Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS

p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical s...
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Autor*in:	Megalamani, Manjunath B. [verfasserIn] Patil, Yuvarajgouda N. [verfasserIn] Nandibewoor, Sharanappa T. [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2023

Schlagwörter:	Drug analysis Nanosheets Voltammetry Urine and water sample analysis

Übergeordnetes Werk:	Enthalten in: Inorganic chemistry communications - Amsterdam [u.a.] : Elsevier Science, 1998, 151
Übergeordnetes Werk:	volume:151

DOI / URN:	10.1016/j.inoche.2023.110617

Katalog-ID:	ELV065128990

Internformat


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520			\|a p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical sensor for p-DAAP trace level monitoring. Synthesized PVA-capped Mn-doped ZnS encapsulated by synthesised MoS2 nanosheets drop-casted on a glassy carbon electrode (Mn:ZnS:MoS2GCE) was used as an electrode for the p-DAAP investigation. XRD, SEM-EDX, and FTIR were used to characterize the surface. The material's performance was investigated using electrochemical impedance spectroscopy (EIS). To evaluate p-DAAP, cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used. Under various phosphate buffer solutions, the p-DAAP displays an oxidation peak and a reduction peak between 0 and 0.8 V capabilities, with pH 6.0 giving the best result. The effect of numerous parameters on electrochemical characteristics was studied, indicating diffusion as a regulator of the electrode process. The DPV is used to calculate the quantitative value of p-DAAP. The linearity field was determined to range from 0.2 µM to 16 µM. The LOD and LOQ were 1.08 × 10−8 M and 3.60 × 10−8 M, respectively, and outperformed previous techniques. Furthermore, the innovative approach was used to assess p-DAAP concentrations in biological and water samples.
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allfields	10.1016/j.inoche.2023.110617 doi (DE-627)ELV065128990 (ELSEVIER)S1387-7003(23)00229-0 DE-627 ger DE-627 rda eng 540 VZ 35.40 bkl Megalamani, Manjunath B. verfasserin aut Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical sensor for p-DAAP trace level monitoring. Synthesized PVA-capped Mn-doped ZnS encapsulated by synthesised MoS2 nanosheets drop-casted on a glassy carbon electrode (Mn:ZnS:MoS2GCE) was used as an electrode for the p-DAAP investigation. XRD, SEM-EDX, and FTIR were used to characterize the surface. The material's performance was investigated using electrochemical impedance spectroscopy (EIS). To evaluate p-DAAP, cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used. Under various phosphate buffer solutions, the p-DAAP displays an oxidation peak and a reduction peak between 0 and 0.8 V capabilities, with pH 6.0 giving the best result. The effect of numerous parameters on electrochemical characteristics was studied, indicating diffusion as a regulator of the electrode process. The DPV is used to calculate the quantitative value of p-DAAP. The linearity field was determined to range from 0.2 µM to 16 µM. The LOD and LOQ were 1.08 × 10−8 M and 3.60 × 10−8 M, respectively, and outperformed previous techniques. Furthermore, the innovative approach was used to assess p-DAAP concentrations in biological and water samples. Drug analysis Nanosheets Voltammetry Urine and water sample analysis Patil, Yuvarajgouda N. verfasserin aut Nandibewoor, Sharanappa T. verfasserin aut Enthalten in Inorganic chemistry communications Amsterdam [u.a.] : Elsevier Science, 1998 151 Online-Ressource (DE-627)324455658 (DE-600)2026959-6 (DE-576)094531595 nnns volume:151 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.40 Anorganische Chemie: Allgemeines VZ AR 151
