Hailong verfasserin aut Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue analysis, and dietary risk assessment. The samples were extracted with acetonitrile, cleaned up using MWCNTs, and detected by HPLC-MS. The results showed that the concentrations and peak areas of benzovindiflupyr showed a good linear correlation (R2 >0.99) in a certain concentration range, and the LOD and LOQ values ranged from 0.001 to 0.002 mg/kg and 0.004–0.008 mg/kg, respectively. The average intra-day and inter-day recovery rates of benzovindiflupyr from four blank matrices spiked at 0.01, 0.04 and 0.1 mg/kg ranged from 82.4% to 101% with a RSDr of 0.790–9.36%, and 83.6–98.7% with a RSDR of 1.61–7.24%, respectively. The dissipation half-lives of benzovindiflupyr in field soil and peanut plants were 8.53–8.56 days and 14.9–17.3 days, respectively. The residual benzovindiflupyr in peanut kernels poses no health risk to Chinese consumers. These findings can help guide the application of benzovindiflupyr in the peanut field environment and minimize the environmental risks associated with its use. Benzovindiflupyr QuEChERS-HPLC-MS Multi-walled carbon nanotubes Peanut Residue analysis Dissipation dynamics Dietary risk assessment Wang, Long verfasserin aut Huang, Chenyu verfasserin aut Zhou, Rendan verfasserin aut Wu, Tianqi verfasserin aut Li, Baotong verfasserin aut Enthalten in Journal of food composition and analysis Orlando, Fla. : Academic Press, 1987 123 Online-Ressource (DE-627)267328400 (DE-600)1469801-8 (DE-576)259483710 0889-1575 nnns volume:123 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.34 Lebensmitteltechnologie VZ AR 123 |
allfieldsSound |
10.1016/j.jfca.2023.105552 doi (DE-627)ELV063482401 (ELSEVIER)S0889-1575(23)00426-X DE-627 ger DE-627 rda eng 630 640 540 660 VZ 58.34 bkl Chang, Hailong verfasserin aut Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue analysis, and dietary risk assessment. The samples were extracted with acetonitrile, cleaned up using MWCNTs, and detected by HPLC-MS. The results showed that the concentrations and peak areas of benzovindiflupyr showed a good linear correlation (R2 >0.99) in a certain concentration range, and the LOD and LOQ values ranged from 0.001 to 0.002 mg/kg and 0.004–0.008 mg/kg, respectively. The average intra-day and inter-day recovery rates of benzovindiflupyr from four blank matrices spiked at 0.01, 0.04 and 0.1 mg/kg ranged from 82.4% to 101% with a RSDr of 0.790–9.36%, and 83.6–98.7% with a RSDR of 1.61–7.24%, respectively. The dissipation half-lives of benzovindiflupyr in field soil and peanut plants were 8.53–8.56 days and 14.9–17.3 days, respectively. The residual benzovindiflupyr in peanut kernels poses no health risk to Chinese consumers. These findings can help guide the application of benzovindiflupyr in the peanut field environment and minimize the environmental risks associated with its use. Benzovindiflupyr QuEChERS-HPLC-MS Multi-walled carbon nanotubes Peanut Residue analysis Dissipation dynamics Dietary risk assessment Wang, Long verfasserin aut Huang, Chenyu verfasserin aut Zhou, Rendan verfasserin aut Wu, Tianqi verfasserin aut Li, Baotong verfasserin aut Enthalten in Journal of food composition and analysis Orlando, Fla. : Academic Press, 1987 123 Online-Ressource (DE-627)267328400 (DE-600)1469801-8 (DE-576)259483710 0889-1575 nnns volume:123 GBV_USEFLAG_U GBV_ELV SYSFLAG_U SSG-OLC-PHA GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 58.34 Lebensmitteltechnologie VZ AR 123 |
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Chang, Hailong @@aut@@ Wang, Long @@aut@@ Huang, Chenyu @@aut@@ Zhou, Rendan @@aut@@ Wu, Tianqi @@aut@@ Li, Baotong @@aut@@ |
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Chang, Hailong |
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Chang, Hailong ddc 630 bkl 58.34 misc Benzovindiflupyr misc QuEChERS-HPLC-MS misc Multi-walled carbon nanotubes misc Peanut misc Residue analysis misc Dissipation dynamics misc Dietary risk assessment Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS |
