Unveiling the transformation pathways of hierarchical γ

Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process. Ausführliche Beschreibung

Gespeichert in:

Autor*in:	Singh, Digvijay [verfasserIn] Tasaki, Wataru [verfasserIn] Yoshinaka, Fumiyoshi [verfasserIn] Takamori, Susumu [verfasserIn] Emura, Satoshi [verfasserIn] Tsuchiya, Koichi [verfasserIn] Sawaguchi, Takahiro [verfasserIn]

Format:	E-Artikel
Sprache:	Englisch

Erschienen:	2023

Schlagwörter:	Martensitic phase transformations Deformation twinning Crystallographic orientation Electron backscattered diffraction (EBSD) Single crystal

Übergeordnetes Werk:	Enthalten in: Materials characterization - New York, NY : Science Direct, 1990, 205
Übergeordnetes Werk:	volume:205

DOI / URN:	10.1016/j.matchar.2023.113358

Katalog-ID:	ELV065325761

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520			\|a Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process.
650		4	\|a Martensitic phase transformations
650		4	\|a Deformation twinning
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650		4	\|a Electron backscattered diffraction (EBSD)
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700	1		\|a Tsuchiya, Koichi \|e verfasserin \|4 aut
700	1		\|a Sawaguchi, Takahiro \|e verfasserin \|4 aut
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matchkey_str	singhdigvijaytasakiwataruyoshinakafumiyo:2023----:nelnternfrainahasf
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allfields	10.1016/j.matchar.2023.113358 doi (DE-627)ELV065325761 (ELSEVIER)S1044-5803(23)00717-9 DE-627 ger DE-627 rda eng 670 VZ 51.30 bkl Singh, Digvijay verfasserin aut Unveiling the transformation pathways of hierarchical γ 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process. Martensitic phase transformations Deformation twinning Crystallographic orientation Electron backscattered diffraction (EBSD) Single crystal Tasaki, Wataru verfasserin aut Yoshinaka, Fumiyoshi verfasserin aut Takamori, Susumu verfasserin aut Emura, Satoshi verfasserin aut Tsuchiya, Koichi verfasserin aut Sawaguchi, Takahiro verfasserin aut Enthalten in Materials characterization New York, NY : Science Direct, 1990 205 Online-Ressource (DE-627)302719288 (DE-600)1491951-5 (DE-576)259483966 nnns volume:205 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 205
spelling	10.1016/j.matchar.2023.113358 doi (DE-627)ELV065325761 (ELSEVIER)S1044-5803(23)00717-9 DE-627 ger DE-627 rda eng 670 VZ 51.30 bkl Singh, Digvijay verfasserin aut Unveiling the transformation pathways of hierarchical γ 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process. Martensitic phase transformations Deformation twinning Crystallographic orientation Electron backscattered diffraction (EBSD) Single crystal Tasaki, Wataru verfasserin aut Yoshinaka, Fumiyoshi verfasserin aut Takamori, Susumu verfasserin aut Emura, Satoshi verfasserin aut Tsuchiya, Koichi verfasserin aut Sawaguchi, Takahiro verfasserin aut Enthalten in Materials characterization New York, NY : Science Direct, 1990 205 Online-Ressource (DE-627)302719288 (DE-600)1491951-5 (DE-576)259483966 nnns volume:205 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 205
allfields_unstemmed	10.1016/j.matchar.2023.113358 doi (DE-627)ELV065325761 (ELSEVIER)S1044-5803(23)00717-9 DE-627 ger DE-627 rda eng 670 VZ 51.30 bkl Singh, Digvijay verfasserin aut Unveiling the transformation pathways of hierarchical γ 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process. Martensitic phase transformations Deformation twinning Crystallographic orientation Electron backscattered diffraction (EBSD) Single crystal Tasaki, Wataru verfasserin aut Yoshinaka, Fumiyoshi verfasserin aut Takamori, Susumu verfasserin aut Emura, Satoshi verfasserin aut Tsuchiya, Koichi verfasserin aut Sawaguchi, Takahiro verfasserin aut Enthalten in Materials characterization New York, NY : Science Direct, 1990 205 Online-Ressource (DE-627)302719288 (DE-600)1491951-5 (DE-576)259483966 nnns volume:205 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 205