spelling	10.1016/j.inoche.2023.110617 doi (DE-627)ELV065128990 (ELSEVIER)S1387-7003(23)00229-0 DE-627 ger DE-627 rda eng 540 VZ 35.40 bkl Megalamani, Manjunath B. verfasserin aut Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical sensor for p-DAAP trace level monitoring. Synthesized PVA-capped Mn-doped ZnS encapsulated by synthesised MoS2 nanosheets drop-casted on a glassy carbon electrode (Mn:ZnS:MoS2GCE) was used as an electrode for the p-DAAP investigation. XRD, SEM-EDX, and FTIR were used to characterize the surface. The material's performance was investigated using electrochemical impedance spectroscopy (EIS). To evaluate p-DAAP, cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used. Under various phosphate buffer solutions, the p-DAAP displays an oxidation peak and a reduction peak between 0 and 0.8 V capabilities, with pH 6.0 giving the best result. The effect of numerous parameters on electrochemical characteristics was studied, indicating diffusion as a regulator of the electrode process. The DPV is used to calculate the quantitative value of p-DAAP. The linearity field was determined to range from 0.2 µM to 16 µM. The LOD and LOQ were 1.08 × 10−8 M and 3.60 × 10−8 M, respectively, and outperformed previous techniques. Furthermore, the innovative approach was used to assess p-DAAP concentrations in biological and water samples. Drug analysis Nanosheets Voltammetry Urine and water sample analysis Patil, Yuvarajgouda N. verfasserin aut Nandibewoor, Sharanappa T. verfasserin aut Enthalten in Inorganic chemistry communications Amsterdam [u.a.] : Elsevier Science, 1998 151 Online-Ressource (DE-627)324455658 (DE-600)2026959-6 (DE-576)094531595 nnns volume:151 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.40 Anorganische Chemie: Allgemeines VZ AR 151
allfields_unstemmed	10.1016/j.inoche.2023.110617 doi (DE-627)ELV065128990 (ELSEVIER)S1387-7003(23)00229-0 DE-627 ger DE-627 rda eng 540 VZ 35.40 bkl Megalamani, Manjunath B. verfasserin aut Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical sensor for p-DAAP trace level monitoring. Synthesized PVA-capped Mn-doped ZnS encapsulated by synthesised MoS2 nanosheets drop-casted on a glassy carbon electrode (Mn:ZnS:MoS2GCE) was used as an electrode for the p-DAAP investigation. XRD, SEM-EDX, and FTIR were used to characterize the surface. The material's performance was investigated using electrochemical impedance spectroscopy (EIS). To evaluate p-DAAP, cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used. Under various phosphate buffer solutions, the p-DAAP displays an oxidation peak and a reduction peak between 0 and 0.8 V capabilities, with pH 6.0 giving the best result. The effect of numerous parameters on electrochemical characteristics was studied, indicating diffusion as a regulator of the electrode process. The DPV is used to calculate the quantitative value of p-DAAP. The linearity field was determined to range from 0.2 µM to 16 µM. The LOD and LOQ were 1.08 × 10−8 M and 3.60 × 10−8 M, respectively, and outperformed previous techniques. Furthermore, the innovative approach was used to assess p-DAAP concentrations in biological and water samples. Drug analysis Nanosheets Voltammetry Urine and water sample analysis Patil, Yuvarajgouda N. verfasserin aut Nandibewoor, Sharanappa T. verfasserin aut Enthalten in Inorganic chemistry communications Amsterdam [u.a.] : Elsevier Science, 1998 151 Online-Ressource (DE-627)324455658 (DE-600)2026959-6 (DE-576)094531595 nnns volume:151 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.40 Anorganische Chemie: Allgemeines VZ AR 151
allfieldsGer	10.1016/j.inoche.2023.110617 doi (DE-627)ELV065128990 (ELSEVIER)S1387-7003(23)00229-0 DE-627 ger DE-627 rda eng 540 VZ 35.40 bkl Megalamani, Manjunath B. verfasserin aut Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical sensor for p-DAAP trace level monitoring. Synthesized PVA-capped Mn-doped ZnS encapsulated by synthesised MoS2 nanosheets drop-casted on a glassy carbon electrode (Mn:ZnS:MoS2GCE) was used as an electrode for the p-DAAP investigation. XRD, SEM-EDX, and FTIR were used to characterize the surface. The material's performance was investigated using electrochemical impedance spectroscopy (EIS). To evaluate p-DAAP, cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used. Under various phosphate buffer solutions, the p-DAAP displays an oxidation peak and a reduction peak between 0 and 0.8 V capabilities, with pH 6.0 giving the best result. The effect of numerous parameters on electrochemical characteristics was studied, indicating diffusion as a regulator of the electrode process. The DPV is used to calculate the quantitative value of p-DAAP. The linearity field was determined to range from 0.2 µM to 16 µM. The LOD and LOQ were 1.08 × 10−8 M and 3.60 × 10−8 M, respectively, and outperformed previous techniques. Furthermore, the innovative approach was used to assess p-DAAP concentrations in biological and water samples. Drug analysis Nanosheets Voltammetry Urine and water sample analysis Patil, Yuvarajgouda N. verfasserin aut Nandibewoor, Sharanappa T. verfasserin aut Enthalten in Inorganic chemistry communications Amsterdam [u.a.] : Elsevier Science, 1998 151 Online-Ressource (DE-627)324455658 (DE-600)2026959-6 (DE-576)094531595 nnns volume:151 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.40 Anorganische Chemie: Allgemeines VZ AR 151