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630 640 540 660 VZ 58.34 bkl Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS Benzovindiflupyr QuEChERS-HPLC-MS Multi-walled carbon nanotubes Peanut Residue analysis Dissipation dynamics Dietary risk assessment |
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residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by lc-ms |
title_auth |
Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS |
abstract |
Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue analysis, and dietary risk assessment. The samples were extracted with acetonitrile, cleaned up using MWCNTs, and detected by HPLC-MS. The results showed that the concentrations and peak areas of benzovindiflupyr showed a good linear correlation (R2 >0.99) in a certain concentration range, and the LOD and LOQ values ranged from 0.001 to 0.002 mg/kg and 0.004–0.008 mg/kg, respectively. The average intra-day and inter-day recovery rates of benzovindiflupyr from four blank matrices spiked at 0.01, 0.04 and 0.1 mg/kg ranged from 82.4% to 101% with a RSDr of 0.790–9.36%, and 83.6–98.7% with a RSDR of 1.61–7.24%, respectively. The dissipation half-lives of benzovindiflupyr in field soil and peanut plants were 8.53–8.56 days and 14.9–17.3 days, respectively. The residual benzovindiflupyr in peanut kernels poses no health risk to Chinese consumers. These findings can help guide the application of benzovindiflupyr in the peanut field environment and minimize the environmental risks associated with its use. |
abstractGer |
Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue analysis, and dietary risk assessment. The samples were extracted with acetonitrile, cleaned up using MWCNTs, and detected by HPLC-MS. The results showed that the concentrations and peak areas of benzovindiflupyr showed a good linear correlation (R2 >0.99) in a certain concentration range, and the LOD and LOQ values ranged from 0.001 to 0.002 mg/kg and 0.004–0.008 mg/kg, respectively. The average intra-day and inter-day recovery rates of benzovindiflupyr from four blank matrices spiked at 0.01, 0.04 and 0.1 mg/kg ranged from 82.4% to 101% with a RSDr of 0.790–9.36%, and 83.6–98.7% with a RSDR of 1.61–7.24%, respectively. The dissipation half-lives of benzovindiflupyr in field soil and peanut plants were 8.53–8.56 days and 14.9–17.3 days, respectively. The residual benzovindiflupyr in peanut kernels poses no health risk to Chinese consumers. These findings can help guide the application of benzovindiflupyr in the peanut field environment and minimize the environmental risks associated with its use. |
abstract_unstemmed |
Benzovindiflupyr is a succinate dehydrogenase inhibitor fungicide, and its residues in the environment could pose a threat to ecological safety. The aim of this study was to develop a method for determining benzovindiflupyr residues in peanut fields and to perform residue dissipation, final residue analysis, and dietary risk assessment. The samples were extracted with acetonitrile, cleaned up using MWCNTs, and detected by HPLC-MS. The results showed that the concentrations and peak areas of benzovindiflupyr showed a good linear correlation (R2 >0.99) in a certain concentration range, and the LOD and LOQ values ranged from 0.001 to 0.002 mg/kg and 0.004–0.008 mg/kg, respectively. The average intra-day and inter-day recovery rates of benzovindiflupyr from four blank matrices spiked at 0.01, 0.04 and 0.1 mg/kg ranged from 82.4% to 101% with a RSDr of 0.790–9.36%, and 83.6–98.7% with a RSDR of 1.61–7.24%, respectively. The dissipation half-lives of benzovindiflupyr in field soil and peanut plants were 8.53–8.56 days and 14.9–17.3 days, respectively. The residual benzovindiflupyr in peanut kernels poses no health risk to Chinese consumers. These findings can help guide the application of benzovindiflupyr in the peanut field environment and minimize the environmental risks associated with its use. |
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Residue analysis, dissipation dynamics, and dietary risk assessment of benzovindiflupyr in peanut field environment by LC-MS |
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score |
7.3992443 |