allfieldsGer	10.1016/j.matchar.2023.113358 doi (DE-627)ELV065325761 (ELSEVIER)S1044-5803(23)00717-9 DE-627 ger DE-627 rda eng 670 VZ 51.30 bkl Singh, Digvijay verfasserin aut Unveiling the transformation pathways of hierarchical γ 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process. Martensitic phase transformations Deformation twinning Crystallographic orientation Electron backscattered diffraction (EBSD) Single crystal Tasaki, Wataru verfasserin aut Yoshinaka, Fumiyoshi verfasserin aut Takamori, Susumu verfasserin aut Emura, Satoshi verfasserin aut Tsuchiya, Koichi verfasserin aut Sawaguchi, Takahiro verfasserin aut Enthalten in Materials characterization New York, NY : Science Direct, 1990 205 Online-Ressource (DE-627)302719288 (DE-600)1491951-5 (DE-576)259483966 nnns volume:205 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 205
allfieldsSound	10.1016/j.matchar.2023.113358 doi (DE-627)ELV065325761 (ELSEVIER)S1044-5803(23)00717-9 DE-627 ger DE-627 rda eng 670 VZ 51.30 bkl Singh, Digvijay verfasserin aut Unveiling the transformation pathways of hierarchical γ 2023 nicht spezifiziert zzz rdacontent Computermedien c rdamedia Online-Ressource cr rdacarrier Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process. Martensitic phase transformations Deformation twinning Crystallographic orientation Electron backscattered diffraction (EBSD) Single crystal Tasaki, Wataru verfasserin aut Yoshinaka, Fumiyoshi verfasserin aut Takamori, Susumu verfasserin aut Emura, Satoshi verfasserin aut Tsuchiya, Koichi verfasserin aut Sawaguchi, Takahiro verfasserin aut Enthalten in Materials characterization New York, NY : Science Direct, 1990 205 Online-Ressource (DE-627)302719288 (DE-600)1491951-5 (DE-576)259483966 nnns volume:205 GBV_USEFLAG_U GBV_ELV SYSFLAG_U GBV_ILN_20 GBV_ILN_22 GBV_ILN_23 GBV_ILN_24 GBV_ILN_31 GBV_ILN_32 GBV_ILN_40 GBV_ILN_60 GBV_ILN_62 GBV_ILN_65 GBV_ILN_69 GBV_ILN_70 GBV_ILN_73 GBV_ILN_74 GBV_ILN_90 GBV_ILN_95 GBV_ILN_100 GBV_ILN_105 GBV_ILN_110 GBV_ILN_150 GBV_ILN_151 GBV_ILN_187 GBV_ILN_213 GBV_ILN_224 GBV_ILN_230 GBV_ILN_370 GBV_ILN_602 GBV_ILN_702 GBV_ILN_2001 GBV_ILN_2003 GBV_ILN_2004 GBV_ILN_2005 GBV_ILN_2007 GBV_ILN_2008 GBV_ILN_2009 GBV_ILN_2010 GBV_ILN_2011 GBV_ILN_2014 GBV_ILN_2015 GBV_ILN_2020 GBV_ILN_2021 GBV_ILN_2025 GBV_ILN_2026 GBV_ILN_2027 GBV_ILN_2034 GBV_ILN_2044 GBV_ILN_2048 GBV_ILN_2049 GBV_ILN_2050 GBV_ILN_2055 GBV_ILN_2056 GBV_ILN_2059 GBV_ILN_2061 GBV_ILN_2064 GBV_ILN_2088 GBV_ILN_2106 GBV_ILN_2110 GBV_ILN_2111 GBV_ILN_2112 GBV_ILN_2122 GBV_ILN_2129 GBV_ILN_2143 GBV_ILN_2152 GBV_ILN_2153 GBV_ILN_2190 GBV_ILN_2232 GBV_ILN_2336 GBV_ILN_2470 GBV_ILN_2507 GBV_ILN_4035 GBV_ILN_4037 GBV_ILN_4112 GBV_ILN_4125 GBV_ILN_4242 GBV_ILN_4249 GBV_ILN_4251 GBV_ILN_4305 GBV_ILN_4306 GBV_ILN_4307 GBV_ILN_4313 GBV_ILN_4322 GBV_ILN_4323 GBV_ILN_4324 GBV_ILN_4325 GBV_ILN_4326 GBV_ILN_4333 GBV_ILN_4334 GBV_ILN_4338 GBV_ILN_4393 GBV_ILN_4700 51.30 Werkstoffprüfung Werkstoffuntersuchung VZ AR 205
language	English
source	Enthalten in Materials characterization 205 volume:205
sourceStr	Enthalten in Materials characterization 205 volume:205
format_phy_str_mv	Article
bklname	Werkstoffprüfung Werkstoffuntersuchung
institution	findex.gbv.de
topic_facet	Martensitic phase transformations Deformation twinning Crystallographic orientation Electron backscattered diffraction (EBSD) Single crystal
dewey-raw	670
isfreeaccess_bool	false
container_title	Materials characterization
authorswithroles_txt_mv	Singh, Digvijay @@aut@@ Tasaki, Wataru @@aut@@ Yoshinaka, Fumiyoshi @@aut@@ Takamori, Susumu @@aut@@ Emura, Satoshi @@aut@@ Tsuchiya, Koichi @@aut@@ Sawaguchi, Takahiro @@aut@@
publishDateDaySort_date	2023-01-01T00:00:00Z
hierarchy_top_id	302719288
dewey-sort	3670
id	ELV065325761
language_de	englisch