allfieldsSound	10.1016/j.inoche.2023.110617 doi (DE-627)ELV065128990 (ELSEVIER)S1387-7003(23)00229-0 DE-627 ger DE-627 rda eng 540 VZ 35.40 bkl Megalamani, Manjunath B. verfasserin aut Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical sensor for p-DAAP trace level monitoring. Synthesized PVA-capped Mn-doped ZnS encapsulated by synthesised MoS2 nanosheets drop-casted on a glassy carbon electrode (Mn:ZnS:MoS2GCE) was used as an electrode for the p-DAAP investigation. XRD, SEM-EDX, and FTIR were used to characterize the surface. The material's performance was investigated using electrochemical impedance spectroscopy (EIS). To evaluate p-DAAP, cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used. Under various phosphate buffer solutions, the p-DAAP displays an oxidation peak and a reduction peak between 0 and 0.8 V capabilities, with pH 6.0 giving the best result. The effect of numerous parameters on electrochemical characteristics was studied, indicating diffusion as a regulator of the electrode process. The DPV is used to calculate the quantitative value of p-DAAP. The linearity field was determined to range from 0.2 µM to 16 µM. The LOD and LOQ were 1.08 × 10−8 M and 3.60 × 10−8 M, respectively, and outperformed previous techniques. Furthermore, the innovative approach was used to assess p-DAAP concentrations in biological and water samples. Drug analysis Nanosheets Voltammetry Urine and water sample analysis Patil, Yuvarajgouda N. verfasserin aut Nandibewoor, Sharanappa T. verfasserin aut Enthalten in Inorganic chemistry communications Amsterdam [u.a.] : Elsevier Science, 1998 151 Online-Ressource (DE-627)324455658 (DE-600)2026959-6 (DE-576)094531595 nnns volume:151 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_101 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 35.40 Anorganische Chemie: Allgemeines VZ AR 151
language	English
source	Enthalten in Inorganic chemistry communications 151 volume:151
sourceStr	Enthalten in Inorganic chemistry communications 151 volume:151
format_phy_str_mv	Article
bklname	Anorganische Chemie: Allgemeines
institution	findex.gbv.de
topic_facet	Drug analysis Nanosheets Voltammetry Urine and water sample analysis
dewey-raw	540
isfreeaccess_bool	false
container_title	Inorganic chemistry communications
authorswithroles_txt_mv	Megalamani, Manjunath B. @@aut@@ Patil, Yuvarajgouda N. @@aut@@ Nandibewoor, Sharanappa T. @@aut@@
publishDateDaySort_date	2023-01-01T00:00:00Z
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language_de	englisch
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author	Megalamani, Manjunath B.
spellingShingle	Megalamani, Manjunath B. ddc 540 bkl 35.40 misc Drug analysis misc Nanosheets misc Voltammetry misc Urine and water sample analysis Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS
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topic_title	540 VZ 35.40 bkl Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS Drug analysis Nanosheets Voltammetry Urine and water sample analysis
topic	ddc 540 bkl 35.40 misc Drug analysis misc Nanosheets misc Voltammetry misc Urine and water sample analysis
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title	Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS
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title_full	Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS
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author_browse	Megalamani, Manjunath B. Patil, Yuvarajgouda N. Nandibewoor, Sharanappa T.
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title_sort	electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly mos
title_auth	Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS
abstract	p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical sensor for p-DAAP trace level monitoring. Synthesized PVA-capped Mn-doped ZnS encapsulated by synthesised MoS2 nanosheets drop-casted on a glassy carbon electrode (Mn:ZnS:MoS2GCE) was used as an electrode for the p-DAAP investigation. XRD, SEM-EDX, and FTIR were used to characterize the surface. The material's performance was investigated using electrochemical impedance spectroscopy (EIS). To evaluate p-DAAP, cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used. Under various phosphate buffer solutions, the p-DAAP displays an oxidation peak and a reduction peak between 0 and 0.8 V capabilities, with pH 6.0 giving the best result. The effect of numerous parameters on electrochemical characteristics was studied, indicating diffusion as a regulator of the electrode process. The DPV is used to calculate the quantitative value of p-DAAP. The linearity field was determined to range from 0.2 µM to 16 µM. The LOD and LOQ were 1.08 × 10−8 M and 3.60 × 10−8 M, respectively, and outperformed previous techniques. Furthermore, the innovative approach was used to assess p-DAAP concentrations in biological and water samples.
abstractGer	p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical sensor for p-DAAP trace level monitoring. Synthesized PVA-capped Mn-doped ZnS encapsulated by synthesised MoS2 nanosheets drop-casted on a glassy carbon electrode (Mn:ZnS:MoS2GCE) was used as an electrode for the p-DAAP investigation. XRD, SEM-EDX, and FTIR were used to characterize the surface. The material's performance was investigated using electrochemical impedance spectroscopy (EIS). To evaluate p-DAAP, cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used. Under various phosphate buffer solutions, the p-DAAP displays an oxidation peak and a reduction peak between 0 and 0.8 V capabilities, with pH 6.0 giving the best result. The effect of numerous parameters on electrochemical characteristics was studied, indicating diffusion as a regulator of the electrode process. The DPV is used to calculate the quantitative value of p-DAAP. The linearity field was determined to range from 0.2 µM to 16 µM. The LOD and LOQ were 1.08 × 10−8 M and 3.60 × 10−8 M, respectively, and outperformed previous techniques. Furthermore, the innovative approach was used to assess p-DAAP concentrations in biological and water samples.
abstract_unstemmed	p-Dimethylamino Antipyrine (p-DAAP) is a carcinogen that causes agranulocytosis and is found as an additive in cocaine samples. It is necessary to use a sensitive analytical approach capable of identifying trace quantities. In this work, we used a voltammetric technique to build an electrochemical sensor for p-DAAP trace level monitoring. Synthesized PVA-capped Mn-doped ZnS encapsulated by synthesised MoS2 nanosheets drop-casted on a glassy carbon electrode (Mn:ZnS:MoS2GCE) was used as an electrode for the p-DAAP investigation. XRD, SEM-EDX, and FTIR were used to characterize the surface. The material's performance was investigated using electrochemical impedance spectroscopy (EIS). To evaluate p-DAAP, cyclic voltammetry (CV) and differential pulse voltammetry (DPV) were used. Under various phosphate buffer solutions, the p-DAAP displays an oxidation peak and a reduction peak between 0 and 0.8 V capabilities, with pH 6.0 giving the best result. The effect of numerous parameters on electrochemical characteristics was studied, indicating diffusion as a regulator of the electrode process. The DPV is used to calculate the quantitative value of p-DAAP. The linearity field was determined to range from 0.2 µM to 16 µM. The LOD and LOQ were 1.08 × 10−8 M and 3.60 × 10−8 M, respectively, and outperformed previous techniques. Furthermore, the innovative approach was used to assess p-DAAP concentrations in biological and water samples.
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title_short	Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS
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up_date	2024-07-06T21:56:06.536Z
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Electrochemical sensing of carcinogenic p-dimethylamino antipyrine using sensor comprised of eco-friendly MoS

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