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author	Singh, Digvijay
spellingShingle	Singh, Digvijay ddc 670 bkl 51.30 misc Martensitic phase transformations misc Deformation twinning misc Crystallographic orientation misc Electron backscattered diffraction (EBSD) misc Single crystal Unveiling the transformation pathways of hierarchical γ
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topic_title	670 VZ 51.30 bkl Unveiling the transformation pathways of hierarchical γ Martensitic phase transformations Deformation twinning Crystallographic orientation Electron backscattered diffraction (EBSD) Single crystal
topic	ddc 670 bkl 51.30 misc Martensitic phase transformations misc Deformation twinning misc Crystallographic orientation misc Electron backscattered diffraction (EBSD) misc Single crystal
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title	Unveiling the transformation pathways of hierarchical γ
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title_full	Unveiling the transformation pathways of hierarchical γ
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author_browse	Singh, Digvijay Tasaki, Wataru Yoshinaka, Fumiyoshi Takamori, Susumu Emura, Satoshi Tsuchiya, Koichi Sawaguchi, Takahiro
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title_sort	unveiling the transformation pathways of hierarchical γ
title_auth	Unveiling the transformation pathways of hierarchical γ
abstract	Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process.
abstractGer	Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process.
abstract_unstemmed	Deformation-induced martensitic transformation (γ-austenite → ε-martensite/α’-martensite) in austenitic steels has garnered significant interest owing to its transformation-induced plasticity effect. To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. Moreover, a novel scheme is proposed to index the α’-martensite crystallographic variants at ε-ε intersections by establishing a correlation between the Bain distortion and double shear process.
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title_short	Unveiling the transformation pathways of hierarchical γ
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author2	Tasaki, Wataru Yoshinaka, Fumiyoshi Takamori, Susumu Emura, Satoshi Tsuchiya, Koichi Sawaguchi, Takahiro
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up_date	2024-07-06T22:38:16.282Z
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To elucidate the orientation-dependent intricate γ/ε/α’ phase microstructure at deformation-induced ε-ε intersection, a single crystal of 316 austenitic stainless steel was compressed along the [001]γ axis at a cryogenic temperature (173 K). Electron backscattered diffraction analysis was employed to reveal the deformed microstructure on the (110)γ surface. A hierarchical triple phase structure was discovered at ε–ε intersection, where the γ rotated 90° from the matrix (γ90), { 10 1 ¯ 2 } ε-twin, and α’ phases coexist. Depending on the operative shear angle with a common intersection axis, either 90° (Type I) or 30° (Type II), three distinct atomic rearrangements of the intersection volume were observed: γ90 was present at Type I intersection, and α’-phase was developed at Type II intersection, respectively. { 10 1 ¯ 2 } ε-twin also occurred at Type I intersection, serving as an accommodation mechanism alongside the intersection γ90. EBSD results confirm the Shoji–Nishiyama (SN), Kurdjumov–Sachs (KS), and Burgers (B) orientation relationships within the complex γ – ε – α’ triple phase structures at ε–ε intersection. Transformation paths for three intersection products were visualized by the unified tetrahedron model, considering T/2 or T/3 γ-twinning shear as an intermediate state. 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Unveiling the transformation pathways of hierarchical γ

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